[Title 40 CFR 268]
[Code of Federal Regulations (annual edition) - July 1, 2002 Edition]
[Title 40 - PROTECTION OF ENVIRONMENT]
[Chapter I - ENVIRONMENTAL PROTECTION]
[Subchapter I - SOLID WASTES (CONTINUED)]
[Part 268 - LAND DISPOSAL RESTRICTIONS]
[From the U.S. Government Printing Office]
40PROTECTION OF ENVIRONMENT232002-07-012002-07-01falseLAND DISPOSAL RESTRICTIONS268PART 268PROTECTION OF ENVIRONMENTENVIRONMENTAL PROTECTIONSOLID WASTES (CONTINUED)
PART 268--LAND DISPOSAL RESTRICTIONS--Table of Contents
Subpart A--General
Sec.
268.1 Purpose, scope, and applicability.
268.2 Definitions applicable in this part.
268.3 Dilution prohibited as a substitute for treatment.
268.4 Treatment surface impoundment exemption.
268.5 Procedures for case-by-case extensions to an effective date.
268.6 Petitions to allow land disposal of a waste prohibited under
subpart C of part 268.
268.7 Testing, tracking, and recordkeeping requirements for generators,
treaters, and disposal facilities.
268.8 [Reserved]
268.9 Special rules regarding wastes that exhibit a characteristic.
Subpart B--Schedule for Land Disposal Prohibition and Establishment of
Treatment Standards
268.10-268.12 [Reserved]
268.13 Schedule for wastes identified or listed after November 8, 1984.
268.14 Surface impoundment exemptions.
Subpart C--Prohibitions on Land Disposal
268.30 Waste specific prohibitions--Wood preserving wastes.
268.31 Waste specific prohibitions--Dioxin-containing wastes.
268.32 Waste specific prohibitions--Soils exhibiting the toxicity
characteristic for metals and containing PCBs.
268.33 Waste specific prohibitions--chlorinated aliphatic wastes.
268.34 Waste specific prohibitions--toxicity characteristic metal
wastes.
268.35 Waste specific prohibitions--petroleum refining wastes.
268.36 Waste specific prohibitions--inorganic chemical wastes
268.37 Waste specific prohibitions--ignitable and corrosive
characteristic wastes whose treatment standards were vacated.
268.38 Waste specific prohibitions--newly identified organic toxicity
characteristic wastes and newly listed coke by-product and
chlorotoluene production wastes.
268.39 Waste specific prohibitions--spent aluminum potliners; reactive;
and carbamate wastes.
Subpart D--Treatment Standards
268.40 Applicability of treatment standards.
268.41 Treatment standards expressed as concentrations in waste extract.
268.42 Treatment standards expressed as specified technologies.
268.43 Treatment standards expressed as waste concentrations.
268.44 Variance from a treatment standard.
268.45 Treatment standards for hazardous debris.
268.46 Alternative treatment standards based on HTMR.
268.48 Universal treatment standards.
268.49 Alternative LDR treatment standards for contaminated soil.
Subpart E--Prohibitions on Storage
268.50 Prohibitions on storage of restricted wastes.
Appendixes I-II to Part 268 [Reserved]
Appendix III to Part 268--List of Halogenated Organic Compounds
Regulated Under Sec. 268.32
Appendix IV to Part 268--Wastes Excluded From Lab Packs Under the
Alternative Treatment Standards of Sec. 268.42(c)
Appendix V to Part 268 [Reserved]
Appendix VI to Part 268--Recommended Technologies to Achieve
Deactivation of Characteristics in Section 268.42
Appendix VII to Part 268--LDR Effective Dates of Surface Disposed
Prohibited Hazardous Wastes
Appendix VIII to Part 268--LDR Effective Dates of Injected Prohibited
Hazardous Wastes
Appendix IX to Part 268--Extraction Procedures (EP) Toxicity Test Method
and Structural Integrity Test (Method 1310)
Appendix X to Part 268 [Reserved]
Appendix XI to Part 268--Metal Bearing Wastes Prohibited From Dilution
in a Combustion Unit According to 40 CFR 268.3(c)
Authority: 42 U.S.C. 6905, 6912(a), 6921, and 6924.
[[Page 139]]
Subpart A--General
Sec. 268.1 Purpose, scope, and applicability.
(a) This part identifies hazardous wastes that are restricted from
land disposal and defines those limited circumstances under which an
otherwise prohibited waste may continue to be land disposed.
(b) Except as specifically provided otherwise in this part or part
261 of this chapter, the requirements of this part apply to persons who
generate or transport hazardous waste and owners and operators of
hazardous waste treatment, storage, and disposal facilities.
(c) Restricted wastes may continue to be land disposed as follows:
(1) Where persons have been granted an extension to the effective
date of a prohibition under subpart C of this part or pursuant to
Sec. 268.5, with respect to those wastes covered by the extension;
(2) Where persons have been granted an exemption from a prohibition
pursuant to a petition under Sec. 268.6, with respect to those wastes
and units covered by the petition;
(3) Wastes that are hazardous only because they exhibit a hazardous
characteristic, and which are otherwise prohibited under this part, or
part 148 of this chapter, are not prohibited if the wastes:
(i) Are disposed into a nonhazardous or hazardous injection well as
defined under 40 CFR 146.6(a); and
(ii) Do not exhibit any prohibited characteristic of hazardous waste
identified in 40 CFR part 261, subpart C at the point of injection.
(4) Wastes that are hazardous only because they exhibit a hazardous
characteristic, and which are otherwise prohibited under this part, are
not prohibited if the wastes meet any of the following criteria, unless
the wastes are subject to a specified method of treatment other than
DEACT in Sec. 268.40, or are D003 reactive cyanide:
(i) The wastes are managed in a treatment system which subsequently
discharges to waters of the U.S. pursuant to a permit issued under
section 402 of the Clean Water Act; or
(ii) The wastes are treated for purposes of the pretreatment
requirements of section 307 of the Clean Water Act; or
(iii) The wastes are managed in a zero discharge system engaged in
Clean Water Act-equivalent treatment as defined in Sec. 268.37(a); and
(iv) The wastes no longer exhibit a prohibited characteristic at the
point of land disposal (i.e., placement in a surface impoundment).
(d) The requirements of this part shall not affect the availability
of a waiver under section 121(d)(4) of the Comprehensive Environmental
Response, Compensation, and Liability Act of 1980 (CERCLA).
(e) The following hazardous wastes are not subject to any provision
of part 268:
(1) Waste generated by small quantity generators of less than 100
kilograms of non-acute hazardous waste or less than 1 kilogram of acute
hazardous waste per month, as defined in Sec. 261.5 of this chapter;
(2) Waste pesticides that a farmer disposes of pursuant to
Sec. 262.70;
(3) Wastes identified or listed as hazardous after November 8, 1984
for which EPA has not promulgated land disposal prohibitions or
treatment standards;
(4) De minimis losses of characteristic wastes to wastewaters are
not considered to be prohibited wastes and are defined as losses from
normal material handling operations (e.g. spills from the unloading or
transfer of materials from bins or other containers, leaks from pipes,
valves or other devices used to transfer materials); minor leaks of
process equipment, storage tanks or containers; leaks from well-
maintained pump packings and seals; sample purgings; and relief device
discharges; discharges from safety showers and rinsing and cleaning of
personal safety equipment; rinsate from empty containers or from
containers that are rendered empty by that rinsing; and laboratory
wastes not exceeding one per cent of the total flow of wastewater into
the facility's headworks on an annual basis, or with a combined
annualized average concentration not exceeding one part per million in
the headworks of the facility's wastewater treatment or pretreatment
facility.
(f) Universal waste handlers and universal waste transporters (as
defined in
[[Page 140]]
40 CFR 260.10) are exempt from 40 CFR 268.7 and 268.50 for the hazardous
wastes listed below. These handlers are subject to regulation under 40
CFR part 273.
(1) Batteries as described in 40 CFR 273.2;
(2) Pesticides as described in Sec. 273.3 of this chapter;
(3) Thermostats as described in Sec. 273.4 of this chapter; and
(4) Lamps as described in 40 CFR 273.5.
[51 FR 40638, Nov. 7, 1986; 52 FR 21016, June 4, 1987, as amended at 53
FR 27165, July 19, 1988; 53 FR 31212, Aug. 17, 1988; 54 FR 36970, Sept.
6, 1989; 55 FR 22686, June 1, 1990; 58 FR 29884, May 24, 1993; 59 FR
48043, Sept. 19, 1994; 60 FR 25542, May 11, 1995; 61 FR 15663, Apr. 8,
1996; 61 FR 33682, June 28, 1996; 62 FR 26019, May 12, 1997; 64 FR
36488, July 6, 1999]
Sec. 268.2 Definitions applicable in this part.
When used in this part the following terms have the meanings given
below:
(a) Halogenated organic compounds or HOCs means those compounds
having a carbon-halogen bond which are listed under appendix III to this
part.
(b) Hazardous constituent or constituents means those constituents
listed in appendix VIII to part 261 of this chapter.
(c) Land disposal means placement in or on the land, except in a
corrective action management unit or staging pile, and includes, but is
not limited to, placement in a landfill, surface impoundment, waste
pile, injection well, land treatment facility, salt dome formation, salt
bed formation, underground mine or cave, or placement in a concrete
vault, or bunker intended for disposal purposes.
(d) Nonwastewaters are wastes that do not meet the criteria for
wastewaters in paragraph (f) of this section.
(e) Polychlorinated biphenyls or PCBs are halogenated organic
compounds defined in accordance with 40 CFR 761.3.
(f) Wastewaters are wastes that contain less than 1% by weight total
organic carbon (TOC) and less than 1% by weight total suspended solids
(TSS).
(g) Debris means solid material exceeding a 60 mm particle size that
is intended for disposal and that is: A manufactured object; or plant or
animal matter; or natural geologic material. However, the following
materials are not debris: Any material for which a specific treatment
standard is provided in Subpart D, Part 268, namely lead acid batteries,
cadmium batteries, and radioactive lead solids; Process residuals such
as smelter slag and residues from the treatment of waste, wastewater,
sludges, or air emission residues; and Intact containers of hazardous
waste that are not ruptured and that retain at least 75% of their
original volume. A mixture of debris that has not been treated to the
standards provided by Sec. 268.45 and other material is subject to
regulation as debris if the mixture is comprised primarily of debris, by
volume, based on visual inspection.
(h) Hazardous debris means debris that contains a hazardous waste
listed in subpart D of part 261 of this chapter, or that exhibits a
characteristic of hazardous waste identified in subpart C of part 261 of
this chapter. Any deliberate mixing of prohibited hazardous waste with
debris that changes its treatment classification (i.e., from waste to
hazardous debris) is not allowed under the dilution prohibition in
Sec. 268.3.
(i) Underlying hazardous constituent means any constituent listed in
Sec. 268.48, Table UTS--Universal Treatment Standards, except fluoride,
selenium, sulfides, vanadium, and zinc, which can reasonably be expected
to be present at the point of generation of the hazardous waste at a
concentration above the constituent-specific UTS treatment standards.
(j) Inorganic metal-bearing waste is one for which EPA has
established treatment standards for metal hazardous constituents, and
which does not otherwise contain significant organic or cyanide content
as described in Sec. 268.3(c)(1), and is specifically listed in appendix
XI of this part.
(k) Soil means unconsolidated earth material composing the
superficial geologic strata (material overlying bedrock), consisting of
clay, silt, sand, or gravel size particles as classified by the U.S.
Natural Resources Conservation Service, or a mixture of such materials
with liquids, sludges or solids which is inseparable by simple
mechanical removal processes and is made up primarily of soil by volume
based on
[[Page 141]]
visual inspection. Any deliberate mixing of prohibited hazardous waste
with soil that changes its treatment classification (i.e., from waste to
contaminated soil) is not allowed under the dilution prohibition in
Sec. 268.3.
[55 FR 22686, June 1, 1990, as amended at 56 FR 3877, Jan. 31, 1991; 57
FR 37270, Aug. 18, 1992; 58 FR 8685, Feb. 16, 1993; 58 FR 29884, May 24,
1993; 59 FR 48043, Sept. 19, 1994; 60 FR 244, Jan. 3, 1995; 61 FR 15597,
15662, Apr. 8, 1996; 61 FR 33682, June 28, 1996; 63 FR 28639, May 26,
1998; 63 FR 65940, Nov. 30, 1998; 64 FR 25414, May 11, 1999]
Sec. 268.3 Dilution prohibited as a substitute for treatment.
(a) Except as provided in paragraph (b) of this section, no
generator, transporter, handler, or owner or operator of a treatment,
storage, or disposal facility shall in any way dilute a restricted waste
or the residual from treatment of a restricted waste as a substitute for
adequate treatment to achieve compliance with subpart D of this part, to
circumvent the effective date of a prohibition in subpart C of this
part, to otherwise avoid a prohibition in subpart C of this part, or to
circumvent a land disposal prohibition imposed by RCRA section 3004.
(b) Dilution of wastes that are hazardous only because they exhibit
a characteristic in treatment systems which include land- based units
which treat wastes subsequently discharged to a water of the United
States pursuant to a permit issued under section 402 of the Clean Water
Act (CWA), or which treat wastes in a CWA-equivalent treatment system,
or which treat wastes for the purposes of pretreatment requirements
under section 307 of the CWA is not impermissible dilution for purposes
of this section unless a method other than DEACT has been specified in
Sec. 268.40 as the treatment standard, or unless the waste is a D003
reactive cyanide wastewater or nonwastewater.
(c) Combustion of the hazardous waste codes listed in Appendix XI of
this part is prohibited, unless the waste, at the point of generation,
or after any bona fide treatment such as cyanide destruction prior to
combustion, can be demonstrated to comply with one or more of the
following criteria (unless otherwise specifically prohibited from
combustion):
(1) The waste contains hazardous organic constituents or cyanide at
levels exceeding the constituent-specific treatment standard found in
Sec. 268.48;
(2) The waste consists of organic, debris-like materials (e.g.,
wood, paper, plastic, or cloth) contaminated with an inorganic metal-
bearing hazardous waste;
(3) The waste, at point of generation, has reasonable heating value
such as greater than or equal to 5000 BTU per pound;
(4) The waste is co-generated with wastes for which combustion is a
required method of treatment;
(5) The waste is subject to Federal and/or State requirements
necessitating reduction of organics (including biological agents); or
(6) The waste contains greater than 1% Total Organic Carbon (TOC).
(d) It is a form of impermissible dilution, and therefore
prohibited, to add iron filings or other metallic forms of iron to lead-
containing hazardous wastes in order to achieve any land disposal
restriction treatment standard for lead. Lead-containing wastes include
D008 wastes (wastes exhibiting a characteristic due to the presence of
lead), all characteristic wastes containing lead as an underlying
hazardous constituent, listed wastes containing lead as a regulated
constituent, and hazardous media containing any of the aforementioned
lead-containing wastes.
[61 FR 15663, Apr. 8, 1996, as amended at 61 FR 33682, June 28, 1996; 63
FR 28639, May 26, 1998]
Sec. 268.4 Treatment surface impoundment exemption.
(a) Wastes which are otherwise prohibited from land disposal under
this part may be treated in a surface impoundment or series of
impoundments provided that:
(1) Treatment of such wastes occurs in the impoundments;
(2) The following conditions are met:
(i) Sampling and testing. For wastes with treatment standards in
subpart D of this part and/or prohibition levels in subpart C of this
part or RCRA section 3004(d), the residues from treatment
[[Page 142]]
are analyzed, as specified in Sec. 268.7 or Sec. 268.32, to determine if
they meet the applicable treatment standards or where no treatment
standards have been established for the waste, the applicable
prohibition levels. The sampling method, specified in the waste analysis
plan under Sec. 264.13 or Sec. 265.13, must be designed such that
representative samples of the sludge and the supernatant are tested
separately rather than mixed to form homogeneous samples.
(ii) Removal. The following treatment residues (including any liquid
waste) must be removed at least annually; residues which do not meet the
treatment standards promulgated under subpart D of this part; residues
which do not meet the prohibition levels established under subpart C of
this part or imposed by statute (where no treatment standards have been
established); residues which are from the treatment of wastes prohibited
from land disposal under subpart C of this part (where no treatment
standards have been established and no prohibition levels apply); or
residues from managing listed wastes which are not delisted under
Sec. 260.22 of this chapter. If the volume of liquid flowing through the
impoundment or series of impoundments annually is greater than the
volume of the impoundment or impoundments, this flow-through constitutes
removal of the supernatant for the purpose of this requirement.
(iii) Subsequent management. Treatment residues may not be placed in
any other surface impoundment for subsequent management.
(iv) Recordkeeping. Sampling and testing and recordkeeping
provisions of Secs. 264.13 and 265.13 of this chapter apply.
(3) The impoundment meets the design requirements of Sec. 264.221(c)
or Sec. 265.221(a) of this chapter, regardless that the unit may not be
new, expanded, or a replacement, and be in compliance with applicable
ground water monitoring requirements of subpart F of part 264 or part
264 of this chapter unless:
(i) Exempted pursuant to Sec. 264.221 (d) or (e) of this chapter, or
to Sec. 265.221 (c) or (d) of this chapter; or,
(ii) Upon application by the owner or operator, the Administrator,
after notice and an opportunity to comment, has granted a waiver of the
requirements on the basis that the surface impoundment:
(A) Has at least one liner, for which there is no evidence that such
liner is leaking;
(B) Is located more than one-quarter mile from an underground source
of drinking water; and
(C) Is in compliance with generally applicable ground water
monitoring requirements for facilities with permits; or,
(iii) Upon application by the owner or operator, the Administrator,
after notice and an opportunity to comment, has granted a modification
to the requirements on the basis of a demonstration that the surface
impoundment is located, designed, and operated so as to assure that
there will be no migration of any hazardous constituent into ground
water or surface water at any future time.
(4) The owner or operator submits to the Regional Administrator a
written certification that the requirements of Sec. 268.4(a)(3) have
been met. The following certification is required:
I certify under penalty of law that the requirements of 40 CFR
268.4(a)(3) have been met for all surface impoundments being used to
treat restricted wastes. I believe that the submitted information is
true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of
fine and imprisonment.
(b) Evaporation of hazardous constituents as the principal means of
treatment is not considered to be treatment for purposes of an exemption
under this section.
[51 FR 40638, Nov. 7, 1986; 52 FR 21016, June 4, 1987, as amended at 52
FR 25788, July 8, 1987; 53 FR 31212, Aug. 17, 1988; 62 FR 26019, May 12,
1997; 63 FR 28639, May 26, 1998]
Sec. 268.5 Procedures for case-by-case extensions to an effective date.
(a) Any person who generates, treats, stores, or disposes of a
hazardous waste may submit an application to the Administrator for an
extension to the effective date of any applicable restriction
established under subpart C of this part. The applicant must demonstrate
the following:
[[Page 143]]
(1) He has made a good-faith effort to locate and contract with
treatment, recovery, or disposal facilities nationwide to manage his
waste in accordance with the effective date of the applicable
restriction established under subpart C of this part;
(2) He has entered into a binding contractual commitment to
construct or otherwise provide alternative treatment, recovery (e.g.,
recycling), or disposal capacity that meets the treatment standards
specified in subpart D or, where treatment standards have not been
specified, such treatment, recovery, or disposal capacity is protective
of human health and the environment.
(3) Due to circumstances beyond the applicant's control, such
alternative capacity cannot reasonably be made available by the
applicable effective date. This demonstration may include a showing that
the technical and practical difficulties associated with providing the
alternative capacity will result in the capacity not being available by
the applicable effective date;
(4) The capacity being constructed or otherwise provided by the
applicant will be sufficient to manage the entire quantity of waste that
is the subject of the application;
(5) He provides a detailed schedule for obtaining required operating
and construction permits or an outline of how and when alternative
capacity will be available;
(6) He has arranged for adequate capacity to manage his waste during
an extension and has documented in the application the location of all
sites at which the waste will be managed; and
(7) Any waste managed in a surface impoundment or landfill during
the extension period will meet the requirements of paragraph (h)(2) of
this section.
(b) An authorized representative signing an application described
under paragraph (a) of this section shall make the following
certification:
I certify under penalty of law that I have personally examined and
am familiar with the information submitted in this document and all
attachments and that, based on my inquiry of those individuals
immediately responsible for obtaining the information, I believe that
the information is true, accurate, and complete. I am aware that there
are significant penalties for submitting false information, including
the possibility of fine and imprisonment.
(c) After receiving an application for an extension, the
Administrator may request any additional information which he deems as
necessary to evaluate the application.
(d) An extension will apply only to the waste generated at the
individual facility covered by the application and will not apply to
restricted waste from any other facility.
(e) On the basis of the information referred to in paragraph (a) of
this section, after notice and opportunity for comment, and after
consultation with appropriate State agencies in all affected States, the
Administrator may grant an extension of up to 1 year from the effective
date. The Administrator may renew this extension for up to 1 additional
year upon the request of the applicant if the demonstration required in
paragraph (a) of this section can still be made. In no event will an
extension extend beyond 24 months from the applicable effective date
specified in subpart C of part 268. The length of any extension
authorized will be determined by the Administrator based on the time
required to construct or obtain the type of capacity needed by the
applicant as described in the completion schedule discussed in paragraph
(a)(5) of this section. The Administrator will give public notice of the
intent to approve or deny a petition and provide an opportunity for
public comment. The final decision on a petition will be published in
the Federal Register.
(f) Any person granted an extension under this section must
immediately notify the Administrator as soon as he has knowledge of any
change in the conditions certified to in the application.
(g) Any person granted an extension under this section shall submit
written progress reports at intervals designated by the Administrator.
Such reports must describe the overall progress made toward constructing
or otherwise providing alternative treatment, recovery or disposal
capacity; must identify any event which may cause or has caused a delay
in the development of the capacity; and must
[[Page 144]]
summarize the steps taken to mitigate the delay. The Administrator can
revoke the extension at any time if the applicant does not demonstrate a
good-faith effort to meet the schedule for completion, if the Agency
denies or revokes any required permit, if conditions certified in the
application change, or for any violation of this chapter.
(h) Whenever the Administrator establishes an extension to an
effective date under this section, during the period for which such
extension is in effect:
(1) The storage restrictions under Sec. 268.50(a) do not apply; and
(2) Such hazardous waste may be disposed in a landfill or surface
impoundment only if such unit is in compliance with the technical
requirements of the following provisions regardless of whether such unit
is existing, new, or a replacement or lateral expansion.
(i) The landfill, if in interim status, is in compliance with the
requirements of subpart F of part 265 and Sec. 265.301 (a), (c), and (d)
of this chapter; or,
(ii) The landfill, if permitted, is in compliance with the
requirements of subpart F of part 264 and Sec. 264.301 (c), (d) and (e)
of this chapter; or
(iii) The surface impoundment, if in interim status, is in
compliance with the requirements of subpart F of part 265, Sec. 265.221
(a), (c), and (d) of this chapter, and RCRA section 3005(j)(1); or
(iv) The surface impoundment, if permitted, is in compliance with
the requirements of subpart F of part 264 and Sec. 264.221 (c), (d) and
(e) of this chapter; or
(v) The surface impoundment, if newly subject to RCRA section
3005(j)(1) due to the promulgation of additional listings or
characteristics for the identification of hazardous waste, is in
compliance with the requirements of subpart F of part 265 of this
chapter within 12 months after the promulgation of additional listings
or characteristics of hazardous waste, and with the requirements of
Sec. 265.221 (a), (c) and (d) of this chapter within 48 months after the
promulgation of additional listings or characteristics of hazardous
waste. If a national capacity variance is granted, during the period the
variance is in effect, the surface impoundment, if newly subject to RCRA
section 3005(j)(1) due to the promulgation of additional listings or
characteristics of hazardous waste, is in compliance with the
requirements of subpart F of part 265 of this chapter within 12 months
after the promulgation of additional listings or characteristics of
hazardous waste, and with the requirements of Sec. 265.221 (a), (c) and
(d) of this chapter within 48 months after the promulgation of
additional listings or characteristics of hazardous waste; or
(vi) The landfill, if disposing of containerized liquid hazardous
wastes containing PCBs at concentrations greater than or equal to 50 ppm
but less than 500 ppm, is also in compliance with the requirements of 40
CFR 761.75 and parts 264 and 265.
(i) Pending a decision on the application the applicant is required
to comply with all restrictions on land disposal under this part once
the effective date for the waste has been reached.
[51 FR 40638, Nov. 7, 1986; 52 FR 21016, June 4, 1987, as amended at 52
FR 25788, July 8, 1987; 54 FR 36971, Sept. 6, 1989; 55 FR 23935, June
13, 1990; 57 FR 37270, Aug. 18, 1992]
Sec. 268.6 Petitions to allow land disposal of a waste prohibited under subpart C of part 268.
(a) Any person seeking an exemption from a prohibition under subpart
C of this part for the disposal of a restricted hazardous waste in a
particular unit or units must submit a petition to the Administrator
demonstrating, to a reasonable degree of certainty, that there will be
no migration of hazardous constituents from the disposal unit or
injection zone for as long as the wastes remain hazardous. The
demonstration must include the following components:
(1) An identification of the specific waste and the specific unit
for which the demonstration will be made;
(2) A waste analysis to describe fully the chemical and physical
characteristics of the subject waste;
(3) A comprehensive characterization of the disposal unit site
including an analysis of background air, soil, and water quality.
(4) A monitoring plan that detects migration at the earliest
practicable time;
[[Page 145]]
(5) Sufficient information to assure the Administrator that the
owner or operator of a land disposal unit receiving restricted waste(s)
will comply with other applicable Federal, State, and local laws.
(b) The demonstration referred to in paragraph (a) of this section
must meet the following criteria:
(1) All waste and environmental sampling, test, and analysis data
must be accurate and reproducible to the extent that state-of-the-art
techniques allow;
(2) All sampling, testing, and estimation techniques for chemical
and physical properties of the waste and all environmental parameters
must have been approved by the Administrator;
(3) Simulation models must be calibrated for the specific waste and
site conditions, and verified for accuracy by comparison with actual
measurements;
(4) A quality assurance and quality control plan that addresses all
aspects of the demonstration must be approved by the Administrator; and,
(5) An analysis must be performed to identify and quantify any
aspects of the demonstration that contribute significantly to
uncertainty. This analysis must include an evaluation of the
consequences of predictable future events, including, but not limited
to, earthquakes, floods, severe storm events, droughts, or other natural
phenomena.
(c) Each petition referred to in paragraph (a) of this section must
include the following:
(1) A monitoring plan that describes the monitoring program
installed at and/or around the unit to verify continued compliance with
the conditions of the variance. This monitoring plan must provide
information on the monitoring of the unit and/or the environment around
the unit. The following specific information must be included in the
plan:
(i) The media monitored in the cases where monitoring of the
environment around the unit is required;
(ii) The type of monitoring conducted at the unit, in the cases
where monitoring of the unit is required;
(iii) The location of the monitoring stations;
(iv) The monitoring interval (frequency of monitoring at each
station);
(v) The specific hazardous constituents to be monitored;
(vi) The implementation schedule for the monitoring program;
(vii) The equipment used at the monitoring stations;
(viii) The sampling and analytical techniques employed; and
(ix) The data recording/reporting procedures.
(2) Where applicable, the monitoring program described in paragraph
(c)(1) of this section must be in place for a period of time specified
by the Administrator, as part of his approval of the petition, prior to
receipt of prohibited waste at the unit.
(3) The monitoring data collected according to the monitoring plan
specified under paragraph (c)(1) of this section must be sent to the
Administrator according to a format and schedule specified and approved
in the monitoring plan, and
(4) A copy of the monitoring data collected under the monitoring
plan specified under paragraph (c)(1) of this section must be kept on-
site at the facility in the operating record.
(5) The monitoring program specified under paragraph (c)(1) of this
section meet the following criteria:
(i) All sampling, testing, and analytical data must be approved by
the Administrator and must provide data that is accurate and
reproducible.
(ii) All estimation and monitoring techniques must be approved by
the Administrator.
(iii) A quality assurance and quality control plan addressing all
aspects of the monitoring program must be provided to and approved by
the Administrator.
(d) Each petition must be submitted to the Administrator.
(e) After a petition has been approved, the owner or operator must
report any changes in conditions at the unit and/or the environment
around the unit that significantly depart from the conditions described
in the variance and affect the potential for migration of hazardous
constituents from the units as follows:
(1) If the owner or operator plans to make changes to the unit
design, construction, or operation, such a change must be proposed, in
writing, and the
[[Page 146]]
owner or operator must submit a demonstration to the Administrator at
least 30 days prior to making the change. The Administrator will
determine whether the proposed change invalidates the terms of the
petition and will determine the appropriate response. Any change must be
approved by the Administrator prior to being made.
(2) If the owner or operator discovers that a condition at the site
which was modeled or predicted in the petition does not occur as
predicted, this change must be reported, in writing, to the
Administrator within 10 days of discovering the change. The
Administrator will determine whether the reported change from the terms
of the petition requires further action, which may include termination
of waste acceptance and revocation of the petition, petition
modifications, or other responses.
(f) If the owner or operator determines that there is migration of
hazardous constituent(s) from the unit, the owner or operator must:
(1) Immediately suspend receipt of prohibited waste at the unit, and
(2) Notify the Administrator, in writing, within 10 days of the
determination that a release has occurred.
(3) Following receipt of the notification the Administrator will
determine, within 60 days of receiving notification, whether the owner
or operator can continue to receive prohibited waste in the unit and
whether the variance is to be revoked. The Administrator shall also
determine whether further examination of any migration is warranted
under applicable provisions of part 264 or part 265.
(g) Each petition must include the following statement signed by the
petitioner or an authorized representative:
I certify under penalty of law that I have personally examined and am
familiar with the information submitted in this petition and all
attached documents, and that, based on my inquiry of those individuals
immediately responsible for obtaining the information, I believe that
submitted information is true, accurate, and complete. I am aware that
there are significant penalties for submitting false information,
including the possibility of fine and imprisonment.
(h) After receiving a petition, the Administrator may request any
additional information that reasonably may be required to evaluate the
demonstration.
(i) If approved, the petition will apply to land disposal of the
specific restricted waste at the individual disposal unit described in
the demonstration and will not apply to any other restricted waste at
that disposal unit, or to that specific restricted waste at any other
disposal unit.
(j) The Administrator will give public notice in the Federal
Register of the intent to approve or deny a petition and provide an
opportunity for public comment. The final decision on a petition will be
published in the Federal Register.
(k) The term of a petition granted under this section shall be no
longer than the term of the RCRA permit if the disposal unit is
operating under a RCRA permit, or up to a maximum of 10 years from the
date of approval provided under paragraph (g) of this section if the
unit is operating under interim status. In either case, the term of the
granted petition shall expire upon the termination or denial of a RCRA
permit, or upon the termination of interim status or when the volume
limit of waste to be land disposed during the term of petition is
reached.
(l) Prior to the Administrator's decision, the applicant is required
to comply with all restrictions on land disposal under this part once
the effective date for the waste has been reached.
(m) The petition granted by the Administrator does not relieve the
petitioner of his responsibilities in the management of hazardous waste
under 40 CFR part 260 through part 271.
(n) Liquid hazardous wastes containing polychlorinated biphenyls at
concentrations greater than or equal to 500 ppm are not eligible for an
exemption under this section.
[51 FR 40638, Nov. 7, 1986; 52 FR 21016, June 4, 1987, as amended at 52
FR 25789, July 8, 1987; 53 FR 31212, Aug. 17, 1988; 54 FR 36971, Sept.
6, 1989]
[[Page 147]]
Sec. 268.7 Testing, tracking, and recordkeeping requirements for generators, treaters, and disposal facilities.
(a) Requirements for generators: (1) A generator of hazardous waste
must determine if the waste has to be treated before it can be land
disposed. This is done by determining if the hazardous waste meets the
treatment standards in Sec. 268.40, Sec. 268.45, or Sec. 268.49. This
determination can be made in either of two ways: testing the waste or
using knowledge of the waste. If the generator tests the waste, testing
would normally determine the total concentration of hazardous
constituents, or the concentration of hazardous constituents in an
extract of the waste obtained using test method 1311 in ``Test Methods
of Evaluating Solid Waste, Physical/Chemical Methods,'' EPA Publication
SW-846, as referenced in Sec. 260.11 of this chapter, depending on
whether the treatment standard for the waste is expressed as a total
concentration or concentration of hazardous constituent in the waste's
extract. In addition, some hazardous wastes must be treated by
particular treatment methods before they can be land disposed and some
soils are contaminated by such hazardous wastes. These treatment
standards are also found in Sec. 268.40, and are described in detail in
Sec. 268.42, Table 1. These wastes, and solids contaminated with such
wastes, do not need to be tested (however, if they are in a waste
mixture, other wastes with concentration level treatment standards would
have to be tested). If a generator determines they are managing a waste
or soil contamination with a waste, that displays a hazardous
characteristic of ignitability, corrosivity, reactivity, or toxicity,
they must comply with the special requirements of Sec. 268.9 of this
part in addition to any applicable requirements in this section.
(2) If the waste or contaminated soil does not meet the treatment
standard: With the initial shipment of waste to each treatment or
storage facility, the generator must send a one-time written notice to
each treatment or storage facility receiving the waste, and place a copy
in the file. The notice must include the information in column
``268.7(a)(2)'' of the Generator Paperwork Requirements Table in
Sec. 268.7(a)(4). No further notification is necessary until such time
that the waste or facility change, in which case a new notification must
be sent and a copy placed in the generator's file.
(i) For contaminated soil, the following certification statement
should be included, signed by an authorized representative:
I certify under penalty of law that I personally have examined this
contaminated soil and it [does/does not] contain listed hazardous waste
and [does/does not] exhibit a characteristic of hazardous waste and
requires treatment to meet the soil treatment standards as provided by
268.49(c).
(ii) [Reserved]
(3) If the waste or contaminated soil meets the treatment standard
at the original point of generation:
(i) With the initial shipment of waste to each treatment, storage,
or disposal facility, the generator must send a one-time written notice
to each treatment, storage, or disposal facility receiving the waste,
and place a copy in the file. The notice must include the information
indicated in column ``268.7(a)(3)'' of the Generator Paperwork
Requirements Table in Sec. 268.7(a)(4) and the following certification
statement, signed by an authorized representative:
I certify under penalty of law that I personally have examined and
am familiar with the waste through analysis and testing or through
knowledge of the waste to support this certification that the waste
complies with the treatment standards specified in 40 CFR part 268
subpart D. I believe that the information I submitted is true, accurate,
and complete. I am aware that there are significant penalties for
submitting a false certification, including the possibility of a fine
and imprisonment.
(ii) For contaminated soil, with the initial shipment of wastes to
each treatment, storage, or disposal facility, the generator must send a
one-time written notice to each facility receiving the waste and place a
copy in the file. The notice must include the information in
``268.7(a)(3) of the Generator Paperwork Requirements Table in
Sec. 268.7(a)(4).
(iii) If the waste changes, the generator must send a new notice and
certification to the receiving facility, and
[[Page 148]]
place a copy in their files. Generators of hazardous debris excluded
from the definition of hazardous waste under Sec. 261.3(f) of this
chapter are not subject to these requirements.
(4) For reporting, tracking, and recordkeeping when exceptions allow
certain wastes or contaminated soil that do not meet the treatment
standards to be land disposed: There are certain exemptions from the
requirement that hazardous wastes or contaminated soil meet treatment
standards before they can be land disposed. These include, but are not
limited to case-by-case extensions under Sec. 268.5, disposal in a no-
migration unit under Sec. 268.6, or a national capacity variance or
case-by-case capacity variance under subpart C of this part. If a
generator's waste is so exempt, then with the initial shipment of waste,
the generator must send a one-time written notice to each land disposal
facility receiving the waste. The notice must include the information
indicated in column ``268.7(a)(4)'' of the Generator Paperwork
Requirements Table below. If the waste changes, the generator must send
a new notice to the receiving facility, and place a copy in their files.
Generator Paperwork Requirements Table
----------------------------------------------------------------------------------------------------------------
Sec. 268.7 Sec. 268.7 Sec. 268.7 Sec. 268.7
Required information (a)(2) (a)(3) (a)(4) (a)(9)
----------------------------------------------------------------------------------------------------------------
1. EPA Hazardous Waste Numbers and Manifest Number of [b r r r
<] <] <] <]
2. Statement: this waste is not prohibited from land [b
<]
3. The waste is subject to the LDRs. The constituents of [b r
hazardous constituents in characteristic wastes, unless <] <]
the waste will be treated and monitored for all
constituents. If all constituents will be treated and
monitored, there is no need to put them all on the LDR
notice.................................................
4. The notice must include the applicable wastewater/ [b r
and subdivisions made within a waste code based on <] <]
waste-specific criteria (such as D003 reactive cyanide)
5. Waste analysis data (when available)................. [b r r
<] <] <]
6. Date the waste is subject to the prohibition......... [b
<]
7. For hazardous debris, when treating with the [b r
268.45: the contaminants subject to treatment, as <] <]
described in Sec. 268.45(b); and an indication that
these contaminants are being treated to comply with
Sec. 268.45...........................................
8. For contaminated soil subject to LDRs as provided in [b r
as described in Sec. 268.49(d), and the following <] <]
statement: This contaminated soil [does/does not]
contain listed hazardous waste and [does/does not]
exhibit a characteristic of hazardous waste and [is
subject to/complies with the soil treatment standards
as provided by Sec. 268.49(c) or the universal
treatment standards....................................
9. A certification is needed (see applicable section for [b r
<] <]
----------------------------------------------------------------------------------------------------------------
(5) If a generator is managing and treating prohibited waste or
contaminated soil in tanks, containers, or containment buildings
regulated under 40 CFR 262.34 to meet applicable LDR treatment standards
found at Sec. 268.40, the generator must develop and follow a written
waste analysis plan which describes the procedures they will carry out
to comply with the treatment standards. (Generators treating hazardous
debris under the alternative treatment standards of Table 1,
Sec. 268.45, however, are not subject to these waste analysis
requirements.) The plan must be kept on site in the generator's records,
and the following requirements must be met:
(i) The waste analysis plan must be based on a detailed chemical and
physical analysis of a representative sample of the prohibited waste(s)
being treated, and contain all information necessary to treat the
waste(s) in accordance with the requirements of this part, including the
selected testing frequency.
(ii) Such plan must be kept in the facility's on-site files and made
available to inspectors.
(iii) Wastes shipped off-site pursuant to this paragraph must comply
with
[[Page 149]]
the notification requirements of Sec. 268.7(a)(3).
(6) If a generator determines that the waste or contaminated soil is
restricted based solely on his knowledge of the waste, all supporting
data used to make this determination must be retained on-site in the
generator's files. If a generator determines that the waste is
restricted based on testing this waste or an extract developed using the
test method 1311 in ``Test Methods for Evaluating Solid Waste, Physical/
Chemical Methods,'' EPA Publication SW-846, as referenced in Sec. 260.11
of this chapter, and all waste analysis data must be retained on-site in
the generator's files.
(7) If a generator determines that he is managing a prohibited waste
that is excluded from the definition of hazardous or solid waste or is
exempted from Subtitle C regulation under 40 CFR 261.2 through 261.6
subsequent to the point of generation (including deactivated
characteristic hazardous wastes managed in wastewater treatment systems
subject to the Clean Water Act (CWA) as specified at 40 CFR 261.4(a)(2)
or that are CWA-equivalent, or are managed in an underground injection
well regulated by the SDWA), he must place a one-time notice describing
such generation, subsequent exclusion from the definition of hazardous
or solid waste or exemption from RCRA Subtitle C regulation, and the
disposition of the waste, in the facility's on-site files.
(8) Generators must retain on-site a copy of all notices,
certifications, waste analysis data, and other documentation produced
pursuant to this section for at least three years from the date that the
waste that is the subject of such documentation was last sent to on-site
or off-site treatment, storage, or disposal. The three year record
retention period is automatically extended during the course of any
unresolved enforcement action regarding the regulated activity or as
requested by the Administrator. The requirements of this paragraph apply
to solid wastes even when the hazardous characteristic is removed prior
to disposal, or when the waste is excluded from the definition of
hazardous or solid waste under 40 CFR 261.2 through 261.6, or exempted
from Subtitle C regulation, subsequent to the point of generation.
(9) If a generator is managing a lab pack containing hazardous
wastes and wishes to use the alternative treatment standard for lab
packs found at Sec. 268.42(c):
(i) With the initial shipment of waste to a treatment facility, the
generator must submit a notice that provides the information in column
``Sec. 268.7(a)(9)'' in the Generator Paperwork Requirements Table of
paragraph (a)(4) of this section, and the following certification. The
certification, which must be signed by an authorized representative and
must be placed in the generator's files, must say the following:
I certify under penalty of law that I personally have examined and
am familiar with the waste and that the lab pack contains only wastes
that have not been excluded under appendix IV to 40 CFR part 268 and
that this lab pack will be sent to a combustion facility in compliance
with the alternative treatment standards for lab packs at 40 CFR
268.42(c). I am aware that there are significant penalties for
submitting a false certification, including the possibility of fine or
imprisonment.
(ii) No further notification is necessary until such time that the
wastes in the lab pack change, or the receiving facility changes, in
which case a new notice and certification must be sent and a copy placed
in the generator's file.
(iii) If the lab pack contains characteristic hazardous wastes
(D001-D043), underlying hazardous constituents (as defined in
Sec. 268.2(i)) need not be determined.
(iv) The generator must also comply with the requirements in
paragraphs (a)(6) and (a)(7) of this section.
(10) Small quantity generators with tolling agreements pursuant to
40 CFR 262.20(e) must comply with the applicable notification and
certification requirements of paragraph (a) of this section for the
initial shipment of the waste subject to the agreement. Such generators
must retain on-site a copy of the notification and certification,
together with the tolling agreement, for at least three years after
termination or expiration of the agreement. The three-year record
retention period is automatically extended during the
[[Page 150]]
course of any unresolved enforcement action regarding the regulated
activity or as requested by the Administrator.
(b) Treatment facilities must test their wastes according to the
frequency specified in their waste analysis plans as required by 40 CFR
264.13 (for permitted TSDs) or 40 CFR 265.13 (for interim status
facilities). Such testing must be performed as provided in paragraphs
(b)(1), (b)(2) and (b)(3) of this section.
(1) For wastes or contaminated soil with treatment standards
expressed in the waste extract (TCLP), the owner or operator of the
treatment facility must test an extract of the treatment residues, using
test method 1311 (the Toxicity Characteristic Leaching Procedure,
described in ``Test Methods for Evaluating Solid Waste, Physical/
Chemical Methods,'' EPA Publication SW-846 as incorporated by reference
in Sec. 260.11 of this chapter) to assure that the treatment residues
extract meet the applicable treatment standards.
(2) For wastes or contaminated soil with treatment standards
expressed as concentrations in the waste, the owner or operator of the
treatment facility must test the treatment residues (not an extract of
such residues) to assure that they meet the applicable treatment
standards.
(3) A one-time notice must be sent with the initial shipment of
waste or contaminated soil to the land disposal facility. A copy of the
notice must be placed in the treatment facility's file.
(i) No further notification is necessary until such time that the
waste or receiving facility change, in which case a new notice must be
sent and a copy placed in the treatment facility's file.
(ii) The one-time notice must include these requirements:
Treatment Facility Paperwork Requirements Table
------------------------------------------------------------------------
Required information Sec. 268.7(b)
------------------------------------------------------------------------
1. EPA Hazardous Waste Numbers and Manifest Number of [b
first shipment......................................... <]
2. The waste is subject to the LDRs. The constituents of [b
concern for F001-F005, and F039, and underlying <]
hazardous constituents in characteristic wastes, unless
the waste will be treated and monitored for all
constituents. If all constituents will be treated and
monitored, there is no need to put them all on the LDR
notice.................................................
3. The notice must include the applicable wastewater/ [b
nonwastewater category (see Secs. 268.2(d) and (f)) <]
and subdivisions made within a waste code based on
waste-specific criteria (such as D003 reactive cyanide)
4. Waste analysis data (when available)................. [b
<]
5. For contaminated soil subject to LDRs as provided in [b
268.49(a), the constituents subject to treatment as <]
described in 268.49(d) and the following statement,
``this contaminated soil [does/does not] exhibit a
characteristic of hazardous waste and [is subject to/
complies with] the soil treatment standards as provided
by 268.49(c)...........................................
6. A certification is needed (see applicable section for [b
exact wording)......................................... <]
------------------------------------------------------------------------
(4) The treatment facility must submit a one-time certification
signed by an authorized representative with the initial shipment of
waste or treatment residue of a restricted waste to the land disposal
facility. The certification must state:
I certify under penalty of law that I have personally examined and
am familiar with the treatment technology and operation of the treatment
process used to support this certification. Based on my inquiry of those
individuals immediately responsible for obtaining this information, I
believe that the treatment process has been operated and maintained
properly so as to comply with the treatment standards specified in 40
CFR 268.40 without impermissible dilution of the prohibited waste. I am
aware there are significant penalties for submitting a false
certification, including the possibility of fine and imprisonment.
A certification is also necessary for contaminated soil and it must
state:
I certify under penalty of law that I have personally examined and
am familiar with the treatment technology and operation of the treatment
process used to support this certification and believe that it has been
maintained and operated properly so as to comply with treatment
standards specified in 40 CFR 268.49 without impermissible dilution of
the prohibited wastes. I am aware there are significant penalties for
submitting a false certification, including the possibility of fine and
imprisonment.
(i) A copy of the certification must be placed in the treatment
facility's on-site files. If the waste or treatment
[[Page 151]]
residue changes, or the receiving facility changes, a new certification
must be sent to the receiving facility, and a copy placed in the file.
(ii) Debris excluded from the definition of hazardous waste under
Sec. 261.3(e) of this chapter (i.e., debris treated by an extraction or
destruction technology provided by Table 1, Sec. 268.45, and debris that
the Director has determined does not contain hazardous waste), however,
is subject to the notification and certification requirements of
paragraph (d) of this section rather than the certification requirements
of this paragraph.
(iii) For wastes with organic constituents having treatment
standards expressed as concentration levels, if compliance with the
treatment standards is based in whole or in part on the analytical
detection limit alternative specified in Sec. 268.40(d), the
certification, signed by an authorized representative, must state the
following:
I certify under penalty of law that I have personally examined and
am familiar with the treatment technology and operation of the treatment
process used to support this certification. Based on my inquiry of those
individuals immediately responsible for obtaining this information, I
believe that the nonwastewater organic constituents have been treated by
combustion units as specified in 268.42, Table 1. I have been unable to
detect the nonwastewater organic constituents, despite having used best
good-faith efforts to analyze for such constituents. I am aware there
are significant penalties for submitting a false certification,
including the possibility of fine and imprisonment.
(iv) For characteristic wastes that are subject to the treatment
standards in Sec. 268.40 (other than those expressed as a method of
treatment), or Sec. 268.49, and that contain underlying hazardous
constituents as defined in Sec. 268.2(i); if these wastes are treated
on-site to remove the hazardous characteristic; and are then sent off-
site for treatment of underlying hazardous constituents, the
certification must state the following:
I certify under penalty of law that the waste has been treated in
accordance with the requirements of 40 CFR 268.40 or 268.49 to remove
the hazardous characteristic. This decharacterized waste contains
underlying hazardous constituents that require further treatment to meet
treatment standards. I am aware that there are significant penalties for
submitting a false certification, including the possibility of fine and
imprisonment.
(v) For characteristic wastes that contain underlying hazardous
constituents as defined Sec. 268.2(i) that are treated on-site to remove
the hazardous characteristic to treat underlying hazardous constituents
to levels in Sec. 268.48 Universal Treatment Standards, the
certification must state the following:
I certify under penalty of law that the waste has been treated in
accordance with the requirements of 40 CFR 268.40 to remove the
hazardous characteristic and that underlying hazardous constituents, as
defined in Sec. 268.2(i) have been treated on-site to meet the
Sec. 268.48 Universal Treatment Standards. I am aware that there are
significant penalties for submitting a false certification, including
the possibility of fine and imprisonment.
(5) If the waste or treatment residue will be further managed at a
different treatment, storage, or disposal facility, the treatment,
storage, or disposal facility sending the waste or treatment residue
off-site must comply with the notice and certification requirements
applicable to generators under this section.
(6) Where the wastes are recyclable materials used in a manner
constituting disposal subject to the provisions of Sec. 268.20(b)
regarding treatment standards and prohibition levels, the owner or
operator of a treatment facility (i.e., the recycler) is not required to
notify the receiving facility, pursuant to paragraph (b)(3) of this
section. With each shipment of such wastes the owner or operator of the
recycling facility must submit a certification described in paragraph
(b)(4) of this section, and a notice which includes the information
listed in paragraph (b)(3) of this section (except the manifest number)
to the Regional Administrator, or his delegated representative. The
recycling facility also must keep records of the name and location of
each entity receiving the hazardous waste-derived product.
(c) Except where the owner or operator is disposing of any waste
that is a recyclable material used in a manner constituting disposal
pursuant to 40 CFR 266.20(b), the owner or operator of any land disposal
facility disposing any waste subject to restrictions under this part
must:
[[Page 152]]
(1) Have copies of the notice and certifications specified in
paragraph (a) or (b) of this section.
(2) Test the waste, or an extract of the waste or treatment residue
developed using test method 1311 (the Toxicity Characteristic Leaching
Procedure), described in ``Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods,'' EPA Publication SW-846 as incorporated by
reference in Sec. 260.11 of this chapter), to assure that the wastes or
treatment residues are in compliance with the applicable treatment
standards set forth in subpart D of this part. Such testing must be
performed according to the frequency specified in the facility's waste
analysis plan as required by Sec. 264.13 or Sec. 265.13 of this chapter.
(d) Generators or treaters who first claim that hazardous debris is
excluded from the definition of hazardous waste under Sec. 261.3(e) of
this chapter (i.e., debris treated by an extraction or destruction
technology provided by Table 1, Sec. 268.45, and debris that the EPA
Regional Administrator (or his designated representative) or State
authorized to implement part 268 requirements has determined does not
contain hazardous waste) are subject to the following notification and
certification requirements:
(1) A one-time notification, including the following information,
must be submitted to the EPA Regional hazardous waste management
division director (or his designated representative) or State authorized
to implement part 268 requirements, or State authorized to implement
part 268 requirements:
(2) The notification must be updated if the debris is shipped to a
different facility, and, for debris excluded under Sec. 261.2(e)(1) of
this chapter, if a different type of debris is treated or if a different
technology is used to treat the debris.
(3) For debris excluded under Sec. 261.3(e)(1) of this chapter, the
owner or operator of the treatment facility must document and certify
compliance with the treatment standards of Table 1, Sec. 268.45, as
follows:
(i) Records must be kept of all inspections, evaluations, and
analyses of treated debris that are made to determine compliance with
the treatment standards;
(ii) Records must be kept of any data or information the treater
obtains during treatment of the debris that identifies key operating
parameters of the treatment unit; and
(iii) For each shipment of treated debris, a certification of
compliance with the treatment standards must be signed by an authorized
representative and placed in the facility's files. The certification
must state the following: ``I certify under penalty of law that the
debris has been treated in accordance with the requirements of 40 CFR
268.45. I am aware that there are significant penalties for making a
false certification, including the possibility of fine and
imprisonment.''
(e) Generators and treaters who first receive from EPA or an
authorized state a determination that a given contaminated soil subject
to LDRs as provided in Sec. 268.49(a) no longer contains a listed
hazardous waste and generators and treaters who first determine that a
contaminated soil subject to LDRs as provided in Sec. 268.49(a) no
longer exhibits a characteristic of hazardous waste must:
(1) Prepare a one-time only documentation of these determinations
including all supporting information; and,
(2) Maintain that information in the facility files and other
records for a minimum of three years.
[51 FR 40638, Nov. 7, 1986; 52 FR 21016, June 4, 1987]
Editorial Note: For Federal Register citations affecting Sec. 268.7,
see the List of CFR Sections Affected, which appears in the Finding Aids
section of the printed volume and on GPO Access.
Sec. 268.8 [Reserved]
Sec. 268.9 Special rules regarding wastes that exhibit a characteristic.
(a) The initial generator of a solid waste must determine each EPA
Hazardous Waste Number (waste code) applicable to the waste in order to
determine the applicable treatment standards under subpart D of this
part. For purposes of part 268, the waste will carry the waste code for
any applicable listed waste (Part 261, Subpart D). In
[[Page 153]]
addition, where the waste exhibits a characteristic, the waste will
carry one or more of the characteristic waste codes (Part 261, Subpart
C), except when the treatment standard for the listed waste operates in
lieu of the treatment standard for the characteristic waste, as
specified in paragraph (b) of this section. If the generator determines
that their waste displays a hazardous characteristic (and is not D001
nonwastewaters treated by CMBST, RORGS, OR POLYM of Sec. 268.42, Table
1), the generator must determine the underlying hazardous constituents
(as defined at Sec. 268.2(i)) in the characteristic waste.
(b) Where a prohibited waste is both listed under 40 CFR part 261,
subpart D and exhibits a characteristic under 40 CFR part 261, subpart
C, the treatment standard for the waste code listed in 40 CFR part 261,
subpart D will operate in lieu of the standard for the waste code under
40 CFR part 261, subpart C, provided that the treatment standard for the
listed waste includes a treatment standard for the constituent that
causes the waste to exhibit the characteristic. Otherwise, the waste
must meet the treatment standards for all applicable listed and
characteristic waste codes.
(c) In addition to any applicable standards determined from the
initial point of generation, no prohibited waste which exhibits a
characteristic under 40 CFR part 261, subpart C may be land disposed
unless the waste complies with the treatment standards under subpart D
of this part.
(d) Wastes that exhibit a characteristic are also subject to
Sec. 268.7 requirements, except that once the waste is no longer
hazardous, a one-time notification and certification must be placed in
the generators or treaters files and sent to the EPA region or
authorized state. The notification and certification that is placed in
the generators or treaters files must be updated if the process or
operation generating the waste changes and/or if the subtitle D facility
receiving the waste changes. However, the generator or treater need only
notify the EPA region or an authorized state on an annual basis if such
changes occur. Such notification and certification should be sent to the
EPA region or authorized state by the end of the calendar year, but no
later that December 31.
(1) The notification must include the following information:
(i) Name and address of the RCRA Subtitle D facility receiving the
waste shipment; and
(ii) A description of the waste as initially generated, including
the applicable EPA hazardous waste code(s), treatability group(s), and
underlying hazardous constituents (as defined in Sec. 268.2(i)), unless
the waste will be treated and monitored for all underlying hazardous
constituents. If all underlying hazardous constituents will be treated
and monitored, there is no requirement to list any of the underlying
hazardous constituents on the notice.
(2) The certification must be signed by an authorized representative
and must state the language found in Sec. 268.7(b)(4).
(i) If treatment removes the characteristic but does not meet
standards applicable to underlying hazardous constituents, then the
certification found in Sec. 268.7(b)(4)(iv) applies.
(ii) [Reserved]
[55 FR 22688, June 1, 1990, as amended at 56 FR 3878, Jan. 31, 1991; 57
FR 37271, Aug. 18, 1992; 58 FR 29885, May 24, 1993; 59 FR 48045, Sept.
19, 1994; 60 FR 245, Jan. 3, 1995; 61 FR 15599, 15662, Apr. 8, 1996; 62
FR 26022, May 12, 1997; 64 FR 25415, May 11, 1999]
Subpart B--Schedule for Land Disposal Prohibition and Establishment of
Treatment Standards
Source: 51 FR 19305, May 28, 1986, unless otherwise noted.
Secs. 268.10-268.12 [Reserved]
Sec. 268.13 Schedule for wastes identified or listed after November 8, 1984.
In the case of any hazardous waste identified or listed under
section 3001 after November 8, 1984, the Administrator shall make a land
disposal prohibition determination within 6 months after the date of
identification or listing.
[[Page 154]]
Sec. 268.14 Surface impoundment exemptions.
(a) This section defines additional circumstances under which an
otherwise prohibited waste may continue to be placed in a surface
impoundment.
(b) Wastes which are newly identified or listed under section 3001
after November 8, 1984, and stored in a surface impoundment that is
newly subject to subtitle C of RCRA as a result of the additional
identification or listing, may continue to be stored in the surface
impoundment for 48 months after the promulgation of the additional
listing or characteristic, not withstanding that the waste is otherwise
prohibited from land disposal, provided that the surface impoundment is
in compliance with the requirements of subpart F of part 265 of this
chapter within 12 months after promulgation of the new listing or
characteristic.
(c) Wastes which are newly identified or listed under section 3001
after November 8, 1984, and treated in a surface impoundment that is
newly subject to subtitle C of RCRA as a result of the additional
identification or listing, may continue to be treated in that surface
impoundment, not withstanding that the waste is otherwise prohibited
from land disposal, provided that surface impoundment is in compliance
with the requirements of subpart F of part 265 of this chapter within 12
months after the promulgation of the new listing or characteristic. In
addition, if the surface impoundment continues to treat hazardous waste
after 48 months from promulgation of the additional listing or
characteristic, it must then be in compliance with Sec. 268.4.
[57 FR 37271, Aug. 18, 1992]
Subpart C--Prohibitions on Land Disposal
Sec. 268.30 Waste specific prohibitions--wood preserving wastes.
(a) Effective August 11, 1997, the following wastes are prohibited
from land disposal: the wastes specified in 40 CFR part 261 as EPA
Hazardous Waste numbers F032, F034, and F035.
(b) Effective May 12, 1999, the following wastes are prohibited from
land disposal: soil and debris contaminated with F032, F034, F035; and
radioactive wastes mixed with EPA Hazardous waste numbers F032, F034,
and F035.
(c) Between May 12, 1997 and May 12, 1999, soil and debris
contaminated with F032, F034, F035; and radioactive waste mixed with
F032, F034, and F035 may be disposed in a landfill or surface
impoundment only if such unit is in compliance with the requirements
specified in Sec. 268.5(h)(2) of this part.
(d) The requirements of paragraphs (a) and (b) of this section do
not apply if:
(1) The wastes meet the applicable treatment standards specified in
Subpart D of this part;
(2) Persons have been granted an exemption from a prohibition
pursuant to a petition under Sec. 268.6, with respect to those wastes
and units covered by the petition;
(3) The wastes meet the applicable alternate treatment standards
established pursuant to a petition granted under Sec. 268.44; or
(4) Persons have been granted an extension to the effective date of
a prohibition pursuant to Sec. 268.5, with respect to those wastes
covered by the extension.
(e) To determine whether a hazardous waste identified in this
section exceeds the applicable treatment standards specified in
Sec. 268.40, the initial generator must test a sample of the waste
extract or the entire waste, depending on whether the treatment
standards are expressed as concentrations in the waste extract or the
waste, or the generator may use knowledge of the waste. If the waste
contains constituents in excess of the applicable Universal Treatment
Standard levels of Sec. 268.48 of this part, the waste is prohibited
from land disposal, and all requirements of part 268 are applicable,
except as otherwise specified.
[62 FR 26022, May 12, 1997]
Sec. 268.31 Waste specific prohibitions--Dioxin-containing wastes.
(a) Effective November 8, 1988, the dioxin-containing wastes
specified in 40 CFR 261.31 as EPA Hazardous Waste Nos. F020, F02l, F022,
F023, F026, F027, and F028, are prohibited from land disposal unless the
following condition applies:
[[Page 155]]
(1) The F020-F023 and F026-F028 dioxin-containing waste is
contaminated soil and debris resulting from a response action taken
under section 104 or 106 of the Comprehensive Environmental Response,
Compensation, and Liability Act of 1980 (CERCLA) or a corrective action
taken under subtitle C of the Resource Conservation and Recovery Act
(RCRA).
(b) Effective November 8, 1990, the F020-F023 and F026-F028 dioxin-
containing wastes listed in paragraph (a)(1) of this section are
prohibited from land disposal.
(c) Between November 8, 1988, and November 8, 1990, wastes included
in paragraph (a)(1) of this section may be disposed in a landfill or
surface impoundment only if such unit is in compliance with the
requirements specified in Sec. 268.5(h)(2) and all other applicable
requirements of parts 264 and 265 of this chapter.
(d) The requirements of paragraphs (a) and (b) of this section do
not apply if:
(1) The wastes meet the standards of subpart D of this part; or
(2) Persons have been granted an exemption from a prohibition
pursuant to a petition under Sec. 268.6, with respect to those wastes
and units covered by the petition; or
(3) Persons have been granted an extension to the effective date of
a prohibition pursuant to Sec. 268.5, with respect to those wastes
covered by the extension.
[53 FR 31216, Aug. 17, 1988]
Sec. 268.32 Waste specific prohibitions--Soils exhibiting the toxicity characteristic for metals and containing PCBs.
(a) Effective December 26, 2000, the following wastes are prohibited
from land disposal: any volumes of soil exhibiting the toxicity
characteristic solely because of the presence of metals (D004--D011) and
containing PCBs.
(b) The requirements of paragraph (a) of this section do not apply
if:
(1)(i) The wastes contain halogenated organic compounds in total
concentration less than 1,000 mg/kg; and
(ii) The wastes meet the treatment standards specified in Subpart D
of this part for EPA hazardous waste numbers D004--D011, as applicable;
or
(2)(i) The wastes contain halogenated organic compounds in total
concentration less than 1,000 mg/kg; and
(ii) The wastes meet the alternative treatment standards specified
in Sec. 268.49 for contaminated soil; or
(3) Persons have been granted an exemption from a prohibition
pursuant to a petition under Sec. 268.6, with respect to those wastes
and units covered by the petition; or
(4) The wastes meet applicable alternative treatment standards
established pursuant to a petition granted under Sec. 268.44.
[65 FR 81380, Dec. 26, 2000]
Sec. 268.33 Waste specific prohibitions--chlorinated aliphatic wastes.
(a) Effective May 8, 2001, the wastes specified in 40 CFR part 261
as EPA Hazardous Wastes Numbers K174, and K175, soil and debris
contaminated with these wastes, radioactive wastes mixed with these
wastes, and soil and debris contaminated with radioactive wastes mixed
with these wastes are prohibited from land disposal.
(b) The requirements of paragraph (a) of this section do not apply
if:
(1) The wastes meet the applicable treatment standards specified in
subpart D of this part;
(2) Persons have been granted an exemption from a prohibition
pursuant to a petition under Sec. 268.6, with respect to those wastes
and units covered by the petition;
(3) The wastes meet the applicable treatment standards established
pursuant to a petition granted under Sec. 268.44;
(4) Hazardous debris has met the treatment standards in Sec. 268.40
or the alternative treatment standards in Sec. 268.45; or
(5) Persons have been granted an extension to the effective date of
a prohibition pursuant to Sec. 268.5, with respect to these wastes
covered by the extension.
(c) To determine whether a hazardous waste identified in this
section exceeds the applicable treatment standards specified in
Sec. 268.40, the initial generator must test a sample of the waste
extract or the entire waste, depending on whether the treatment
standards
[[Page 156]]
are expressed as concentrations in the waste extract or the waste, or
the generator may use knowledge of the waste. If the waste contains
regulated constituents in excess of the applicable levels of subpart D
of this part, the waste is prohibited from land disposal, and all
requirements of part 268 are applicable, except as otherwise specified.
(d) Disposal of K175 wastes that have complied with all applicable
40 CFR 268.40 treatment standards must also be macroencapsulated in
accordance with 40 CFR 268.45 Table 1 unless the waste is placed in:
(1) A Subtitle C monofill containing only K175 wastes that meet all
applicable 40 CFR 268.40 treatment standards; or
(2) A dedicated Subtitle C landfill cell in which all other wastes
being co-disposed are at pH[le]6.0.
[65 FR 67127, Nov. 8, 2000]
Sec. 268.34 Waste specific prohibitions--toxicity characteristic metal wastes.
(a) Effective August 24, 1998, the following wastes are prohibited
from land disposal: the wastes specified in 40 CFR Part 261 as EPA
Hazardous Waste numbers D004-D011 that are newly identified (i.e.
wastes, soil, or debris identified as hazardous by the Toxic
Characteristic Leaching Procedure but not the Extraction Procedure), and
waste, soil, or debris from mineral processing operations that is
identified as hazardous by the specifications at 40 CFR Part 261.
(b) Effective November 26, 1998, the following waste is prohibited
from land disposal: Slag from secondary lead smelting which exhibits the
Toxicity Characteristic due to the presence of one or more metals.
(c) Effective May 26, 2000, the following wastes are prohibited from
land disposal: newly identified characteristic wastes from elemental
phosphorus processing; radioactive wastes mixed with EPA Hazardous
wastes D004-D011 that are newly identified (i.e., wastes, soil, or
debris identified as hazardous by the Toxic Characteristic Leaching
Procedure but not the Extraction Procedure); or mixed with newly
identified characteristic mineral processing wastes, soil, or debris.
(d) Between May 26, 1998 and May 26, 2000, newly identified
characteristic wastes from elemental phosphorus processing, radioactive
waste mixed with D004-D011 wastes that are newly identified (i.e.,
wastes, soil, or debris identified as hazardous by the Toxic
Characteristic Leaching Procedure but not the Extraction Procedure), or
mixed with newly identified characteristic mineral processing wastes,
soil, or debris may be disposed in a landfill or surface impoundment
only if such unit is in compliance with the requirements specified in
Sec. 268.5(h) of this part.
(e) The requirements of paragraphs (a) and (b) of this section do
not apply if:
(1) The wastes meet the applicable treatment standards specified in
subpart D of this part:
(2) Persons have been granted an exemption from a prohibition
pursuant to a petition under Sec. 268.6, with respect to those wastes
and units covered by the petition;
(3) The wastes meet the applicable alternate treatment standards
established pursuant to a petition granted under Sec. 268.44; or
(4) Persons have been granted an extension to the effective date of
a prohibition pursuant to Sec. 268.5, with respect to these wastes
covered by the extension.
(f) To determine whether a hazardous waste identified in this
section exceeds the applicable treatment standards specified in
Sec. 268.40, the initial generator must test a sample of the waste
extract or the entire waste, depending on whether the treatment
standards are expressed as concentration in the waste extract or the
waste, or the generator may use knowledge of the waste. If the waste
contains constituents (including underlying hazardous constituents in
characteristic wastes) in excess of the applicable Universal Treatment
Standard levels of Sec. 268.48 of this part, the waste is prohibited
from land disposal, and all requirements of part 268 are applicable,
except as otherwise specified.
[63 FR 28641, May 26, 1998, as amended at 63 FR 48127, Sept. 9, 1998]
[[Page 157]]
Sec. 268.35 Waste specific prohibitions--petroleum refining wastes.
(a) Effective February 8, 1999, the wastes specified in 40 CFR part
261 as EPA Hazardous Wastes Numbers K169, K170, K171, and K172, soils
and debris contaminated with these wastes, radioactive wastes mixed with
these hazardous wastes, and soils and debris contaminated with these
radioactive mixed wastes, are prohibited from land disposal.
(b) The requirements of paragraph (a) of this section do not apply
if:
(1) The wastes meet the applicable treatment standards specified in
Subpart D of this part;
(2) Persons have been granted an exemption from a prohibition
pursuant to a petition under Sec. 268.6, with respect to those wastes
and units covered by the petition;
(3) The wastes meet the applicable treatment standards established
pursuant to a petition granted under Sec. 268.44;
(4) Hazardous debris that have met treatment standards in
Sec. 268.40 or in the alternative treatment standards in Sec. 268.45; or
(5) Persons have been granted an extension to the effective date of
a prohibition pursuant to Sec. 268.5, with respect to these wastes
covered by the extension.
(c) To determine whether a hazardous waste identified in this
section exceeds the applicable treatment standards specified in
Sec. 268.40, the initial generator must test a sample of the waste
extract or the entire waste, depending on whether the treatment
standards are expressed as concentrations in the waste extract or the
waste, or the generator may use knowledge of the waste. If the waste
contains constituents in excess of the applicable Universal Treatment
Standard levels of Sec. 268.48, the waste is prohibited from land
disposal, and all requirements of this part are applicable, except as
otherwise specified.
[63 FR 42186, Aug. 6, 1998]
Sec. 268.36 Waste specific prohibitions--inorganic chemical wastes
(a) Effective May 20, 2002, the wastes specified in 40 CFR part 261
as EPA Hazardous Wastes Numbers K176, K177, and K178, and soil and
debris contaminated with these wastes, radioactive wastes mixed with
these wastes, and soil and debris contaminated with radioactive wastes
mixed with these wastes are prohibited from land disposal.
(b) The requirements of paragraph (a) of this section do not apply
if:
(1) The wastes meet the applicable treatment standards specified in
subpart D of this part;
(2) Persons have been granted an exemption from a prohibition
pursuant to a petition under Sec. 268.6, with respect to those wastes
and units covered by the petition;
(3) The wastes meet the applicable treatment standards established
pursuant to a petition granted under Sec. 268.44;
(4) Hazardous debris has met the treatment standards in Sec. 268.40
or the alternative treatment standards in Sec. 268.45; or
(5) Persons have been granted an extension to the effective date of
a prohibition pursuant to Sec. 268.5, with respect to these wastes
covered by the extension.
(c) To determine whether a hazardous waste identified in this
section exceeds the applicable treatment standards specified in
Sec. 268.40, the initial generator must test a sample of the waste
extract or the entire waste, depending on whether the treatment
standards are expressed as concentrations in the waste extract or the
waste, or the generator may use knowledge of the waste. If the waste
contains regulated constituents in excess of the applicable subpart D
levels, the waste is prohibited from land disposal, and all requirements
of this part are applicable, except as otherwise specified.
[66 FR 58298, Nov. 20, 2001]
Sec. 268.37 Waste specific prohibitions--ignitable and corrosive characteristic wastes whose treatment standards were vacated.
(a) Effective August 9, 1993, the wastes specified in 40 CFR 261.21
as D001 (and is not in the High TOC Ignitable Liquids Subcategory), and
specified in Sec. 261.22 as D002, that are managed in systems other than
those whose discharge is regulated under the Clean Water Act (CWA), or
that inject
[[Page 158]]
in Class I deep wells regulated under the Safe Drinking Water Act
(SDWA), or that are zero dischargers that engage in CWA-equivalent
treatment before ultimate land disposal, are prohibited from land
disposal. CWA-equivalent treatment means biological treatment for
organics, alkaline chlorination or ferrous sulfate precipitation for
cyanide, precipitation/sedimentation for metals, reduction of hexavalent
chromium, or other treatment technology that can be demonstrated to
perform equally or greater than these technologies.
(b) Effective February 10, 1994, the wastes specified in 40 CFR
261.21 as D001 (and is not in the High TOC Ignitable Liquids
Subcategory), and specified in Sec. 261.22 as D002, that are managed in
systems defined in 40 CFR 144.6(e) and 146.6(e) as Class V injection
wells, that do not engage in CWA-equivalent treatment before injection,
are prohibited from land disposal.
[58 FR 29885, May 24, 1993]
Sec. 268.38 Waste specific prohibitions--newly identified organic toxicity characteristic wastes and newly listed coke by-product and chlorotoluene production
wastes.
(a) Effective December 19, 1994, the wastes specified in 40 CFR
261.32 as EPA Hazardous Waste numbers K141, K142, K143, K144, K145,
K147, K148, K149, K150, and K151 are prohibited from land disposal. In
addition, debris contaminated with EPA Hazardous Waste numbers F037,
F038, K107-K112, K117, K118, K123-K126, K131, K132, K136, U328, U353,
U359, and soil and debris contaminated with D012-D043, K141-K145, and
K147-K151 are prohibited from land disposal. The following wastes that
are specified in 40 CFR 261.24, Table 1 as EPA Hazardous Waste numbers:
D012, D013, D014, D015, D016, D017, D018, D019, D020, D021, D022, D023,
D024, D025, D026, D027, D028, D029, D030, D031, D032, D033, D034, D035,
D036, D037, D038, D039, D040, D041, D042, D043 that are not radioactive,
or that are managed in systems other than those whose discharge is
regulated under the Clean Water Act (CWA), or that are zero dischargers
that do not engage in CWA-equivalent treatment before ultimate land
disposal, or that are injected in Class I deep wells regulated under the
Safe Drinking Water Act (SDWA), are prohibited from land disposal. CWA-
equivalent treatment means biological treatment for organics, alkaline
chlorination or ferrous sulfate precipitation for cyanide,
precipitation/ sedimentation for metals, reduction of hexavalent
chromium, or other treatment technology that can be demonstrated to
perform equally or better than these technologies.
(b) On September 19, 1996, radioactive wastes that are mixed with
D018-D043 that are managed in systems other than those whose discharge
is regulated under the Clean Water Act (CWA), or that inject in Class I
deep wells regulated under the Safe Drinking Water Act (SDWA), or that
are zero dischargers that engage in CWA-equivalent treatment before
ultimate land disposal, are prohibited from land disposal. CWA-
equivalent treatment means biological treatment for organics, alkaline
chlorination or ferrous sulfate precipitation for cyanide,
precipitation/ sedimentation for metals, reduction of hexavalent
chromium, or other treatment technology that can be demonstrated to
perform equally or greater than these technologies. Radioactive wastes
mixed with K141-K145, and K147-K151 are also prohibited from land
disposal. In addition, soil and debris contaminated with these
radioactive mixed wastes are prohibited from land disposal.
(c) Between December 19, 1994 and September 19, 1996, the wastes
included in paragraphs (b) of this section may be disposed in a landfill
or surface impoundment, only if such unit is in compliance with the
requirements specified in Sec. 268.5(h)(2) of this Part.
(d) The requirements of paragraphs (a), (b), and (c) of this section
do not apply if:
(1) The wastes meet the applicable treatment standards specified in
Subpart D of this part;
(2) Persons have been granted an exemption from a prohibition
pursuant to a petition under Sec. 268.6, with respect to those wastes
and units covered by the petition;
[[Page 159]]
(3) The wastes meet the applicable alternate treatment standards
established pursuant to a petition granted under Sec. 268.44;
(4) Persons have been granted an extension to the effective date of
a prohibition pursuant to Sec. 268.5, with respect to these wastes
covered by the extension.
(e) To determine whether a hazardous waste identified in this
section exceeds the applicable treatment standards specified in
Sec. 268.40, the initial generator must test a sample of the waste
extract or the entire waste, depending on whether the treatment
standards are expressed as concentrations in the waste extract or the
waste, or the generator may use knowledge of the waste. If the waste
contains constituents in excess of the applicable Subpart D levels, the
waste is prohibited from land disposal, and all requirements of part 268
are applicable, except as otherwise specified.
[59 FR 48045, Sept. 19, 1995]
Sec. 268.39 Waste specific prohibitions--spent aluminum potliners; reactive; and carbamate wastes.
(a) On July 8, 1996, the wastes specified in 40 CFR 261.32 as EPA
Hazardous Waste numbers K156-K159, and K161; and in 40 CFR 261.33 as EPA
Hazardous Waste numbers P127, P128, P185, P188-P192, P194, P196-P199,
P201-P205, U271, U278-U280, U364, U367, U372, U373, U387, U389, U394,
U395, U404, and U409-U411 are prohibited from land disposal. In
addition, soil and debris contaminated with these wastes are prohibited
from land disposal.
(b) On July 8, 1996, the wastes identified in 40 CFR 261.23 as D003
that are managed in systems other than those whose discharge is
regulated under the Clean Water Act (CWA), or that inject in Class I
deep wells regulated under the Safe Drinking Water Act (SDWA), or that
are zero dischargers that engage in CWA-equivalent treatment before
ultimate land disposal, are prohibited from land disposal. This
prohibition does not apply to unexploded ordnance and other explosive
devices which have been the subject of an emergency response. (Such D003
wastes are prohibited unless they meet the treatment standard of DEACT
before land disposal (see Sec. 268.40)).
(c) On September 21, 1998, the wastes specified in 40 CFR 261.32 as
EPA Hazardous Waste number K088 are prohibited from land disposal. In
addition, soil and debris contaminated with these wastes are prohibited
from land disposal.
(d) On April 8, 1998, radioactive wastes mixed with K088, K156-K159,
K161, P127, P128, P185, P188-P192, P194, P196-P199, P201-P205, U271,
U278-U280, U364, U367, U372, U373, U387, U389, U394, U395, U404, and
U409-U411 are prohibited from land disposal. In addition, soil and
debris contaminated with these radioactive mixed wastes are prohibited
from land disposal.
(e) Between July 8, 1996, and April 8, 1998, the wastes included in
paragraphs (a), (c), and (d) of this section may be disposed in a
landfill or surface impoundment, only if such unit is in compliance with
the requirements specified in Sec. 268.5(h)(2).
(f) The requirements of paragraphs (a), (b), (c), and (d) of this
section do not apply if:
(1) The wastes meet the applicable treatment standards specified in
Subpart D of this part;
(2) Persons have been granted an exemption from a prohibition
pursuant to a petition under Sec. 268.6, with respect to those wastes
and units covered by the petition;
(3) The wastes meet the applicable alternate treatment standards
established pursuant to a petition granted under Sec. 268.44;
(4) Persons have been granted an extension to the effective date of
a prohibition pursuant to Sec. 268.5, with respect to these wastes
covered by the extension.
(g) To determine whether a hazardous waste identified in this
section exceeds the applicable treatment standards specified in
Sec. 268.40, the initial generator must test a sample of the waste
extract or the entire waste, depending on whether the treatment
standards are expressed as concentrations in the waste extract or the
waste, or the generator may use knowledge of the waste. If the waste
contains constituents in excess of the applicable
[[Page 160]]
Subpart D levels, the waste is prohibited from land disposal, and all
requirements of this part 268 are applicable, except as otherwise
specified.
[61 FR 15663, Apr. 8, 1996, as amended at 61 FR 33683, June 28, 1996; 62
FR 1997, Jan. 14, 1997; 62 FR 32979, June 17, 1997; 62 FR 37699, July
14, 1997; 63 FR 51264, Sept. 24, 1998]
Subpart D--Treatment Standards
Sec. 268.40 Applicability of treatment standards.
(a) A prohibited waste identified in the table ``Treatment Standards
for Hazardous Wastes'' may be land disposed only if it meets the
requirements found in the table. For each waste, the table identifies
one of three types of treatment standard requirements:
(1) All hazardous constituents in the waste or in the treatment
residue must be at or below the values found in the table for that waste
(``total waste standards''); or
(2) The hazardous constituents in the extract of the waste or in the
extract of the treatment residue must be at or below the values found in
the table (``waste extract standards''); or
(3) The waste must be treated using the technology specified in the
table (``technology standard''), which are described in detail in
Sec. 268.42, Table 1--Technology Codes and Description of Technology-
Based Standards.
(b) For wastewaters, compliance with concentration level standards
is based on maximums for any one day, except for D004 through D011
wastes for which the previously promulgated treatment standards based on
grab samples remain in effect. For all nonwastewaters, compliance with
concentration level standards is based on grab sampling. For wastes
covered by the waste extract standards, the test Method 1311, the
Toxicity Characteristic Leaching Procedure found in ``Test Methods for
Evaluating Solid Waste, Physical/Chemical Methods'', EPA Publication SW-
846, as incorporated by reference in Sec. 260.11, must be used to
measure compliance. An exception is made for D004 and D008, for which
either of two test methods may be used: Method 1311, or Method 1310, the
Extraction Procedure Toxicity Test. For wastes covered by a technology
standard, the wastes may be land disposed after being treated using that
specified technology or an equivalent treatment technology approved by
the Administrator under the procedures set forth in Sec. 268.42(b).
(c) When wastes with differing treatment standards for a constituent
of concern are combined for purposes of treatment, the treatment residue
must meet the lowest treatment standard for the constituent of concern.
(d) Notwithstanding the prohibitions specified in paragraph (a) of
this section, treatment and disposal facilities may demonstrate (and
certify pursuant to 40 CFR 268.7(b)(5)) compliance with the treatment
standards for organic constituents specified by a footnote in the table
``Treatment Standards for Hazardous Wastes'' in this section, provided
the following conditions are satisfied:
(1) The treatment standards for the organic constituents were
established based on incineration in units operated in accordance with
the technical requirements of 40 CFR part 264, subpart O, or based on
combustion in fuel substitution units operating in accordance with
applicable technical requirements;
(2) The treatment or disposal facility has used the methods
referenced in paragraph (d)(1) of this section to treat the organic
constituents; and
(3) The treatment or disposal facility may demonstrate compliance
with organic constituents if good-faith analytical efforts achieve
detection limits for the regulated organic constituents that do not
exceed the treatment standards specified in this section by an order of
magnitude.
(e) For characteristic wastes (D001-D043) that are subject to
treatment standards in the following table ``Treatment Standards for
Hazardous Wastes,'' and are not managed in a wastewater treatment system
that is regulated under the Clean Water Act (CWA), that is CWA-
equivalent, or that is injected into a Class I nonhazardous deep
injection well, all underlying hazardous constituents (as defined in
Sec. 268.2(i)) must meet Universal Treatment Standards, found in
Sec. 268.48, Table Universal Treatment Standards, prior to land disposal
as defined in Sec. 268.2(c) of this part.
[[Page 161]]
(f) The treatment standards for F001-F005 nonwastewater constituents
carbon disulfide, cyclohexanone, and/or methanol apply to wastes which
contain only one, two, or three of these constituents. Compliance is
measured for these constituents in the waste extract from test Method
1311, the Toxicity Characteristic Leaching Procedure found in ``Test
Methods for Evaluating Solid Waste, Physical/Chemical Methods'', EPA
Publication SW-846, as incorporated by reference in Sec. 260.11. If the
waste contains any of these three constituents along with any of the
other 25 constituents found in F001-F005, then compliance with treatment
standards for carbon disulfide, cyclohexanone, and/or methanol are not
required.
(g) Between August 26, 1996 and March 4, 1999 the treatment
standards for the wastes specified in 40 CFR 261.32 as EPA Hazardous
Waste numbers K156-K161; and in 40 CFR 261.33 as EPA Hazardous Waste
numbers P127, P128, P185, P188-P192, P194, P196-P199, P201-P205, U271,
U277-U280, U364-U367, U372, U373, U375-U379, U381-U387, U389-U396, U400-
U404, U407, and U409-U411; and soil contaminated with these wastes; may
be satisfied by either meeting the constituent concentrations presented
in the table ``Treatment Standards for Hazardous Wastes'' in this
section, or by treating the waste by the following technologies:
combustion, as defined by the technology code CMBST at Sec. 268.42 Table
1, for nonwastewaters; and, biodegradation as definded by the technology
code BIODG, carbon adsorption as defined by the technology code CARBN,
chemical oxidation as defined by the technology code CHOXD, or
combustion as defined as technology code CMBST at Sec. 268.42 Table 1,
for wastewaters.
(h) Prohibited D004-D011 mixed radioactive wastes and mixed
radioactive listed wastes containing metal constituents, that were
previously treated by stabilization to the treatment standards in effect
at that time and then put into storage, do not have to be re-treated to
meet treatment standards in this section prior to land disposal.
(i) Zinc micronutrient fertilizers that are produced for the general
public's use and that are produced from or contain recycled
characteristic hazardous wastes (D004-D011) are subject to the
applicable treatment standards in Sec. 268.41 contained in the 40 CFR,
parts 260 to 299, edition revised as of July 1, 1990.
(j) Effective September 4, 1998, the treatment standards for the
wastes specified in 40 CFR 261.33 as EPA Hazardous Waste numbers P185,
P191, P192, P197, U364, U394, and U395 may be satisfied by either
meeting the constituent concentrations presented in the table
``Treatment Standards for Hazardous Wastes'' in this section, or by
treating the waste by the following technologies: combustion, as defined
by the technology code CMBST at Sec. 268.42 Table 1 of this Part, for
nonwastewaters; and, biodegradation as defined by the technology code
BIODG, carbon adsorption as defined by the technology code CARBN,
chemical oxidation as defined by the technology code CHOXD, or
combustion as defined as technology code CMBST at Sec. 268.42 Table 1 of
this Part, for wastewaters.
[[Page 162]]
Treatment Standards For Hazardous Wastes
[Note: NA means not applicable]
------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------
Regulated hazardous constituent Wastewaters Nonwastewaters
-------------------------------------------------------------------------------------------------
Concentration in
Concentration in mg/kg \5\ unless
Waste code Waste description and treatment/Regulatory subcategory \1\ CAS \2\ mg/L \3\; or noted as ``mg/L
Common name number Technology Code TCLP''; or
\4\ Technology Code
\4\
------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------
D001 \9\ Ignitable Characteristic Wastes, except for the Sec. 261.21(a)(1) High TOC NA NA DEACT and meet DEACT and meet
Subcategory. Sec. 268.48 Sec. 268.48
standards \8\; or standards \8\; or
RORGS; or CMBST RORGS; or CMBST
------------------------------------------------------------------------------
High TOC Ignitable Characteristic Liquids Subcategory based on 40 CFR NA NA NA RORGS; CMBST; or
261.21(a)(1)--Greater than or equal to 10% total organic carbon. (Note: POLYM
This subcategory consists of nonwastewaters only.)
------------------
D002 \9\ Corrosive Characteristic Wastes. NA NA DEACT and meet DEACT and meet
Sec. 268.48 Sec. 268.48
standards \8\ standards \8\
------------------
D002, D004, D005, Radioactive high level wastes generated during the reprocessing of fuel Corrosivity (pH) NA NA HLVIT
D006, D007, rods. (Note: This subcategory consists of nonwastewaters only.) Arsenic 7440-38-2 NA HLVIT
D008, D009, Barium 7440-39-3 NA HLVIT
D010, D011 Cadmium 7440-43-9 NA HLVIT
Chromium (Total) 7440-47-3 NA HLVIT
Lead 7439-92-1 NA HLVIT
Mercury 7439-97-6 NA HLVIT
Selenium 7782-49-2 NA HLVIT
Silver 7440-22-4 NA HLVIT
------------------
D003 \9\ Reactive Sulfides Subcategory based on 261.23(a)(5). NA NA DEACT DEACT
------------------------------------------------------------------------------
Explosives Subcategory based on 261.23(a)(6),(7), and (8). NA NA DEACT and meet DEACT and meet
Sec. 268.48 Sec. 268.48
standards \8\ standards \8\
------------------------------------------------------------------------------
Unexploded ordnance and other explosive devices which have been the subject NA NA DEACT DEACT
of an emergency response.
------------------------------------------------------------------------------
Other Reactives Subcategory based on 261.23(a)(1). NA NA DEACT and meet DEACT and meet
Sec. 268.48 Sec. 268.48
standards \8\ standards \8\
------------------------------------------------------------------------------
[[Page 163]]
Water Reactive Subcategory based on 261.23(a)(2), (3), and (4). (Note: This NA NA NA DEACT and meet
subcategory consists of nonwastewaters only). Sec. 268.48
standards \8\
------------------------------------------------------------------------------
Reactive Cyanides Subcategory based on 261.23(a)(5). Cyanides (Total) \7\ 57-12-5 Reserved 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
------------------
D004 \9\ Wastes that exhibit, or are expected to exhibit, the characteristic of Arsenic 7440-38-2 1.4 and meet Sec. 5.0 mg/L TCLP and
toxicity for arsenic based on the toxicity characteristic leaching 268.48 standards meet Sec. 268.48
procedure (TCLP) in SW846. \8\ standards \8\
------------------
D005 \9\ Wastes that exhibit, or are expected to exhibit, the characteristic of Barium 7440-39-3 1.2 and meet Sec. 21 mg/L TCLP and
toxicity for barium based on the toxicity characteristic leaching 268.48 standards meet Sec. 268.48
procedure (TCLP) in SW846. \8\ standards \8\
------------------
D006 \9\ Wastes that exhibit, or are expected to exhibit, the characteristic of Cadmium 7440-43-9 0.69 and meet Sec. 0.11 mg/L TCLP and
toxicity for cadmium based on the toxicity characteristic leaching 268.48 standards meet Sec. 268.48
procedure (TCLP) in SW846. \8\ standards \8\
------------------------------------------------------------------------------
Cadmium Containing Batteries Subcategory. (Note: This subcategory consists Cadmium 7440-43-9 NA RTHRM
of nonwastewaters only).
------------------
D007 \9\ Wastes that exhibit, or are expected to exhibit, the characteristic of Chromium (Total) 7440-47-3 2.77 and meet Sec. 0.60 mg/L TCLP and
toxicity for chromium based on the toxicity characteristic leaching 268.48 standards meet Sec. 268.48
procedure (TCLP) in SW846. \8\ standards \8\
------------------
D008 \9\ Wastes that exhibit, or are expected to exhibit, the characteristic of Lead 7439-92-1 0.69 and meet Sec. 0.75 mg/L TCLP and
toxicity for lead based on the toxicity characteristic leaching procedure 268.48 standards meet Sec. 268.48
(TCLP) in SW846. \8\ standards \8\
------------------------------------------------------------------------------
Lead Acid Batteries Subcategory (Note: This standard only applies to lead Lead 7439-92-1 NA RLEAD
acid batteries that are identified as RCRA hazardous wastes and that are
not excluded elsewhere from regulation under the land disposal
restrictions of 40 CFR 268 or exempted under other EPA regulations (see 40
CFR 266.80). This subcategory consists of nonwastewaters only.)
------------------------------------------------------------------------------
Radioactive Lead Solids Subcategory (Note: These lead solids include, but Lead 7439-92-1 NA MACRO
are not limited to, all forms of lead shielding and other elemental forms
of lead. These lead solids do not include treatment residuals such as
hydroxide sludges, other wastewater treatment residuals, or incinerator
ashes that can undergo conventional pozzolanic stabilization, nor do they
include organo-lead materials that can be incinerated and stabilized as
ash. This subcategory consists of nonwastewaters only.)
------------------
D009 \9\ Nonwastewaters that exhibit, or are expected to exhibit, the characteristic Mercury 7439-97-6 NA IMERC; OR RMERC
of toxicity for mercury based on the toxicity characteristic leaching
procedure (TCLP) in SW846; and contain greater than or equal to 260 mg/kg
total mercury that also contain organics and are not incinerator residues.
(High Mercury-Organic Subcategory)
------------------------------------------------------------------------------
[[Page 164]]
Nonwastewaters that exhibit, or are expected to exhibit, the characteristic Mercury 7439-97-6 NA RMERC
of toxicity for mercury based on the toxicity characteristic leaching
procedure (TCLP) in SW846; and contain greater than or equal to 260 mg/kg
total mercury that are inorganic, including incinerator residues and
residues from RMERC. (High Mercury-Inorganic Subcategory)
------------------------------------------------------------------------------
Nonwastewaters that exhibit, or are expected to exhibit, the characteristic Mercury 7439-97-6 NA 0.20 mg/L TCLP and
of toxicity for mercury based on the toxicity characteristic leaching meet Sec. 268.48
procedure (TCLP) in SW846; and contain less than 260 mg/kg total mercury standards \8\
and that are residues from RMERC only. (Low Mercury Subcategory)
------------------------------------------------------------------------------
All other nonwastewaters that exhibit, or are expected to exhibit, the Mercury 7439-97-6 NA 0.025 mg/L TCLP
characteristic of toxicity for mercury based on the toxicity and meet Sec.
characteristic leaching procedure (TCLP) in SW846; and contain less than 268.48 standards
260 gm/kg total mercury and that are not residues from RMERC. (Low Mercury \8\
Subcategory)
------------------------------------------------------------------------------
All D009 wastewaters. Mercury 7439-97-6 0.15 mg/L TCLP and NA
meet Sec. 268.48
standards \8\
------------------------------------------------------------------------------
Elemental mercury contaminated with radioactive materials. (Note: This Mercury 7439-97-6 NA AMLGM
subcategory consists of nonwastewaters only.)
------------------------------------------------------------------------------
Hydraulic oil contaminated with Mercury Radioactive Materials Subcategory. Mercury 7439-97-6 NA IMERC
(Note: This subcategory consists of nonwastewaters only.)
------------------
D010 \9\ Wastes that exhibit, or are expected to exhibit, the characteristic of Selenium 7782-49-2 0.82 and meet Sec. 5.7 mg/L TCLP and
toxicity for selenium based on the toxicity characteristic leaching 268.48 standards meet Sec. 268.48
procedure (TCLP) in SW846. \8\ standards \8\
------------------
D011 \9\ Wastes that exhibit, or are expected to exhibit, the characteristic of Silver 7440-22-4 0.43 and meet Sec. 0.14 mg/L TCLP and
toxicity for silver based on the toxicity characteristic leaching 268.48 standards meet Sec. 268.48
procedure (TCLP) in SW846. \8\ standards \8\
------------------
D012 \9\ Wastes that are TC for Endrin based on the TCLP in SW846 Method 1311. Endrin 72-20-8 BIODG; or CMB0.13 and meet Sec.
268.48 standards
\8\
[[Page 165]]
........................................................................... Endrin aldehyde 7421-93-4 BIODG; or CMB0.13 and meet Sec.
268.48 standards
\8\
------------------
D013 \9\ Wastes that are TC for Lindane based on the TCLP in SW846 Method 1311. alpha-BHC 319-84-6 CARBN;0.066 and meet
Sec. 268.48
standards \8\
........................................................................... beta-BHC 319-85-7 CARBN;0.066 and meet
Sec. 268.48
standards \8\
........................................................................... delta-BHC 319-86-8 CARBN;0.066 and meet
Sec. 268.48
standards \8\
........................................................................... gamma-BHC (Lindane) 58-89-9 CARBN;0.066 and meet
Sec. 268.48
standards \8\
------------------
D014 \9\ Wastes that are TC for Methoxychlor based on the TCLP in SW846 Method 1311. Methoxychlor 72-43-5 WETOX or CMB0.18 and meet Sec.
268.48 standards
\8\
------------------
D015 \9\ Wastes that are TC for Toxaphene based on the TCLP in SW846 Method 1311. Toxaphene 8001-35-2 BIODG or CMB2.6 and meet Sec.
268.48 standards
\8\
------------------
D16 \9\ Wastes that are TC for 2,4-D (2,4-Dichlorophenoxyacetic acid) based on the 2,4,-D (2,4-Dichlorophenoxyacetic acid) 94-75-7 CHOX10 and meet Sec.
TCLP in SW846 Method 1311. CMBS268.48 standards
\8\
------------------
D17 \9\ Wastes that are TC for 2,4,5-TP (Silvex) based on the TCLP in SW846 Method 2,4,5-TP (Silvex) 93-72-1 CHO7.9 and meet Sec.
1311. 268.48 standards
\8\
------------------
D018 \9\ Wastes that are TC for Benzene based on the TCLP in SW846 Method 1311. Benzene 71-43-2 0.14 and meet Sec. 10 and meet Sec.
268.48 standards 268.48 standards
\8\ \8\
------------------
D019 \9\ Wastes that are TC for Carbon tetrachloride based on the TCLP in SW846 Carbon tetrachloride 56-23-5 0.057 and meet 6.0 and meet Sec.
Method 1311. Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D020 \9\ Wastes that are TC for Chlordane based on the TCLP in SW846 Method 1311. Chlordane (alpha and gamma isomers) 57-74-9 0.0033 and meet 0.26 and meet Sec.
Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D021 \9\ Wastes that are TC for Chlorobenzene based on the TCLP in SW846 Method Chlorobenzene 108-90-7 0.057 and meet 6.0 and meet Sec.
1311. Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
[[Page 166]]
D022 \9\ Wastes that are TC for Chloroform based on the TCLP in SW846 Method 1311. Chloroform 67-66-3 0.046 and meet 6.0 and meet Sec.
Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D023 \9\ Wastes that are TC for o-Cresol based on the TCLP in SW846 Method 1311. o-Cresol 95-48-7 0.11 and meet Sec. 5.6 and meet Sec.
268.48 standards 268.48 standards
\8\ \8\
------------------
D024 \9\ Wastes that are TC for m-Cresol based on the TCLP in SW846 Method 1311. m-Cresol (difficult to distinguish from p- 108-39-4 0.77 and meet Sec. 5.6 and meet Sec.
cresol) 268.48 standards 268.48 standards
\8\ \8\
------------------
D025 \9\ Wastes that are TC for p-Cresol based on the TCLP in SW846 Method 1311. p-Cresol (difficult to distinguish from m- 106-44-5 0.77 and meet Sec. 5.6 and meet Sec.
cresol) 268.48 standards 268.48 standards
\8\ \8\
------------------
D026 \9\ Wastes that are TC for Cresols (Total) based on the TCLP in SW846 Method Cresol-mixed isomers (Cresylic acid) (sum 1319-77-3 0.88 and meet Sec. 11.2 and meet Sec.
1311. of o-, m-, and p-cresol concentrations) 268.48 standards 268.48 standards
\8\ \8\
------------------
D027 \9\ Wastes that are TC for p-Dichlorobenzene based on the TCLP in SW846 Method p-Dichlorobenzene (1,4-Dichlorobenzene) 106-46-7 0.090 and meet 6.0 and meet Sec.
1311. Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D028 \9\ Wastes that are TC for 1,2-Dichloroethane based on the TCLP in SW846 Method 1,2-Dichloroethane 107-06-2 0.21 and meet Sec. 6.0 and meet Sec.
1311. 268.48 standards 268.48 standards
\8\ \8\
------------------
D029 \9\ Wastes that are TC for 1,1-Dichloroethylene based on the TCLP in SW846 1,1-Dichloroethylene 75-35-4 0.025 and meet 6.0 and meet Sec.
Method 1311. Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D030 \9\ Wastes that are TC for 2,4-Dinitrotoluene based on the TCLP in SW846 Method 2,4-Dinitrotoluene 121-14-2 0.32 and meet Sec. 140 and meet Sec.
1311. 268.48 standards 268.48 standards
\8\ \8\
------------------
D031 \9\ Wastes that are TC for Heptachlor based on the TCLP in SW846 Method 1311. Heptachlor 76-44-8 0.0012 and meet 0.066 and meet
Sec. 268.48 Sec. 268.48
standards \8\ standards \8\
[[Page 167]]
........................................................................... Heptachlor epoxide 1024-57-3 0.016 and meet 0.066 and meet
Sec. 268.48 Sec. 268.48
standards \8\ standards \8\
------------------
D032 \9\ Wastes that are TC for Hexachlorobenzene based on the TCLP in SW846 Method Hexachlorobenzene 118-74-1 0.055 and meet 10 and meet Sec.
1311. Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D033 \9\ Wastes that are TC for Hexachlorobutadiene based on the TCLP in SW846 Hexachlorobutadiene 87-68-3 0.055 and meet 5.6 and meet Sec.
Method 1311. Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D034 \9\ Wastes that are TC for Hexachloroethane based on the TCLP in SW846 Method Hexachloroethane 67-72-1 0.055 and meet 30 and meet Sec.
1311. Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D035 \9\ Wastes that are TC for Methyl ethyl ketone based on the TCLP in SW846 Methyl ethyl ketone 78-93-3 0.28 and meet Sec. 36 and meet Sec.
Method 1311. 268.48 standards 268.48 standards
\8\ \8\
------------------
D036 \9\ Wastes that are TC for Nitrobenzene based on the TCLP in SW846 Method 1311. Nitrobenzene 98-95-3 0.068 and meet 14 and meet Sec.
Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D037 \9\ Wastes that are TC for Pentachlorophenol based on the TCLP in SW846 Method Pentachlorophenol 87-86-5 0.089 and meet 7.4 and meet Sec.
1311. Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D038 \9\ Wastes that are TC for Pyridine based on the TCLP in SW846 Method 1311. Pyridine 110-86-1 0.014 and meet 16 and meet Sec.
Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D039 \9\ Wastes that are TC for Tetrachloroethylene based on the TCLP in SW846 Tetrachloroethylene 127-18-4 0.056 and meet 6.0 and meet Sec.
Method 1311. Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D040 \9\ Wastes that are TC for Trichloroethylene based on the TCLP in SW846 Method Trichloroethylene 79-01-6 0.054 and meet 6.0 and meet Sec.
1311. Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
D041 \9\ Wastes that are TC for 2,4,5-Trichlorophenol based on the TCLP in SW846 2,4,5-Trichlorophenol 95-95-4 0.18 and meet Sec. 7.4 and meet Sec.
Method 1311. 268.48 standards 268.48 standards
\8\ \8\
------------------
D042 \9\ Wastes that are TC for 2,4,6-Trichlorophenol based on the TCLP in SW846 2,4,6-Trichlorophenol 88-06-2 0.035 and meet 7.4 and meet Sec.
Method 1311. Sec. 268.48 268.48 standards
standards \8\ \8\
------------------
[[Page 168]]
D043 \9\ Wastes that are TC for Vinyl chloride based on the TCLP in SW846 Method Vinyl chloride 75-01-4 0.27 and meet Sec. 6.0 and meet Sec.
1311. 268.48 standards 268.48 standards
\8\ \8\
------------------
F001, F002, F003, F001, F002, F003, F004 and/or F005 solvent wastes that contain any Acetone 67-64-1 0.28 160
F004, & F005 combination of one or more of the following spent solvents: acetone, Benzene 71-43-2 0.14 10
benzene, n-butyl alcohol, carbon disulfide, carbon tetrachloride, n-Buthyl alcohol 71-36-3 5.6 2.6
chlorinated fluorocarbons, chlorobenzene, o-cresol, m-cresol, p-cresol, Carbon disulfide 75-15-0 3.8 NA
cyclohexanone, o-dichlorobenzene, 2-ethoxyethanol, ethyl acetate, ethyl Carbon tetrachloride 56-23-5 0.057 6.0
benzene, ethyl ether, isobutyl alcohol, methanol, methylene chloride, Chlorobenzene 108-90-7 0.057 6.0
methyl ethyl ketone, methyl isobutyl ketone, nitrobenzene, 2-nitropropane, o-Cresol 95-48-7 0.11 5.6
pyridine, tetrachloroethylene, toluene, 1,1,1-trichloroethane, 1,1,2- m-Cresol (difficult to distinguish from p- 108-39-4 0.77 5.6
trichloroethane, 1,1,2-trichloro-1,2,2-trifluoroethane, trichloroethylene, cresol) ............ .................. ..................
trichlorofluoromethane, and/or xylenes [except as specifically noted in p-Cresol (difficult to distinguish from m- 106-44-5 0.77 5.6
other subcategories]. See further details of these listings in Sec. cresol) ............ .................. ..................
261.31. Cresol-mixed isomers (Cresylic acid) (sum 1319-77-3 0.88 11.2
of o-, m-, and p-cresol concentrations) ............ ..................
............ ..................
........................................................................... Cyclohexanone 108-94-1 0.36 NA
........................................................................... o-Dichlorobenzene 95-50-1 0.088 6.0
........................................................................... Ethyl acetate 141-78-6 0.34 33
........................................................................... Ethyl benzene 100-41-4 0.057 10
........................................................................... Ethyl ether 60-29-7 0.12 160
........................................................................... Isobutyl alcohol 78-83-1 5.6 170
........................................................................... Methanol 67-56-1 5.6 NA
........................................................................... Methylene chloride 75-9-2 0.089 30
........................................................................... Methyl ethyl ketone 78-93-3 0.28 36
........................................................................... Methyl isobutyl ketone 108-10-1 0.14 33
........................................................................... Nitrobenzene 98-95-3 0.068 14
........................................................................... Pyridine 110-86-1 0.014 16
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
........................................................................... Toluene 108-88-3 0.080 10
........................................................................... 1,1,1-Trichloroethane 71-55-6 0.054 6.0
........................................................................... 1,1,2-Trichloroethane 79-00-5 0.054 6.0
........................................................................... 1,1,2-Trichloro-1,2,2-trifluoroethane 76-13-1 0.057 30
........................................................................... Trichloroethylene 79-01-6 0.054 6.0
........................................................................... Trichlorofluoromethane 75-69-4 0.020 30
[[Page 169]]
........................................................................... Xylenes-mixed isomers (sum of o-, m-, and 1330-20-7 0.32 30
p-xylene concentrations)
------------------------------------------------------------------------------
F003 and/or F005 solvent wastes that contain any combination of one or more Carbon disulfide 75-15-0 3.8 4.8 mg/L TCLP
of the following three solvents as the only listed F001-5 solvents: carbon Cyclohexanone 108-94-1 0.36 0.75 mg/L TCLP
disulfide, cyclohexanone, and/or methanol. (formerly 268.41(c)) Methanol 67-56-1 5.6 0.75 mg/L TCLP
------------------------------------------------------------------------------
F005 solvent waste containing 2-Nitropropane as the only listed F001-5 2-Nitropropane 79-46-9 (WETOX or CHOXD) CMBST
solvent. fb CARBN; or CMBST
------------------------------------------------------------------------------
F005 solvent waste containing 2-Ethoxyethanol as the only listed F001-5 2-Ethoxyethanol 110-80-5 BIODG; or CMBST CMBST
solvent.
------------------
F006 Wastewater treatment sludges from electroplating operations except from the Cadmium 7440-43-9 0.69 0.11 mg/L TCLP
following processes: (1) Sulfuric acid anodizing of aluminum; (2) tin Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
plating on carbon steel; (3) zinc plating (segregated basis) on carbon Cyanides (Total) \7\ 57-12-5 1.2 590
steel; (4) aluminum or zinc-aluminum plating on carbon steel; (5) cleaning/ Cyanides (Amenable) \7\ 57-12-5 0.86 30
stripping associated with tin, zinc and aluminum plating on carbon steel; Lead 7439-92-1 0.69 0.75 mg/L TCLP
and (6) chemical etching and milling of aluminum. Nickel 7440-02-0 3.98 11 mg/L TCLP
Silver 7440-22-4 NA 0.14 mg/L TCLP
------------------
F007 Spent cyanide plating bath solutions from electroplating operations. Cadmium 7440-43-9 NA 0.11 mg/L TCLP
Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
........................................................................... Silver 7440-22-4 NA 0.14 mg/L TCLP
------------------
F008 Plating bath residues from the bottom of plating baths from electroplating Cadmium 7440-43-9 NA 0.11 mg/L TCLP
operations where cyanides are used in the process. Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
........................................................................... Silver 7440-22-4 NA 0.14 mg/L TCLP
------------------
F009 Spent stripping and cleaning bath solutions from electroplating operations Cadmium 7440-43-9 NA 0.11 mg/L TCLP
where cyanides are used in the process. Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
........................................................................... Silver 7440-22-4 NA 0.14 mg/L TCLP
------------------
F010 Quenching bath residues from oil baths from metal heat treating operations Cyanides (Total) \7\ 57-12-5 1.2 590
where cyanides are used in the process. Cyanides (Amenable) \7\ 57-12-5 0.86 NA
------------------
[[Page 170]]
F011 Spent cyanide solutions from salt bath pot cleaning from metal heat Cadmium 7440-43-9 NA 0.11 mg/L TCLP
treating operations. Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
........................................................................... Silver 7440-22-4 NA 0.14 mg/L TCLP
------------------
F012 Quenching wastewater treatment sludges from metal heat treating operations Cadmium 7440-43-9 NA 0.11 mg/L TCLP
where cyanides are used in the process. Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
........................................................................... Silver 7440-22-4 NA 0.14 mg/L TCLP
------------------
F019 Wastewater treatment sludges from the chemical conversion coating of Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
aluminum except from zirconium phosphating in aluminum can washing when Cyanides (Total) \7\ 57-12-5 1.2 590
such phosphating is an exclusive conversion coating process. Cyanides (Amendable) \7\ 57-12-5 0.86 30
------------------
F020, F021, F022, Wastes (except wastewater and spent carbon from hydrogen chloride HxCDDs (All Hexachlorodibenzo-p-dioxins) NA 0.000063 0.001
F023, F026 purification) from the production or manufacturing use (as a reactant, Hx CDFs (All Hexachlorodibenzofurans) ............ .................. ..................
chemical intermediate, or component in a formulating process) of: (1) tri- PeCDDs (All Pentachlorodibenzo-p-dioxins) NA 0.000063 0.001
or tetrachlorophenol, or of intermediates used to produce their pesticide PeCDFs (All Pentachlorodibenzofurans) ............ .................. ..................
derivatives, excluding wastes from the production of Hexachlorophene from Pentachlorophenol NA 0.000063 0.001
highly purified, 2,4,5-trichlorophenol (F020); (2) pentachlorophenol, or TCDDs (All Tetrachlorodibenzo-p-dioxins) ............ .................. ..................
of intermediates used to produce its derivatives (i.e., F021); (3) tetra-, TCDFs (All Tetrachlorodibenzofurans) NA 0.000035 0.001
penta-, or hexachlorobenzenes under alkaline conditions (i.e., F022); and 2,4,5-Trichlorophenol ............ .................. ..................
from the production of materials on equipment previously used for the 2,4-6-Trichlorophenol 87-86-5 0.089 7.4
production or manufacturing use (as a reactant, chemical intermediate, or 2,3,4,6-Tetrachlorophenol NA 0.000063 0.001
component in a formulating process) of: (1) tri- or tetrachlorophenols, ............ .................. ..................
excluding wastes from equipment used only for the production of NA 0.000063 0.001
Hexachlorophene from highly purified 2,4,5-trichlorophenol (F023); (2) ............ .................. ..................
tetra- penta, or hexachlorobenzenes under alkaline conditions (i.e., 95-95-4 0.18 7.4
F026). 88-06-2 0.035 7.4
58-90-2 0.030 7.4
------------------
[[Page 171]]
F024 Process wastes, including but not limited to, distillation residues, heavy All F024 wastes NA CMBST \11\ CMBST \11\
ends, tars, and reactor clean-out wastes, from the production of certain 2-Chloro-1,3-butadiene 126-99-8 0.057 0.28
chlorinated aliphatic hydrocarbons by free radical catalyzed processes. 3-Chloropropylene 107-05-1 0.036 30
These chlorinated aliphatic hydrocarbons are those having carbon chain 1,1-Dichloroethane 75-34-3 0.059 6.0
lengths ranging from one to and including five, with varying amounts and 1,2-Dichloroethane 107-06-2 0.21 6.0
positions of chlorine substitution. (This listing does not include 1,2-Dichloropropane 78-87-5 0.85 18
wastewaters, wastewater treatment sludges, spent catalysts, and wastes cis-1,3-Dichloropropylene 10061-01-5 0.036 18
listed in Sec. 261.31 or Sec. 261.32). trans-1-3-Dichloropropylene 10061-02-6 0.036 18
bis(2-Ethylhexyl)phthalate 117-81-7 0.28 28
Hexachloroethane 67-72-1 0.055 30
Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
Nickel 7440-02-0 3.98 11 mg/L TCLP
------------------
F025 Condensed light ends from the production of certain chlorinated aliphatic Carbon tetrachloride 56-23-5 0.057 6.0
hydrocarbons, by free radical catalyzed processes. These chlorinated Chloroform 67-66-3 0.046 6.0
aliphatic hydrocarbons are those having carbon chain lengths ranging from 1,2-Dichloroethane 107-06-2 0.21 6.0
one to and including five, with varying amounts and positions of chlorine 1,1-Dichloroethylene 75-35-4 0.025 6.0
substitution. Methylene chloride 75-9-2 0.089 30
F025--Light Ends Subcategory 1,1,2-Trichloroethane 79-00-5 0.054 6.0
Trichloroethylene 79-01-6 0.054 6.0
Vinyl chloride 75-01-4 0.027 6.0
------------------------------------------------------------------------------
Spent filters and filter aids, and spent desiccant wastes from the Carbon tetrachloride 56-23-5 0.057 6.0
production of certain chlorinated aliphatic hydrocarbons, by free radical Chloroform 67-66-3 0.046 6.0
catalyzed processes. These chlorinated aliphatic hydrocarbons are those Hexachlorobenzene 118-74-1 0.055 10
having carbon chain lengths ranging from one to and including five, with Hexachlorobutadiene 87-68-3 0.055 5.6
varying amounts and positions of chlorine substitution. Hexachloroethane 67-72-1 0.055 30
F025--Spent Filters/Aids and Desiccants Subcategory Methylene chloride 75-9-2 0.089 30
1,1,2-Trichloroethane 79-00-5 0.054 6.0
Trichloroethylene 79-01-6 0.054 6.0
Vinyl chloride 75-01-4 0.27 6.0
------------------
F027 Discarded unused formulations containing tri-, tetra-, or pentachlorophenol HxCDDs (All Hexachlorodibenzo-p-dioxins) NA 0.000063 0.001
or discarded unused formulations containing compounds derived from these HxCDFs (All Hexachlorodibenzofurans) ............ .................. ..................
chlorophenols. (This listing does not include formulations containing PeCDDs (All Pentachlorodibenzo-p-dioxins) NA 0.000063 0.001
hexachlorophene synthesized from prepurified 2,4,5-trichlorophenol as the PeCDFs (All Pentachlorodibenzofurans) ............ .................. ..................
sole component.) Pentachlorophenol NA 0.000063 0.001
TCDDs (All Tetrachlorodibenzo-p-dioxins) ............ .................. ..................
TCDFs (All Tetrachlorodibenzofurans) NA 0.000035 0.001
2,4,5-Trichlorophenol ............ .................. ..................
2,4,6-Trichlorophenol 87-86-5 0.089 7.4
2,3,4,6-Tetrachlorophenol NA .................. ..................
............ 0.000063 0.001
NA .................. ..................
............ 0.000063 0.001
95-95-4 0.18 7.4
88-06-2 0.035 7.4
58-90-2 0.030 7.4
------------------
[[Page 172]]
F028 Residues resulting from the incineration or thermal treatment of soil HxCDDs (All Hexachlorodibenzo-p-dioxins) NA 0.000063 0.001
contaminated with EPA Hazardous Wastes Nos. F020, F021, F023, F026, and HxCDFs (All Hexachlorodibenzofurans) ............ .................. ..................
F027. PeCDDs (All Pentachlorodibenzo-p-dioxins) NA 0.000063 0.001
............ .................. ..................
NA 0.000063 0.001
........................................................................... PeCDFs (All Pentachlorodibenzofurans) NA 0.000035 0.001
........................................................................... Pentachlorophenol 87-86-5 0.089 7.4
........................................................................... TCDDs (All Tetrachlorodibenzo-p-dioxins) NA 0.000063 0.001
........................................................................... TCDFs (All Tetrachlorodibenzofurans) NA 0.000063 0.001
........................................................................... 2,4,5-Trichlorophenol 95-95-4 0.18 7.4
........................................................................... 2,4,6-Trichlorophenol 88-06-2 0.035 7.4
........................................................................... 2,3,4,6-Tetrachlorophenol 58-90-2 0.030 7.4
------------------
F032 Wastewaters (except those that have not come into contact with process Acenaphthene 83-32-9 0.059 3.4
contaminants), process residuals, preservative drippage, and spent Anthracene 120-12-7 0.059 3.4
formulations from wood preserving processes generated at plants that Benz(a)anthracene 56-55-3 0.059 3.4
currently use or have previously used chlorophenolic formulations (except Benzo(b)fluoranthene (difficult to 205-99-2 0.11 6.8
potentially cross-contaminated wastes that have had the F032 waste code distinguish from benzo(k)fluoranthene) ............ .................. ..................
deleted in accordance with Sec. 261.35 of this chapter or potentially Benzo(k)fluoranthene (difficult to ............ 0.11 ..................
cross-contaminated wastes that are otherwise currently regulated as distinguish from benzo(b)fluoranthene) 207-08-9 .................. 6.8
hazardous wastes (i.e., F034 or F035), and where the generator does not Benzo(a)pyrene ............ .................. ..................
resume or initiate use of chlorophenolic formulations). This listing does Chrysene 50-32-8 0.061 3.4
not include K001 bottom sediment sludge from the treatment of wastewater Dibenz(a,h) anthracene ............ .................. ..................
from wood preserving processes that use creosote and/or penta- 2-4-Dimethyl phenol 218-01-9 0.059 3.4
chlorophenol. Fluorene 53-70-3 0.055 8.2
Hexachlorodibenzo-p-dioxins 105-67-9 0.036 14
.......................................... 86-73-7 0.059 3.4
Hexachlorodibenzofurans NA 0.000063, or CMBST 0.001, or CMBST
............ \11\ \11\
NA 0.000063, or CMBST 0.001, or CMBST
\11\ \11\
........................................................................... Indeno (1,2,3-c,d) pyrene 193-39-5 0.0055 3.4
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Pentachlorodibenzo-p-dioxins NA 0.000063, or CMBST 0.001, or CMBST
\11\ \11\
[[Page 173]]
........................................................................... Pentachlorodibenzofurans NA 0.00035, or CMBST 0.001, or CMBST
\11\ \11\
........................................................................... Pentachlorophenol 87-86-5 0.089 7.4
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Pyrene 129-00-0 0.067 8.2
........................................................................... Tetrachlorodibenzo-p-dioxins NA 0.000063, or CMBST 0.001, or CMBST
\11\ \11\
........................................................................... Tetrachlorodibenzofurans NA 0.000063, or CMBST 0.001, or CMBST
\11\ \11\
........................................................................... 2,3,4,6-Tetrachlorophenol 58-90-2 0.030 7.4
........................................................................... 2,4,6-Trichlorophenol 88-06-2 0.035 7.4
........................................................................... Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
------------------
F034 Wasteswaters (except those that have not come into contact with process Acenaphthene 83-32-9 0.059 3.4
contaminants), process residuals, preservative drippage, and spent Anthracene 120-12-7 0.059 3.4
formulations from wood preserving processes generated at plants that use Benz(a)anthracene 56-55-3 0.059 3.4
creosote formulations. This listing does not include K001 bottom sediment Benzo(b)fluoranthene (difficult to 205-99-2 0.11 6.8
sludge from the treatment of wastewater from wood preserving processes distinguish from benzo(k)fluoranthene) ............ .................. ..................
that use creosote and/or pentachlorophenol. Benzo(k)fluoranthene (difficult to ............ .................. 6.8
distinguish from benzo(b)fluoranthene) 207-08-9 0.11 ..................
Benzo(a)pyrene ............ .................. 3.4
............ 0.061
50-32-8
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Dibenz(a,h)anthracene 53-70-3 0.055 8.2
........................................................................... Fluorene 86-73-7 0.059 3.4
........................................................................... Indeno(1,2,3-c,d)pyrene 193-39-5 0.0055 3.4
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... Pyrene 129-00-0 0.067 8.2
........................................................................... Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
------------------
F035 Wastewaters (except those that have not come into contact with process Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
contaminants), process residuals, preservative drippage, and spent Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
formulations from wood preserving processes generated at plants that use
inorganic preservatives containing arsenic or chromium. This listing does
not include K001 bottom sediment sludge from the treatment of wastewater
from wood preserving processes that use creosote and/or pentachlorophenol.
------------------
[[Page 174]]
F037 Petroleum refinery primary oil/water/solids separation sludge--Any sludge Acenaphthene 83-32-9 0.059 NA
generated from the gravitational separation of oil/water/solids during the Anthracene 120-12-7 0.059 3.4
storage or treatment of process wastewaters and oily cooling wastewaters Benzene 71-43-2 0.14 10
from petroleum refineries. Such sludges include, but are not limited to, Benz(a)anthracene 56-55-3 0.059 3.4
those generated in: oil/water/solids separators; tanks and impoundments; Benzo(a)pyrene 50-32-8 0.061 3.4
ditches and other conveyances; sumps; and stormwater units receiving dry bis(2-Ethylhexyl) phthalate 117-81-7 0.28 28
weather flow. Sludge generated in stormwater units that do not receive dry Chrysene 218-01-9 0.059 3.4
weather flow, sludges generated from non-contact once-through cooling Di-n-butyl phthalate 84-74-2 0.057 28
waters segregated for treatment from other process or oily cooling waters, Ethylbenzene 100-41-4 0.057 10
sludges generated in aggressive biological treatment units as defined in Fluorene 86-73-7 0.059 NA
Sec. 261.31(b)(2) (including sludges generated in one or more additional Naphthalene 91-20-3 0.059 5.6
units after wastewaters have been treated in aggressive biological Phenanthrene 85-01-8 0.059 5.6
treatment units) and K051 wastes are not included in this listing. Phenol 108-95-2 0.039 6.2
Pyrene 129-00-0 0.067 8.2
Toluene 108-88-3 0.080 10
Xylenes-mixed isomers (sum of o, m-, and p- 1330-20-7 0.32 30
xylene concentrations)
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Lead 7439-92-1 0.69 NA
........................................................................... Nickel 7440-02-0 NA 11 mg/L TCLP
------------------
[[Page 175]]
F038 Petroleum refinery secondary (emulsified) oil/water/solids separation Benzene 71-43-2 0.14 10
sludge and/or float generated from the physical and/or chemical separation Benzo(a)pyrene 50-32-8 0.061 3.4
of oil/water/solids in process wastewaters and oily cooling wastewaters bis(2-Ethylhexyl) phthalate 117-81-7 0.28 28
from petroleum refineries. Such wastes include, but are not limited to, Chrysene 218-01-9 0.059 3.4
all sludges and floats generated in: induced air floatation (IAF) units, Di-n-butyl phthalate 84-74-2 0.057 28
tanks and impoundments, and all sludges generated in DAF units. Sludges Ethylbenzene 100-41-4 0.057 10
generated in stormwater units that do not receive dry weather flow, Fluorene 86-73-7 0.059 NA
sludges generated from non-contact once-through cooling waters segregated Naphthalene 91-20-3 0.059 5.6
for treatment from other process or oily cooling waters, sludges and Phenanthrene 85-01-8 0.059 5.6
floats generated in aggressive biological treatment units as defined in Phenol 108-95-2 0.039 6.2
Sec. 261.31(b)(2) (including sludges and floats generated in one or more Pyrene 129-00-0 0.067 8.2
additional units after wastewaters have been treated in aggressive Toluene 108-88-3 0.080 10
biological units) and F037, K048, and K051 are not included in this Xylenes-mixed isomers (sum of o, m-, and p- 1330-20-7 0.32 30
listing. xylene concentrations) ............ .................. ..................
Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
Cyanides (Total) \7\ 57-12-5 1.2 590
Lead 7439-92-1 0.69 NA
........................................................................... Nickel 7440-02-0 NA 11 mg/L TCLP
------------------
F039 Leachate (liquids that have percolated through land disposed wastes) Acenaphthylene 208-96-8 0.059 3,4
resulting from the disposal of more than one restricted waste classified Acenaphthene 83-32-9 0.059 3.4
as hazardous under subpart D of this part. (Leachate resulting from the Acetone 67-64-1 0.28 160
disposal of one or more of the following EPA Hazardous Wastes and no other Acetonitrile 75-05-8 5.6 NA
Hazardous Wastes retains its EPA Hazardous Waste Number(s): F020, F021, Acetophenone 96-86-2 0.010 9.7
F022, F026, F027, and/or F028.) 2-Acetylaminofluorene 53-96-3 0.059 140
Acrolein 107-02-8 0.29 NA
........................................................................... Acrylonitrile 107-13-1 0.24 84
........................................................................... Aldrin 309-00-2 0.021 0.066
........................................................................... 4-Aminobiphenyl 92-67-1 0.13 NA
........................................................................... Aniline 62-53-3 0.81 14
........................................................................... Anthracene 120-12-7 0.059 3.4
........................................................................... Aramite 140-57-8 0.36 NA
........................................................................... alpha-BHC 319-84-6 0.00014 0.066
........................................................................... beta-BHC 319-85-7 0.00014 0.066
........................................................................... delta-BHC 319-86-8 0.023 0.066
........................................................................... gamma-BHC 58-89-9 0.0017 0.066
........................................................................... Benzene 71-43-2 0.14 10
........................................................................... Benz(a)anthracene 56-55-3 0.059 3.4
........................................................................... Benzo(b)fluoranthene (difficult to 205-99-2 0.11 6.8
distinguish from benzo(k)fluoranthene)
........................................................................... Benzo(k)fluoranthene (difficult to 207-08-9 0.11 6.8
distinguish from benzo(b)fluoranthene)
........................................................................... Benzo(g,h,i)perylene 191-24-2 0.0055 1.8
........................................................................... Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... Bromodichloromethane 75-27-4 0.35 15
........................................................................... Methyl bromide (Bromomethane) 74-83-9 0.11 15
........................................................................... 4-Bromophenyl phenyl ether 101-55-3 0.055 15
........................................................................... n-Butyl alcohol 71-36-3 5.6 2.6
........................................................................... Butyl benzyl phthalate 85-68-7 0.017 28
........................................................................... 2-sec-Buty-4,6-dinitrophenol (Dinoseb) 88-85-7 0.066 2.5
[[Page 176]]
........................................................................... Carbon disulfide 75-15-0 3.8 NA
........................................................................... Carbon tetrachloride 56-23-5 0.057 6.0
........................................................................... Chlordane (alpha and gamma isomers) 57-74-9 0.0033 0.26
........................................................................... p-Chloroaniline 106-47-8 0.46 16
........................................................................... Chlorobenzene 108-90-7 0.057 6.0
........................................................................... Chlorobenzilate 510-15-6 0.10 NA
........................................................................... 2-Chloro-1,3-butadiene 126-99-8 0.057 NA
........................................................................... Chlorodibromomethane 124-48-1 0.057 15
........................................................................... Chloroethane 75-00-3 0.27 6.0
........................................................................... bis(2-Chloroethoxy)methane 111-91-1 0.036 7.2
........................................................................... bis(2-Chloroethyl)ether 111-44-4 0.033 6.0
........................................................................... Chloroform 67-66-3 0.046 6.0
........................................................................... bis(2-Chloroisopropyl)ether 39638-32-9 0.055 7.2
........................................................................... p-Chloro-m-cresol 59-50-7 0.018 14
........................................................................... Chloromethane (Methyl chloride) 74-87-3 0.19 30
........................................................................... 2-Chloronaphthalene 91-58-7 0.055 5.6
........................................................................... 2-Chlorophenol 95-57-8 0.044 5.7
........................................................................... 3-Chloropropylene 107-05-1 0.036 30
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... o-Cresol 95-48-7 0.11 5.6
........................................................................... m-Cresol (difficult to distinguish from p- 108-39-4 0.77 5.6
cresol)
........................................................................... p-Cresol (difficult to distinguish from m- 106-44-5 0.77 5.6
cresol)
........................................................................... Cyclohexanone 108-94-1 0.36 NA
........................................................................... 1,2-Dibromo-3-chloropropane 96-12-8 0.11 15
........................................................................... Ethylene dibromide (1,2-Dibromoethane) 106-93-4 0.028 15
........................................................................... Dibromomethane 74-95-3 0.11 15
........................................................................... 2,4-D (2,4-Dichlorophenoxyacetic acid) 94-75-7 0.72 10
........................................................................... o,p'-DD 53-19-0 0.023 0.087
........................................................................... p,p'-DDD 72-54-8 0.023 0.087
........................................................................... o,p'-DDE 3424-82-6 0.031 0.087
........................................................................... p,p'-DDE 72-55-9 0.031 0.087
........................................................................... o,p'-DDT 789-02-6 0.0039 0.087
........................................................................... p,p'-DDT 50-29-3 0.0039 0.087
........................................................................... Dibenz(a,h)anthracene 53-70-3 0.055 8.2
........................................................................... Dibenz(a,e)pyrene 192-65-4 0.061 NA
[[Page 177]]
........................................................................... m-Dichlorobenzene 541-73-1 0.036 6.0
........................................................................... o-Dichlorobenzene 95-50-1 0.088 6.0
........................................................................... p-Dichlorobenzene 106-46-7 0.090 6.0
........................................................................... Dichlorodifluoromethane 75-71-8 0.23 7.2
........................................................................... 1,1-Dichloroethane 75-34-3 0.059 6.0
........................................................................... 1,2-Dichloroethane 107-06-2 0.21 6.0
........................................................................... 1,1-Dichloroethylene 75-35-4 0.025 6.0
........................................................................... trans-1,2-Dichloroethylene 156-60-5 0.054 30
........................................................................... 2,4-Dichlorophenol 120-83-2 0.044 14
........................................................................... 2,6-Dichlorophenol 87-65-0 0.044 14
........................................................................... 1,2-Dichloropropane 78-87-5 0.85 18
........................................................................... cis-1,3-Dichloropropylene 10061-01-5 0.036 18
........................................................................... trans-1,3-Dichloropropylene 10061-02-6 0.036 18
........................................................................... Dieldrin 60-57-1 0.017 0.13
........................................................................... Diethyl phthalate 84-66-2 0.20 28
........................................................................... 2-4-Dimethyl phenol 105-67-9 0.036 14
........................................................................... Dimethyl phthalate 131-11-3 0.047 28
........................................................................... Di-n-butyl phthalate 84-74-2 0.057 28
........................................................................... 1,4-Dinitrobenzene 100-25-4 0.32 2.3
........................................................................... 4,6-Dinitro-o-cresol 534-52-1 0.28 160
........................................................................... 2,4-Dinitrophenol 51-28-5 0.12 160
........................................................................... 2,4-Dinitrotoluene 121-14-2 0.32 140
........................................................................... 2,6-Dinitrotoluene 606-20-2 0.55 28
........................................................................... Di-n-octyl phthalate 117-84-0 0.017 28
........................................................................... Di-n-propylnitrosamine 621-64-7 0.40 14
........................................................................... 1,4-Dioxane 123-91-1 12.0 170
........................................................................... Diphenylamine (difficult to distinguish 122-39-4 0.92 NA
from diphenylnitrosamine)
........................................................................... Diphenylnitrosamine (difficult to 86-30-6 0.92 NA
distinguish from diphenylamine)
........................................................................... 1,2-Diphenylhydrazine 122-66-7 0.087 NA
........................................................................... Disulfoton 298-04-4 0.017 6.2
........................................................................... Endosulfan I 939-98-8 0.023 0.066
........................................................................... Endosulfan II 33213-6-5 0.029 0.13
........................................................................... Endosulfan sulfate 1031-07-8 0.029 0.13
........................................................................... Endrin 72-20-8 0.0028 0.13
........................................................................... Endrin aldehyde 7421-93-4 0.025 0.13
........................................................................... Ethyl acetate 141-78-6 0.34 33
........................................................................... Ethyl cyanide (Propanenitrile) 107-12-0 0.24 360
........................................................................... Ethyl benzene 100-41-4 0.057 10
........................................................................... Ethyl ether 60-29-7 0.12 160
........................................................................... bis(2-Ethylhexyl) phthalate 117-81-7 0.28 28
........................................................................... Ethyl methacrylate 97-63-2 0.14 160
........................................................................... Ethylene oxide 75-21-8 0.12 NA
........................................................................... Famphur 52-85-7 0.017 15
........................................................................... Fluoranthene 206-44-0 0.068 3.4
........................................................................... Fluorene 86-73-7 0.059 3.4
........................................................................... Heptachlor 76-44-8 0.0012 0.066
........................................................................... Heptachlor epoxide 1024-57-3 0.016 0.066
........................................................................... 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin 35822-46-9 0.000035 0.0025
(1,2,3,4,6,7,8-HpCDD)
[[Page 178]]
........................................................................... 1, 2,3,4,6,7,8-Heptachlorodibenzofuran 67562-39-4 0.000035 0.0025
(1,2,3,4,6,7,8-HpCDF)
........................................................................... 1,2,3,4,7,8,9-Heptachlorodibenzofuran 55673-89-7 0.000035 0.0025
(1,2,3,4,7,8,9-HpCDF)
........................................................................... Hexachlorobenzene 118-74-1 0.055 10
........................................................................... Hexachlorobutadiene 87-68-3 0.055 5.6
........................................................................... Hexachlorocyclopentadiene 77-47-4 0.057 2.4
........................................................................... HxCDDs (All Hexachlorodibenzo-p-dioxins) NA 0.000063 0.001
........................................................................... HxCDFs (All Hexachlorodibenzofurans) NA 0.000063 0.001
........................................................................... Hexachloroethane 67-72-1 0.055 30
........................................................................... Hexachloropropylene 1888-71-7 0.035 30
........................................................................... Indeno (1,2,3-c,d) pyrene 193-39-5 0.0055 3.4
........................................................................... Indomethane 74-88-4 0.019 65
........................................................................... Isobutyl alcohol 78-83-1 5.6 170
........................................................................... Isodrin 465-73-6 0.021 0.066
........................................................................... Isosafrole 120-58-1 0.081 2.6
........................................................................... Kepone 143-50-8 0.0011 0.13
........................................................................... Methacylonitrile 126-98-7 0.24 84
........................................................................... Methanol 67-56-1 5.6 NA
........................................................................... Methapyrilene 91-80-5 0.081 1.5
........................................................................... Methoxychlor 72-43-5 0.25 0.18
........................................................................... 3-Methylcholanthrene 56-49-5 0.0055 15
........................................................................... 4,4-Methylene bis(2-chloroaniline) 101-14-4 0.50 30
........................................................................... Methylene chloride 75-09-2 0.089 30
........................................................................... Methyl ethyl ketone 78-93-3 0.28 36
........................................................................... Methyl isobutyl ketone 108-10-1 0.14 33
........................................................................... Methyl methacrylate 80-62-6 0.14 160
........................................................................... Methyl methanesulfonate 66-27-3 0.018 NA
........................................................................... Methyl parathion 298-00-0 0.014 4.6
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... 2-Naphthylamine 91-59-8 0.52 NA
........................................................................... p-Nitroaniline 100-01-6 0.028 28
........................................................................... Nitrobenzene 98-95-3 0.068 14
........................................................................... 5-Nitro-o-toluidine 99-55-8 0.32 28
........................................................................... p-Nitrophenol 100-02-7 0.12 29
........................................................................... N-Nitrosodiethylamine 55-18-5 0.40 28
........................................................................... N-Nitrosodimethylamine 62-75-9 0.40 NA
[[Page 179]]
........................................................................... N-Nitroso-di-n-butylamine 924-16-3 0.40 17
........................................................................... N-Nitrosomethylethylamine 10595-95-6 0.40 2.3
........................................................................... N-Nitrosomorpholine 59-89-2 0.40 2.3
........................................................................... N-Nitrosopiperidine 100-75-4 0.013 35
........................................................................... N-Nitrosopyrrolidine 930-55-2 0.013 35
........................................................................... 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin 3268-87-9 0.000063 0.005
(OCDD)
........................................................................... 1,2,3,4,6,7,8,9-Octachlorodibenzofuran 39001-02-0 0.000063 0.005
(OCDF)
........................................................................... Parathion 56-38-2 0.014 4.6
........................................................................... Total PCBs (sum of all PCB isomers, or all 1336-36-3 0.10 10
Aroclors)
........................................................................... Pentachlorobenzene 608-93-5 0.055 10
........................................................................... PeCDDs (All Pentachlorodibenzo-p-dioxins) NA 0.000063 0.001
........................................................................... PeCDFs (All Pentachlorodibenzofurans) NA 0.000035 0.001
........................................................................... Pentachloronitrobenzene 82-68-8 0.055 4.8
........................................................................... Pentachlorophenol 87-86-5 0.089 7.4
........................................................................... Phenacetin 62-44-2 0.081 16
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Phorate 298-02-2 0.021 4.6
........................................................................... Phthalic anhydride 85-44-9 0.055 NA
........................................................................... Pronamide 23950-58-5 0.093 1.5
........................................................................... Pyrene 129-00-0 0.067 8.2
........................................................................... Pyridine 110-86-1 0.014 16
........................................................................... Safrole 94-59-7 0.081 22
........................................................................... Silvex (2,4,5-TP) 93-72-1 0.72 7.9
........................................................................... 2,4,5-T 93-76-5 0.72 7.9
........................................................................... 1,2,4,5-Tetrachlorobenzene 95-94-3 0.055 14
........................................................................... TCDDs (All Tetrachlorodibenzo-p-dioxins) NA 0.000063 0.001
........................................................................... TCDFs (All Tetrachlorodibenzofurans) NA 0.000063 0.001
........................................................................... 1,1,1,2-Tetrachloroethane 630-20-6 0.057 6.0
........................................................................... 1,1,2,2-Tetrachloroethane 79-34-6 0.057 6.0
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
........................................................................... 2,3,4,6-Tetrachlorophenol 58-90-2 0.030 7.4
........................................................................... Toluene 108-88-3 0.080 10
........................................................................... Toxaphene 8001-35-2 0.0095 2.6
........................................................................... Bromoform (Tribromomethane) 75-25-2 0.63 15
........................................................................... 1,2,4-Trichlorobenzene 120-82-1 0.055 19
........................................................................... 1,1,1-Trichloroethane 71-55-6 0.054 6.0
........................................................................... 1,1,2-Trichloroethane 79-00-5 0.054 6.0
........................................................................... Trichloroethylene 79-01-6 0.054 6.0
........................................................................... Trichlorofluoromethane 75-69-4 0.020 30
........................................................................... 2,4,5-Trichlorophenol 95-95-4 0.18 7.4
........................................................................... 2,4,6-Trichlorophenol 88-06-2 0.035 7.4
........................................................................... 1,2,3-Trichloropropane 96-18-4 0.85 30
........................................................................... 1,1,2-Trichloro-1,2,2-trifluoroethane 76-13-1 0.057 30
[[Page 180]]
........................................................................... tris(2,3-Dibromopropyl) phosphate 126-72-7 0.11 NA
........................................................................... Vinyl chloride 75-01-4 0.27 6.0
........................................................................... Xylenes-mixed isomers (sum of o-, m-, and 1330-20-7 0.32 30
p-xylene concentrations)
........................................................................... Antimony 7440-36-0 1.9 1.15 mg/L TCLP
........................................................................... Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
........................................................................... Barium 7440-39-3 1.2 21 mg/L TCLP
........................................................................... Beryllium 7440-41-7 0.82 NA
........................................................................... Cadmium 7440-43-9 0.69 0.11 mg/L TCLP
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 NA
........................................................................... Fluoride 16984-48-8 35 NA
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
........................................................................... Mercury 7439-97-6 0.15 0.25 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
........................................................................... Selenium 7782-49-2 0.82 5.7 mg/L TCLP
........................................................................... Silver 7440-22-4 0.43 0.14 mg/L TCLP
........................................................................... Sulfide 8496-25-8 14 NA
........................................................................... Thallium 7440-28-0 1.4 NA
........................................................................... Vanadium 7440-62-2 4.3 NA
------------------
K001 Bottom sediment sludge from the treatment of wastewaters from wood Naphthalene 91-20-3 0.059 5.6
preserving processes that use creosote and/or pentachlorophenol. Pentachlorophenol 87-86-5 0.089 7.4
Phenanthrene 85-01-8 0.059 5.6
Pyrene 129-00-0 0.067 8.2
........................................................................... Toluene 108-88-3 0.080 10
........................................................................... Xylenes-mixed isomers (sum of o-, m-, and 1330-20-7 0.32 30
p-xylene concentrations)
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
K002 Wastewater treatment sludge from the production of chrome yellow and orange Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
pigments. Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
K003 Wastewater treatment sludge from the production of molybdate orange Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
pigments. Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
[[Page 181]]
K004 Wastewater treatment sludge from the production of zinc yellow pigments. Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
K005 Wastewater treatment sludge from the production of chrome green pigments. Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
Lead 7439-92-1 0.69 0.75 mg/L TCLP
Cyanides (Total) \7\ 57-12-5 1.2 590
------------------
K006 Wastewater treatment sludge from the production of chrome oxide green Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
pigments (anhydrous). Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------------------------------------------------------------------
Wastewater treatment sludge from the production of chrome oxide green Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
pigments (hydrated). Lead 7439-92-1 0.69 NA
------------------
K007 Wastewater treatment sludge from the production of iron blue pigments. Chromium (Total) 7440-47-3 2,77 0.60 mg/L TCLP
Lead 7439-92-1 0.69 0.75 mg/L TCLP
Cyanides (Total) \7\ 57-12-5 1.2 590
------------------
K008 Oven residue from the production of chrome oxide green pigments. Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
K009 Distillation bottoms from the production of acetaldehyde from ethylene. Chloroform 67-66-3 0.046 6.0
------------------
K010 Distillation side cuts from the production of acetaldehyde from ethylene. Chloroform 67-66-3 0.046 6.0
------------------
K011 Bottom stream from the wastewater stripper in the production of Acetonitrile 75-05-8 5.6 38
acrylonitrile. Acrylonitrile 107-13-1 0.24 84
........................................................................... Acrylamide 79-06-1 19 23
........................................................................... Benzene 71-43-2 0.14 10
........................................................................... Cyanide (Total) 57-12-5 1.2 590
------------------
K013 Bottom stream from the acetonitrile column in the production of Acetonitrile 75-05-8 5.6 38
acrylonitrile. Acrylonitrile 107-13-1 0.24 84
........................................................................... Acrylamide 79-06-1 19 23
........................................................................... Benzene 71-43-2 0.14 10
........................................................................... Cyanide (Total) 57-12-5 1.2 590
------------------
K014 Bottoms from the acetonitrile purification column in the production of Acetonitrile 75-05-8 5.6 38
acrylonitrile. Acrylonitrile 107-13-1 0.24 84
........................................................................... Acrylamide 79-06-1 19 23
........................................................................... Benzene 71-43-2 0.14 10
........................................................................... Cyanide (Total) 57-12-5 1.2 590
------------------
K015 Still bottoms from the distillation of benzyl chloride. Anthracene 120-12-7 0.059 3.4
Benzal chloride 98-87-3 0.055 6.0
........................................................................... Benzo(b)fluoranthene (difficult to 205-99-2 0.11 6.8
distinguish from benzo(k)fluoranthene)
........................................................................... Benzo(k)fluoranthene (difficult to 207-08-9 0.11 6.8
distinguish from benzo(b)fluoranthene)
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... Toluene 108-88-3 0.080 10
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
[[Page 182]]
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
------------------
K016 Heavy ends or distillation residues from the production of carbon Hexachlorobenzene 118-74-1 0.055 10
tetrachloride. Hexachlorobutadiene 87-68-3 0.055 5.6
........................................................................... Hexachlorocyclopentadiene 77-47-4 0.057 2.4
........................................................................... Hexachloroethane 67-72-1 0.055 30
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
------------------
K017 Heavy ends (still bottoms) from the purification column in the production bis(2-Chloroethyl)ether 111-44-4 0.033 6.0
of epichlorohydrin. 1,2-Dichloropropane 78-87-5 0.85 18
1,2,3-Trichloropropane 96-18-4 0.85 30
------------------
K018 Heavy ends from the fractionation column in ethyl chloride production. Chloroethane 75-00-3 0.27 6.0
Chloromethane 74-87-3 0.19 NA
1,1-Dichloroethane 75-34-3 0.059 6.0
........................................................................... 1,2-Dichloroethane 107-06-2 0.21 6.0
........................................................................... Hexachlorobenzene 118-74-1 0.055 10
........................................................................... Hexachlorobutadiene 87-68-3 0.055 5.6
........................................................................... Hexachloroethane 67-72-1 0.055 30
........................................................................... Pentachloroethane 76-01-7 NA 6.0
........................................................................... 1,1,1-Trichloroethane 71-55-6 0.054 6.0
------------------
K019 Heavy ends from the distillation of ethylene dichloride in ethylene bis(2-Chloroethyl)ether 111-44-4 0.033 6.0
dichloride production. Chlorobenzene 108-90-7 0.057 6.0
........................................................................... Chloroform 67-66-3 0.046 6.0
........................................................................... p-Dichlorobenzene 106-46-7 0.090 NA
........................................................................... 1,2-Dichloroethane 107-06-2 0.21 6.0
........................................................................... Fluorene 86-73-7 0.059 NA
........................................................................... Hexachloroethane 67-72-1 0.055 30
........................................................................... Nephthalene 91-20-3 0.059 5.6
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... 1,2,4,5-Tetrachlorobenzene 95-94-3 0.055 NA
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
........................................................................... 1,2,4-Trichlorobenzene 120-82-1 0.055 19
........................................................................... 1,1,1-Trichloroethane 71-55-6 0.054 6.0
------------------
[[Page 183]]
K020 Heavy ends from the distillation of vinyl chloride in vinyl chloride 1,2-Dichloroethane 107-06-2 0.21 6.0
monomer production. 1,1,2,2-Tetrachloroethane 79-34-6 0.057 6.0
Tetrachloroethylene 127-18-4 0.056 6.0
------------------
K021 Aqueous spent antimony catalyst waste from fluoromethanes production. Carbon tetrachloride 56-23-5 0.057 6.0
Chloroform 67-66-3 0.046 6.0
Antimony 7440-36-0 1.9 1.15 mg/L TCLP
------------------
K022 Distillation bottoms tars from the production of phenol/acetone from Toluene 108-88-3 0.080 10
cumene. Acetophenone 96-86-2 0.010 9.7
........................................................................... Diphenylamine (difficult to distinguish 122-39-4 0.92 13
from diphenylnitrosamine)
........................................................................... Diphenylnitrosamine (difficult to 86-30-6 0.92 13
distinguish from diphenylamine)
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
------------------
K023 Distillation light ends from the production of phthalic anhydride from Phthalic anhydride (measured as Phthalic 100-21-0 0.055 28
naphthalene. acid or Terephthalic acid)
........................................................................... Phthalic anhydride (measured as Phthalic 85-44-9 0.055 28
acid or Terephthalic acid)
------------------
K024 Distillation bottoms from the production of phthalic anhydride from Phthalic anhydride (measured as Phthalic 100-21-0 0.055 28
naphthalene. acid or Terephthalic acid)
........................................................................... Phthalic anhydride (measured as Phthalic 85-44-9 0.055 28
acid or Terephthalic acid)
------------------
K025 Distillation bottoms from the production of nitrobenzene by the nitration NA NA LLEXT fb SSTRP fb CMBST
of benzene. CARBN; or CMBST
------------------
K026 Stripping still tails from the production of methyl ethyl pyridines. NA NA CMBST CMBST
------------------
K027 Centrifuge and distillation residues from toluene diisocyanate production. NA NA CARBN; or CMBST CMBST
------------------
K028 Spent catalyst from the hydrochlorinator reactor in the production of 1,1,1- 1,1-Dichloroethane 75-34-3 0.059 6.0
trichloroethane. trans-1,2-Dichloroethylene 156-60-5 0.054 30
........................................................................... Hexachlorobutadiene 87-68-3 0.055 5.6
........................................................................... Hexachloroethane 67-72-1 0.055 30
........................................................................... Pentachloroethane 76-01-7 NA 6.0
........................................................................... 1,1,1,2-Tetrachloroethane 630-20-6 0.057 6.0
........................................................................... 1,1,2,2-Tetrachloroethane 79-34-6 0.057 6.0
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
........................................................................... 1,1,1-Trichloroethane 71-55-6 0.054 6.0
........................................................................... 1,1,2-Trichloroethane 79-00-5 0.054 6.0
........................................................................... Cadmium 7440-43-9 0.69 NA
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
[[Page 184]]
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
------------------
K029 Waste from the product steam stripper in the production of 1,1,1- Chloroform 67-66-3 0.046 6.0
trichloroethane. 1,2-Dichloroethane 107-06-2 0.21 6.0
........................................................................... 1,1-Dichloroethylene 75-35-4 0.025 6.0
........................................................................... 1,1,1-Trichloroethane 71-55-6 0.054 6.0
........................................................................... Vinyl chloride 75-01-4 0.27 6.0
------------------
K030 Column bodies or heavy ends from the combined production of o-Dichlorobenzene 95-50-1 0.088 NA
trichloroethylene and perchloroethylene. p-Dichlorobenzene 106-46-7 0.090 NA
........................................................................... Hexachlorobutadiene 87-68-3 0.055 5.6
........................................................................... Hexachloroethane 67-72-1 0.055 30
........................................................................... Hexachloropropylene 1888-71-7 NA 30
........................................................................... Pentachlorobenzene 608-93-5 NA 10
........................................................................... Pentachloroethane 76-01-7 NA 6.0
........................................................................... 1,2,4,5-Tetrachlorobenzene 95-94-3 0.055 14
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
........................................................................... 1,2,4-Trichlorobenzene 120-82-1 0.055 19
------------------
K031 By-product salts generated in the production of MSMA and cacodylic acid. Arsenic 7440-38-2 14 5.0 mg/L TCLP
------------------
K032 Wastewater treatment sludge from the production of chlordane. Hexachlorocyclopentadiene 77-47-4 0.057 2.4
Chlordane (alpha and gamma isomers) 57-74-9 0.0033 0.26
........................................................................... Heptachlor 76-44-8 0.0012 0.066
........................................................................... Heptachlor epoxide 1024-57-3 0.016 0.066
------------------
K033 Wastewater and scrub water from the clorination of cyclopentadiene in the Hexachlorocyclopentadiene 77-47-4 0.057 2.4
production of chlordane.
------------------
K034 Filter solids from the filtration of hexachlorocyclopentadiene in the Hexachlorocyclopentadiene 77-47-4 0.057 2.4
production of chlordane.
------------------
K035 Wastewater treatment sludges generated in the production of cresote. Acenaphthene 83-32-9 NA 3.4
Anthracene 120-12-7 NA 3.4
........................................................................... Benz(a)anthracene 56-55-3 0.059 3.4
........................................................................... Bemzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... o-Cresol 95-48-7 0.11 5.6
[[Page 185]]
........................................................................... m-Cresol (difficult to distinguish from p- 108-39-4 0.77 5.6
cresol)
........................................................................... p-Cresol (difficult to distinguish from m- 106-44-5 0.77 5.6
cresol)
........................................................................... Dibenz(a,h)anthracene 53-70-3 NA 8.2
........................................................................... Fluoranthene 206-44-0 0.068 3.4
........................................................................... Fluorene 86-73-7 NA 3.4
........................................................................... Indeno(1,2,3-cd)pyrene 193-39-5 NA 3.4
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Phenanthrene 85-01-1 0.059 5.6
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Pyrene 129-00-0 0.067 8.2
------------------
K036 Still bottoms from toluene reclamation distillation in the production of Disulfoton 298-04-4 0.017 6.2
disulfoton.
------------------
K037 Wastewater treatment sludges from the production of disulfoton. Disulfoton 298-04-4 0.017 6.2
Toluene 108-88-3 0.080 10
------------------
K038 Wastewater from the washing and stripping of phorate production. Phorate 298-02-2 0.021 4.6
------------------
K039 Filter cake from the filtration of diethylphorphorodithioic acid in the NA NA CARBN; or CMBST CMBST
production of phorate.
------------------
K040 Wastewater treatment sludge from the production of phorate. Phorate 298-02-2 0.021 4.6
------------------
K041 Wastewater treatment sludge from the production of toxaphene. Toxaphene 8001-35-2 0.0095 2.6
------------------
K042 Heavy ends or distillation residues from the distillation of o-Dichlorobenzene 95-50-1 0.088 6.0
tetrachlorobenzene in the production of 2,4,5-T. p-Dichlorobenzene 106-46-7 0.090 6.0
Pentachlorobenzene 608-93-5 0.055 10
........................................................................... 1,2,4,5-Tetrachlorobenzene 95-94-3 0.055 14
........................................................................... 1,2,4-Trichlorobenzene 120-82-1 0.055 19
------------------
K043 2,6-Dichlorophenol waste from the production of 2,4-D. 2,4-Dichlorophenol 120-83-2 0.044 14
........................................................................... 2,6-Dichlorophenol 187-65-0 0.044 14
........................................................................... 2,4,5-Trichlorophenol 95-95-4 0.18 7.4
........................................................................... 2,4,6-Trichlorophenol 88-06-2 0.035 7.4
........................................................................... 2,3,4,6-Tetrachlorophenol 58-90-2 0.030 7.4
........................................................................... Pentachlorophenol 87-86-5 0.089 7.4
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
........................................................................... HxCDDs (All Hexachlorodibenzo-p-dioxins) NA 0.000063 0.001
........................................................................... HxCDFs (All Hexachlorodibenzofurans) NA 0.000063 0.001
........................................................................... PeCDDs (All Pentachlorodibenzo-p-dioxins) NA 0.000063 0.001
........................................................................... PeCDFs (All Pentachlorodibenzofurans) NA 0.000035 0.001
........................................................................... TCDDs (All Tetrachlorodibenzo-p-dioxins) NA 0.000063 0.001
[[Page 186]]
........................................................................... TCDFs (All Tetrachlorodibenzofurans) NA 0.000063 0.001
------------------
K044 Wastewater treatment sludges from the manufacturing and processing of NA NA DEACT DEACT
explosives.
------------------
K045 Spent carbon from the treatment of wastewater containing explosives. NA NA DEACT DEACT
------------------
K046 Wastewater treatment sludges from the manufacturing, formulation and Lead 7439-92-1 0.69 0.75 mg/L TCLP
loading of lead-based initiating compounds.
------------------
K047 Pink/red water form TNT operations. NA NA DEACT DEACT
------------------
K048 Dissolved air flotation (DAF) float from the petroleum refining industry. Benzene 71-43-2 0.14 10
Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... bis(2-Ethylhexyl)phthalate 117-81-7 0.28 28
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Di-n-butyl phthalate 84-74-2 0.057 28
........................................................................... Ethylbenzene 100-41-4 0.057 10
........................................................................... Fluorene 86-73-7 0.059 NA
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Pyrene 129-00-0 0.067 8.2
........................................................................... Toluene 108-88-33 0.080 10
........................................................................... Xylenes-mixed isomers (sum of o-, m-, and 1330-20-7 0.32 30
p-xylene concentrations)
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Chanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Lead 7439-92-1 0.69 NA
........................................................................... Nickel 7440-02-0 NA 11 mg/L TCLP
------------------
K049 Slop oil emulsion solids from the petroleum refining industry. Anthracene 120-12-7 0.059 3.4
Benzene 71-43-2 0.14 10
........................................................................... Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... bis(2-Ethylhexyl)phthalate 117-81-7 0.28 28
........................................................................... Carbon disulfide 75-15-0 3.8 NA
........................................................................... Chrysene 2218-01-9 0.059 3.4
........................................................................... 2,4-Dimethylphenol 105-67-9 0.036 NA
........................................................................... Ethylbenzene 100-41-4 0.057 10
[[Page 187]]
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Pyrene 129-00-0 0.067 8.2
........................................................................... Toluene 108-88-3 0.080 10
........................................................................... Xylenes-mixed isomers (sum of o-, m-, and 1330-20-7 0.32 30
p-xylene concentrations)
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Lead 7439-92-1 0.69 NA
........................................................................... Nickel 7440-02-0 NA 11 mg/L TCLP
------------------
K050 Heat exchanger bundle cleaning sludge from the petroleum refining industry. Benzo(a)pyrene 50-32-8 0.061 3.4
Phenol 108-95-2 0.039 6.2
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Lead 7439-92-1 0.69 NA
........................................................................... Nickel 7440-02-0 NA 11 mg/L TCLP
------------------
K051 API separator sludge from the petroleum refining industry. Acenaphthene 83-32-9 0.059 NA
Anthracene 120-12-7 0.059 3.4
........................................................................... Benz(a)anthracene 56-55-3 0.059 3.4
........................................................................... Benzene 71-43-2 0.14 10
........................................................................... Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... bis(2-Ethylhexyl)phthalate 117-81-7 0.28 28
........................................................................... Chrysene 2218-01-9 0.059 3.4
........................................................................... Di-n-butyl phthalate 105-67-9 0.057 28
........................................................................... Ethylbenzene 100-41-4 0.057 10
........................................................................... Fluorene 86-73-7 0.059 NA
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Pyrene 129-00-0 0.067 8.2
........................................................................... Toluene 108-88-3 0.08 10
........................................................................... Xylenes-mixed isomers (sum of o-, m-, and 1330-20-7 0.32 30
p-xylene concentrations)
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Lead 7439-92-1 0.69 NA
........................................................................... Nickel 7440-02-0 NA 11 mg/L TCLP
------------------
K052 Tank bottoms (leaded) from the petroleum refining industry. Benzene 71-43-2 0.14 10
Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... o-Cresol 95-48-7 0.11 5.6
........................................................................... m-Cresol (difficult to distinguish from p- 108-39-4 0.77 5.6
cresol)
........................................................................... p-Cresol (difficult to distinguish from m- 106-44-5 0.77 5.6
cresol)
........................................................................... 2,4-Dimethylphenol 105-67-9 0.036 NA
........................................................................... Ethylbenzene 100-41-4 0.057 10
........................................................................... Naphthalene 91-20-3 0.059 5.6
[[Page 188]]
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Toluene 108-88-3 0.08 10
........................................................................... Xylenes-mixed isomers (sum of o-, m-, and 1330-20-7 0.32 30
p-xylene concentrations)
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Lead 7439-92-1 0.69 NA
........................................................................... Nickel 7440-02-0 NA 11 mg/L TCLP
------------------
K060 Ammonia still lime sludge from coking operations. Benzene 71-43-2 0.14 10
........................................................................... Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
------------------
K061 Emission control dust/sludge from the primary production of steel in Antimony 7440-36-0 NA 1.15 mg/L TCLP
electric furnaces. Arsenic 7440-38-2 NA 5.0 mg/L TCLP
........................................................................... Barium 7440-39-3 NA 21 mg/L TCLP
........................................................................... Beryllium 7440-41-7 NA 1.22 mg/L TCLP
........................................................................... Cadmium 7440-43-9 0.69 0.11 mg/L TCLP
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
........................................................................... Mercury 7439-97-6 NA 0.025 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
........................................................................... Selenium 7782-49-2 NA 5.7 mg/L TCLP
........................................................................... Silver 7440-22-4 NA 0.14 mg/L TCLP
........................................................................... Thallium 7440-28-0 NA 0.20 mg/L TCLP
........................................................................... Zinc 7440-66-6 NA 4.3 mg/L TCLP
------------------
K062 Spent pickle liquor generated by steel finishing operations of facilities Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
within the iron and steel industry (SIC Codes 331 and 332). Lead 7439-92-1 0.69 0.75 mg/L TCLP
Nickel 7440-02-0 3.98 NA
------------------
K069 Emission control dust/sludge from secondary lead smelting.--Calcium Sulfate Cadmium 7440-43-9 0.69 0.11 mg/L TCLP
(Low Lead) Subcategory Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------------------------------------------------------------------
[[Page 189]]
Emission control dust/sludge from secondary lead smelting.--Non-Calcium NA NA NA RLEAD
Sulfate (High Lead) Subcategory
------------------
K071 K071 (Brine purification muds from the mercury cell process in chlorine Mercury 7439-97-6 NA 0.20 mg/L TCLP
production, where separately prepurified brine is not used) nonwastewaters
that are residues from RMERC.
------------------------------------------------------------------------------
K071 (Brine purification muds from the mercury cell process in chlorine Mercury 7439-97-6 NA 0.025 mg/L TCLP
production, where separately prepurified brine is not used.)
nonwastewaters that are not residues from RMERC.
------------------------------------------------------------------------------
All K071 wastewaters. Mercury 7439-97-6 0.15 NA
------------------
K073 Chlorinated hydrocarbon waste from the purification step of the diaphragm Carbon tetrachloride 56-23-5 0.057 6.0
cell process using graphite anodes in chlorine production. Chloroform 67-66-3 0.046 6.0
Hexachloroethane 67-72-1 0.055 30
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
........................................................................... 1,1,1-Trichloroethane 71-55-6 0.054 6.0
------------------
K083 Distillation bottoms from aniline production. Aniline 62-53-3 0.81 14
........................................................................... Benzene 71-43-2 0.14 10
........................................................................... Cyclohexanone 108-94-1 0.36 NA
........................................................................... Diphenylamine (difficult to distinguish 122-39-4 0.92 13
from diphenylnitrosamine
........................................................................... Diphenylnitrosamine (difficult to 86-30-6 0.92 13
distinguish from diphenylamine)
........................................................................... Nitrobenzene 98-95-3 0.068 14
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
------------------
K084 Wastewater treatment sludges generated during the production of veterinary Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
pharmaceuticals from arsenic or organo-arsenic compounds.
------------------
K085 Distillation or fractionation column bottoms from the production of Benzene 71-43-2 0.14 10
chlorobenzenes. Chlorobenzene 108-90-7 0.057 6.0
m-Dichlorobenzene 541-73-1 0.036 6.0
........................................................................... o-Dichlorobenzene 95-50-1 0.088 6.0
........................................................................... p-Dichlorobenzene 106-46-7 0.090 6.0
........................................................................... Hexachlorobenzene 118-74-1 0.055 10
........................................................................... Total PCBs (sum of all PCB isomers, or all 1336-36-3 0.10 10
Aroclors)
........................................................................... Pentachlorobenzene 608-93-5 0.055 10
........................................................................... 1,2,4,5-Tetrachlorobenzene 95-94-3 0.055 14
........................................................................... 1,2,4-Trichlorobenzene 120-82-1 0.055 19
------------------
K086 Solvent wastes and sludges, caustic washes and sludges, or water washes and Acetone 67-64-1 0.28 160
sludges from cleaning tubs and equipment used in the formulation of ink Acetophenone 96-86-2 0.010 9.7
from pigments, driers, soaps, and stabilizers containing chromium and bis(2-Ethylhexyl) phthalate 117-81-7 0.28 28
lead. n-Butyl alcohol 71-36-3 5.6 2.6
........................................................................... Butylbenzyl phthalate 85-68-7 0.017 28
........................................................................... Cyclohexanone 108-94-1 0.36 NA
[[Page 190]]
........................................................................... o-Dichlorobenzene 95-50-1 0.088 6.0
........................................................................... Diethyl phthalate 84-66-2 0.20 28
........................................................................... Dimethyl phthalate 131-11-3 0.047 28
........................................................................... Di-n-butyl phthalate 84-74-2 0.057 28
........................................................................... Di-n-octyl phthalate 117-84-0 0.017 28
........................................................................... Ethyl acetate 141-78-6 0.34 33
........................................................................... Ethylbenzene 100-41-4 0.057 10
........................................................................... Methanol 67-56-1 5.6 NA
........................................................................... Methyl ethyl ketone 78-93-3 0.28 36
........................................................................... Methyl isobutyl ketone 108-10-1 0.14 33
........................................................................... Methylene chloride 75-09-2 0.089 30
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Nitrobenzene 98-95-3 0.068 14
........................................................................... Toluene 108-88-3 0.080 10
........................................................................... 1,1,1-Trichloroethane 71-55-6 0.054 6.0
........................................................................... Trichloroethylene 79-01-6 0.054 6.0
........................................................................... Xylenes-mixed isomers (sum of o-, m-, and 1330-20-7 0.32 30
p-xylene concentrations)
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
K087 Decanter tank tar sludge from coking operations. Acenaphthylene 208-96-8 0.059 3.4
........................................................................... Benzene 71-43-2 0.14 10
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Fluoranthene 206-44-0 0.068 3.4
........................................................................... Indeno(1,2,3-cd)pyrene 193-39-5 0.0055 3.4
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... Toluene 108-88-3 0.080 10
........................................................................... Xylenes-mixed isomers (sum of o, m-, and p- 1330-20-7 0.32 30
xylene concentrations)
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
K088 Spent potliners from primary aluminum reduction. Acenaphthene 83-32-9 0.059 3.4
........................................................................... Anthracene 120-12-7 0.059 3.4
........................................................................... Bemz(a)anthracene 56-55-3 0.059 3.4
........................................................................... Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... Benzo(b)fluoranthene 205-99-2 0.11 6.8
[[Page 191]]
........................................................................... Benzo(k)fluoranthene 207-08-9 0.11 6.8
........................................................................... Benzo(g,h,i)perylene 191-24-2 0.0055 1.8
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Dibenz(a,h)anthracene 53-70-3 0.055 8.2
........................................................................... Fluoranthene 206-44-0 0.068 3.4
........................................................................... Indeno(1,2,3,-c,d)pyrene 193-39-5 0.0055 3.4
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... Pyrene 129-00-0 0.067 8.2
........................................................................... Antimony 7440-36-0 1.9 1.15 mg/L TCLP
........................................................................... Arsenic 7440-38-2 1.4 26.1
........................................................................... Barium 7440-39-3 1.2 21 mg/L TCLP
........................................................................... Beryllium 7440-41-7 0.82 1.22 mg/L TCLP
........................................................................... Cadmium 7440-43-9 0.69 0.11 mg/L TCLP
........................................................................... Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
........................................................................... Mercury 7439-97-6 0.15 0.025 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
........................................................................... Selenium 7782-49-2 0.82 5.7 mg/L TCLP
........................................................................... Silver 7440-22-4 0.43 0.14 mg/L TCLP
........................................................................... Cyanide (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanide (Amenable) \7\ 57-12-5 0.86 30
........................................................................... Fluoride 16984-48-8 35 NA
------------------
K093 Distillation light ends from the production of phthalic anhydride from Phthalic anhydride (measured as Phthalic 100-21-0 0.055 28
ortho-xylene acid or Terephthalic acid)
........................................................................... Phthalic anhydride (measured as Phthalic 85-44-9 0.055 28
acid or Terephthalic acid)
------------------
K094 Distillation bottoms from the production of phthalic anhydride from ortho- Phthalic anhydride (measured as Phthalic 100-21-0 0.055 28
xylene. acid or Terephthalic acid)
........................................................................... Phthalic anhydride (measured as Phthalic 85-44-9 0.055 28
acid or Terephthalic acid)
------------------
K095 Distillation bottoms from the production of 1,1,1-trichloroethane. Hexachloroethane 67-72-1 0.055 30
Pentachloroethane 76-01-7 0.055 6.0
........................................................................... 1,1,1,2-Tetrachloroethane 630-20-6 0.057 6.0
........................................................................... 1,1,2,2-Tetrachloroethane 79-34-6 0.057 6.0
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
........................................................................... 1,1,2-Trichloroethane 79-00-5 0.054 6.0
........................................................................... Trichloroethylene 79-01-1 0.054 6.0
------------------
K096 Heavy ends from the heavy ends column from the production of 1,1,1- m-Dichlorobenzene 541-73-1 0.036 6.0
trichloroethane. Pentachloroethane 76-01-1 0.055 6.0
........................................................................... 1,1,1,2-Tetrachloroethane 630-20-6 0.057 6.0
........................................................................... 1,1,2,2-Tetrachloroethane 79-34-6 0.057 6.0
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
........................................................................... 1,2,4-Trichlorobenzene 120-82-1 0.055 19
........................................................................... 1,1,2-Trichloroethane 79-00-5 0.054 6.0
........................................................................... Trichloroethylene 79-01-6 0.054 6.0
------------------
[[Page 192]]
K097 Vacuum stripper discharge from the chlordane clorinator in the production Chlordane (alpha and gamma isomers) 57-74-9 0.0033 0.26
of chlordane. Heptachlor 76-44-8 0.0012 0.066
........................................................................... Heptachlor epoxide 1024-57-3 0.016 0.066
........................................................................... Hexachlorocyclopentadiene 77-47-4 0.057 2.4
------------------
K098 Untreated process wastewater from the production of toxaphene. Toxaphene 8001-35-2 0.0095 2.6
------------------
K099 Untreated wastewater from the production of 2,4-D. 2,4-Dichlorophenoxyacetic acid 94-75-7 0.72 10
........................................................................... HxCDDs (All Hexachlorodibenzo-p-dioxins) NA 0.000063 0.001
........................................................................... HxCDFs (All Hexachlorodibenzofurans) NA 0.000063 0.001
........................................................................... PeCDDs (All Pentachlorodibenzo-p-dioxins) NA 0.000063 0.001
........................................................................... PeCDFs (All Pentachlorodibenzofurans) NA 0.000035 0.001
........................................................................... TCDDs (All Tetrachlorodibenzo-p-dioxins) NA 0.000063 0.001
........................................................................... TCDFs (All Tetrachlorodibenzofurans) NA 0.000063 0.001
------------------
K100 Waste leaching solution from acid leaching of emission control dust/sludge Cadmium 7440-43-9 0.69 0.11 mg/L TCLP
from secondary lead smelting. Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
K101 Distillation tar residues from the distillation of aniline-based compounds o-Nitroaniline 88-74-4 0.27 14
in the production of veterinary pharmaceuticals from arsenic or organo- Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
arsenic compounds. Cadmium 7440-43-9 0.69 NA
........................................................................... Lead 7439-92-1 0.69 NA
........................................................................... Mercury 7439-97-6 0.15 NA
------------------
K102 Residue from the use of activated carbon for decolorization in the o-Nitrophenol 88-75-5 0.028 13
production of veterinary pharmaceuticals from arsenic or organo-arsenic Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
compounds. Cadmium 7440-43-9 0.69 NA
........................................................................... Lead 7439-92-1 0.69 NA
........................................................................... Mercury 7439-97-6 0.15 NA
------------------
K103 Process residues from aniline extraction from the production of aniline. Aniline 62-53-3 0.81 14
Benzene 71-43-2 0.14 10
[[Page 193]]
........................................................................... 2,4-Dinitrophenol 51-28-5 0.12 160
........................................................................... Nitrobenzene 98-95-3 0.068 14
........................................................................... Phenol 108-95-2 0.039 6.2
------------------
K104 Combined wastewater streams generated from nitrobenzene/aniline production. Aniline 62-53-3 0.81 14
Benzene 71-43-2 0.14 10
........................................................................... 2,4-Dinitrophenol 51-28-5 0.12 160
........................................................................... Nitrobenzene 98-95-3 0.068 14
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
------------------
K105 Separated aqueous stream from the reactor product washing step in the Benzene 71-43-2 0.14 10
production of chlorobenzenes. Chlorobenzene 108-90-7 0.057 6.0
........................................................................... 2-Chlorophenol 95-57-8 0.044 5.7
........................................................................... o-Dichlorobenzene 95-50-1 0.088 6.0
........................................................................... p-Dichlorobenzene 106-46-7 0.090 6.0
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... 2,4,5-Trichlorophenol 95-95-4 0.18 7.4
........................................................................... 2,4,6-Trichlorophenol 88-06-2 0.035 7.4
------------------
K106 K106 (wastewater treatment sludge from the mercury cell process in chlorine Mercury 7439-97-6 NA RMERC
production) nonwastewaters that contain greater than or equal to 260 mg/kg
total mercury.
------------------------------------------------------------------------------
K106 (wastewater treatment sludge from the mercury cell process in chlorine Mercury 7439-97-6 NA 0.20 mg/L TCLP
production) nonwastewaters that contain less than 260 mg/kg total mercury
that are residues from RMERC.
------------------------------------------------------------------------------
Other K106 nonwastewaters that contain less than 260 mg/kg total mercury Mercury 7439-97-6 NA 0.025 mg/L TCLP
and are not residues from RMERC.
------------------------------------------------------------------------------
All K106 wastewaters. Mercury 7439-97-6 0.15 NA
------------------
K107 Column bottoms from production separation from the production of 1,1- NA NA CMBST; or CHOXD fb CMBST
dimethylhydrazine (UDMH) from carboxylic acid hydrazides. CARBN; or BIODG fb
CARBN
------------------
K108 Condensed column overheads from product separation and condensed reactor NA NA CMBST; or CHOXD fb CMBST
vent gases from the production of 1,1-dimethylhydrazine (UDMH) from CARBN; or BIODG fb
carboxylic acid hydrazides. CARBN
------------------
K109 Spent filter cartridges from product purification from the production of NA NA CMBST; or CHOXD fb CMBST
1,1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides. CARBN; or BIODG fb
CARBN
------------------
[[Page 194]]
K110 Condensed column overheads from intermediate separation from the production NA NA CMBST; or CHOXD fb CMBST
of 1,1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides. CARBN; or BIODG fb
CARBN
------------------
K111 Product washwaters from the production of dinitrotoluene via nitration of 2,4-Dinitrotoluene 121-1-2 0.32 140
toluene. 2,6-Dinitrotoluene 606-20-2 0.55 28
------------------
K112 Reaction by-product water from the drying column in the production of NA NA CMBST; or CHOXD fb CMBST
toluenediamine via hydrogenation of dinitrotoluene. CARBN; or BIODG fb
CARBN
------------------
K113 Condensed liquid light ends from the purification of toluenediamine in the NA NA CARBN; or CMBST CMBST
production of toluenediamine via hydrogenation of dinitrotoluene.
------------------
K114 Vicinals from the purification of toluenediamine in the production of NA NA CARBN; or CMBST CMBST
toluenediamine via hydrogenation of dinitrotolune.
------------------
K115 Heavy ends from the purification of toluenediamine in the production of Nickel 7440-02-2 3.98 11 mg/L TCLP
toluenediamine via hydrogenation of dinitrotoluene. NA NA CARBN; or CMBST CMBST
------------------
K116 Organic condensate from the solvent recovery column in the production of NA NA CARBN; or CMBST CMBST
toluene diisocyanate via phosgenation of toluenediamine.
------------------
K117 Wastewater from the reactor vent gas scrubber in the production of ethylene Methyl bromide (Bromomethane) 74-83-9 0.11 15
dibromide via bromination of ethene. Chloroform ............ .................. ..................
67-66-3 0.046 6.0
........................................................................... Ethylene dibromide (1,2-Dibromoethane) 106-93-4 0.028 15
------------------
K118 Spent absorbent solids from purification of ethylene dibromide in the Methyl bromide (Bromomethane) 74-83-9 0.11 15
production of ethylene dibromide via bromination of ethene. Chloroform ............ .................. ..................
67-66-3 0.046 6.0
........................................................................... Ethylene dibromide (1,2,-Dibromoethane) 106-93-4 0.028 15
------------------
[[Page 195]]
K123 Process wastewater (including supernates, filtrates, and washwaters) from NA NA CMBST; or CHOXD fb CMBST
the production of ethylenebisdithiocarbamic acid and its salts. (BIODG or CARBN)
------------------
K124 Reactor vent scrubber water from the production of NA NA CMBST; or CHOXD fb CMBST
ethylenebisdithiocarbamic acid and its salts. (BIODG or CARBN)
------------------
K125 Filtration, evaporation, and centrifugation solids from the production of NA NA CMBST; or CHOXD fb CMBST
ethylenebisdithiocarbamic acid and its salts. (BIODG or CARBN)
------------------
K126 Baghouse dust and floor sweepings in milling and packaging operations from NA NA CMBST; or CHOXD fb CMBST
the production or formulation of ethylenebisdithiocarbamic acid and its (BIODG or CARBN)
salts.
------------------
K131 Wastewater from the reactor and spent sulfuric acid from the acid dryer Methyl bromide (Bromomethane) 74-83-9 0.11 15
from the production of methyl bromide.
------------------
K132 Spent absorbent and wastewater separator solids from the production of Methyl bromide (Bromomethane) 74-83-9 0.11 15
methyl bromide.
------------------
K136 Still bottoms from the purification of ethylene dibromide in the production Methyl bromide (Bromomethane) 74-83-9 0.11 15
of ethylene dibromide via bromination of ethene. Chloroform ............ .................. ..................
67-66-3 0.46 6.0
........................................................................... Ethylene dibromide (1,2-Dibromoethane) 106-93-4 0.028 15
------------------
K141 Process residues from the recovery of coal tar, including, but not limited Benzene 71-43-2 0.14 10
to, collecting sump residues from the production of coke or the recovery Benz(a)anthracene 56-55-3 0.059 3.4
of coke by-products produced from coal. This listing does not include K087 Benzo(a)pyrene 50-2-8 0.061 3.4
(decanter tank tar sludge from coking operations). Benzo(b)fluoranthene (difficult to 205-99-2 0.11 6.8
distinguish from benzo(k)fluoranthene)
........................................................................... Benzo(k)fluoranthene (difficult to 207-08-9 0.11 6.8
distinguish from benzo(b)fluoranthene)
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Dibenz(a,h)anthracene 53-70-3 0.055 8.2
........................................................................... Indeno(1,2,3-cd)pyrene 193-39-5 0.0055 3.4
------------------
K142 Tar storage tank residues from the production of coke from coal or from the Benzene 71-43-2 0.14 10
recovery of coke by-products produced from coal. Benz(a)anthracene 56-55-3 0.059 3.4
........................................................................... Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... Benzo(b)fluoranthene (difficult to 205-99-2 0.11 6.8
distinguish from benzo(k)fluoranthene)
........................................................................... Benzo(k)fluoranthene (difficult to 207-08-9 0.11 6.8
distinguish from benzo(b)fluoranthene)
[[Page 196]]
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Dibenz(a,h)anthracene 53-70-3 0.055 8.2
........................................................................... Indeno(1,2,3-cd)pyrene 193-39-5 0.0055 3.4
------------------
K143 Process residues from the recovery of light oil, including, but not limited Benzene 71-43-2 0.14 10
to, those generated in stills, decanters, and wash oil recovery units from Benz(a)anthracene 56-55-3 0.059 3.4
the recovery of coke by-products produced from coal. Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... Benzo(b)fluoranthene (difficult to 205-99-2 0.11 6.8
distinguish from benzo(k)fluoranthene)
........................................................................... Benzo(k)flouranthene (difficult to 207-08-9 0.11 6.8
distinguish from benzo(b)fluoranthene
........................................................................... Chrysene 218-01-9 0.059 3.4
------------------
K144 Wastewater sump residues from light oil refining, including, but not Benzene 71-43-2 0.14 10
limited to, intercepting or contamination sump sludges from the recovery Benz(a)pyrene 56-55-3 0.059 3.4
of coke by-products produced from coal. Benzo(a)anthracene 50-32-8 0.061 3.4
........................................................................... Benzo(b)fluoranthene (difficult to 205-99-2 0.11 6.8
distinguish from benzo(k)fluoranthene)
........................................................................... Benzo(k)fluoranthene (difficult to 207-08-9 0.11 6.8
distinguish from benzo(b)fluoranthene)
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Dibenz(a,h)anthracene 53-70-3 0.055 8.2
------------------
K145 Residues from naphthalene collection and recovery operations from the Benzene 71-43-2 0.14 10
recovery of coke by-products produced from coal. Benz(a)anthracene 56-55-3 0.059 3.4
........................................................................... Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Dibenz(a,h)anthracene 53-70-3 0.055 8.2
........................................................................... Naphthalene 91-20-3 0.059 5.6
------------------
K147 Tar storage tank residues from coal tar refining. Benzene 71-43-2 0.14 10
........................................................................... Benz(a)anthracene 56-55-3 0.059 3.4
........................................................................... Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... Benzo(b)fluoranthene (difficult to 205-99-2 0.11 6.8
distinguish from benzo(k)fluoranthene)
........................................................................... Benzo(k)fluoranthene (difficult to 207-08-9 0.11 6.8
distinguish from benzo(b)fluoranthene)
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Dibenz(a,h)anthracene 53-70-3 0.055 8.2
[[Page 197]]
........................................................................... Indeno(1,2,3-cd)pyrene 193-39-5 0.0055 3.4
------------------
K148 Residues from coal tar distillation, including, but not limited to, still Benz(a)anthracene 56-55-3 0.059 3.4
bottoms. Benzo(a)pyrene 50-32-8 0.061 3.4
........................................................................... Benzo(b)fluoranthene (difficult to 205-99-2 0.11 6.8
distinguish from benzo(k)fluoranthene)
........................................................................... Benzo(k)fluoranthene (difficult to 207-08-9 0.11 6.8
distinguish from benzo(b)fluoranthene)
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Dibenz(a,h)anthracene 53-70-3 0.055 8.2
........................................................................... Indeno(1,2,3-cd)pyrene 193-39-5 0.0055 3.4
------------------
K149 Distillation bottoms from the production of alpha- (or methyl-) chlorinated Chlorobenzene 108-90-7 0.057 6.0
toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with Chloroform 67-66-3 0.046 6.0
mixtures of these functional groups. (This waste does not include still Chloromethane 74-87-3 0.19 30
bottoms from the distillations of benzyl chloride.) p-Dichlorobenzene 106-46-7 0.090 6.0
Hexachlorobenzene 118-74-1 0.055 10
........................................................................... Pentachlorobenzene 608-93-5 0.055 10
........................................................................... 1,2,4,5-Tetrachlorobenzene 95-94-3 0.055 14
........................................................................... Toluene 108-88-3 0.080 10
------------------
K150 Organic residuals, excluding spent carbon adsorbent, from the spent Carbon tetrachloride 56-23-5 0.057 6.0
chlorine gas and hydrochloric acid recovery processes associated with the Chloroform 67-66-3 0.046 6.0
production of alpha- (or methyl-) chlorinated toluenes, ring-chlorinated Chloromethane 74-87-3 0.019 30
toluenes, benzoyl chlorides, and compounds with mixtures of these p-Dichlorobenzene 106-46-7 0.090 6.0
functional groups. Hexachlorobenzene 118-74-1 0.055 10
........................................................................... Pentachlorobenzene 608-93-5 0.055 10
........................................................................... 1,2,4,5-Tetrachlorobenzene 95-94-3 0.055 14
........................................................................... 1,1,2,2-Tetrachloroethane 79-34-5 0.057 6.0
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
........................................................................... 1,2,4-Trichlorobenzene 120-82-1 0.055 19
------------------
K151 Wastewater treatment sludges, excluding neutralization and biological Benzene 71-43-2 0.14 10
sludges, generated during the treatment of wastewaters from the production Carbon tetrachloride 56-23-5 0.057 6.0
of alpha- or (methyl-) chlorinated toluenes, ring-chlorinated toluenes, Chloroform 67-66-3 0.046 6.0
benzoyl chlorides, and compounds with mixtures of these functional groups. Hexachlorobenzene 118-74-1 0.055 10
Pentachlorobenzene 608-93-5 0.055 10
........................................................................... 1,2,4,5-Tetrachlorobenzene 95-94-3 0.055 14
........................................................................... Tetrachloroethylene 127-18-4 0.056 6.0
........................................................................... Toluene 108-88-3 0.080 10
------------------
K156 Organic waste (including heavy ends, still bottoms, light ends, spent Acetonitrile 75-05-8 5.6 1.8
solvents, filtrates, and decantates) from the production of carbamates and Acetophenone 96-86-2 0.010 9.7
carbamoyl oximes. Aniline 62-53-3 0.81 14
........................................................................... Benomyl 17804-35-2 0.056 1.4
........................................................................... Benzene 71-43-2 0.14 10
........................................................................... Carbaryl 63-25-2 0.006 0.14
........................................................................... Carbenzadim 10605-21-7 0.056 1.4
........................................................................... Carbofuran 1563-66-2 0.006 0.14
........................................................................... Carbosulfan 55285-14-8 0.028 1.4
[[Page 198]]
........................................................................... Chlorobenzene 108-90-7 0.057 6.0
........................................................................... Chloroform 67-66-3 0.046 6.0
........................................................................... o-Dichlorobenzene 95-50-1 0.088 6.0
........................................................................... Methomyl 16752-77-5 0.028 0.14
........................................................................... Methylene chloride 75-09-2 0.089 30
........................................................................... Methyl ethyl ketone 78-93-3 0.28 36
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Phenol 108-95-2 0.039 6.2
........................................................................... Pyridine 110-86-1 0.014 16
........................................................................... Toluene 108-88-3 0.080 10
........................................................................... Triethylamine 101-44-8 0.081 1.5
------------------
K157 Wastewaters (including scrubber waters, condenser waters, washwaters, and Carbon tetrachloride 56-23-5 0.057 6.0
separation waters) from the production of carbamates and carbamoyl oximes. Chloroform 67-66-3 0.046 6.0
Chloromethane 74-87-3 0.19 30
Methomyl 16752-77-5 0.028 0.14
........................................................................... Methylene chloride 75-09-2 0.089 30
........................................................................... Methyl ethyl ketone 78-93-3 0.28 36
........................................................................... Pyridine 110-86-1 0.014 16
........................................................................... Triethylamine 121-44-8 0.081 1.5
------------------
K158 Bag house dusts and filter/separation solids from the production of Benomyl 17804-35-2 0.056 1.4
carbamates and carbamoyl oximes. Benzene 71-43-2 0.14 10
........................................................................... Carbenzadim 10605-21-7 0.056 1.4
........................................................................... Carbofuran 1563-66-2 0.006 0.14
........................................................................... Carbosulfan 55285-14-8 0.028 1.4
........................................................................... Chloroform 67-66-3 0.046 6.0
........................................................................... Methylene chloride 75-09-2 0.089 30
........................................................................... Phenol 108-95-2 0.039 6.2
------------------
K159 Organics from the treatment of thiocarbamate wastes. Benzene 71-43-2 0.14 10
........................................................................... Butylate 2008-41-5 0.042 1.4
........................................................................... EPTC (Eptam) 759-94-4 0.042 1.4
........................................................................... Molinate 2212-67-1 0.042 1.4
........................................................................... Pebulate 1114-71-2 0.042 1.4
........................................................................... Vernolate 1929-77-7 0.042 1.4
------------------
[[Page 199]]
K161 Purification solids (including filtration, evaporation, and centrifugation Antimony 7440-36-0 1.9 1.15 mg/L TCLP
solids), baghouse dust and floor sweepings from the production of Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
dithiocarbamate acids and their salts. Carbon disulfide 75-15-0 3.8 4.8 mg/L TCLP
........................................................................... Dithiocarbamates (total) NA 0.028 28
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11.0 mg/L TCLP
........................................................................... Selenium 7782-49-2 0.82 5.7 mg/L TCLP
------------------
K169 Crude oil tank sediment from petroleum refining operations. Benz(a)anthracene 56-55-3 0.059 3.4
........................................................................... Benzene 71-43-2 0.14 10
........................................................................... Benzo(g,h,i)perylene 191-24-2 0.0055 1.8
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Ethyl benzene 100-41-4 0.057 10
........................................................................... Fluorene 86-73-7 0.059 3.4
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Phenanthrene 81-05-8 0.059 5.6
........................................................................... Pyrene 129-00-0 0.067 8.2
........................................................................... Toluene (Methyl Benzene) 108-88-3 0.080 10
........................................................................... Xylene(s) (Total) 1330-20-7 0.32 30
------------------
K170 Clarified slurry oil sediment from petroleum refining operations. Benz(a)anthracene 56-55-3 0.059 3.4
Benzene 71-43-2 0.14 10
........................................................................... Benzo(g,h,i)perylene 191-24-2 0.0055 1.8
........................................................................... Chrysene 218-01-9 0.059 3.4
........................................................................... Dibenz(a,h)anthracene 53-70-3 0.055 8.2
........................................................................... Ethyl benzene 100-41-4 0.057 10
........................................................................... Fluorene 86-73-7 0.059 3.4
........................................................................... Indeno(1,3,4-cd)pyrene 193-39-5 0.0055 3.4
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Phenanthrene 81-05-8 0.059 5.6
........................................................................... Pyrene 129-00-0 0.067 8.2
........................................................................... Toluene (Methyl Benzene) 108-88-3 0.080 10
........................................................................... Xylene(s) (Total) 1330-20-7 0.32 30
------------------
K171 Spent hydrotreating catalyst from petroleum refining operations, including Benz(a)anthracene 56-55-3 0.059 3.4
guard beds used to desulfurize feeds to other catalytic reactors (this Benzene 71-43-2 0.14 10
listing does not include inert support media). Chrysene 218-01-9 0.059 3.4
Ethyl benzene 100-41-4 0.057 10
........................................................................... Naphthalene 91-20-3 0.059 5.6
........................................................................... Phenanthrene 81-05-8 0.059 5.6
........................................................................... Pyrene 129-00-0 0.67 8.2
........................................................................... Toluene (Methyl Benzene) 108-88-3 0.080 10
........................................................................... Xylene(s) (Total) 1330-20-7 0.32 30
........................................................................... Arsenic 7740-38-2 1.4 5 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11.0 mg/L TCLP
........................................................................... Vanadium 7440-62-2 4.3 1.6 mg/L TCLP
........................................................................... Reactive sulfides NA DEACT DEACT
------------------
[[Page 200]]
K172 Spent hydrorefining catalyst from petroleum refining operations, including Benzene 71-43-2 0.14 10
guard beds used to desulfurize feeds to other catalytic reactors (this Ethyl benzene 100-41-4 0.57 10
listing does not include inert support media.). Toluene (Methyl Benzene) 108-88-3 0.080 10
Xylene(s) (Total) 1330-20-7 0.32 30
........................................................................... Antimony 7740-36-0 1.9 1.15 mg/L TCLP
........................................................................... Arsenic 7740-38-2 1.4 5 mg/L TCLP
........................................................................... Nickel 7440-02-0 3.98 11.0 mg/L TCLP
........................................................................... Vanadium 7440-62-2 4.3 1.6 mg/L TCLP
........................................................................... Reactive sulfides NA DEACT DEACT
------------------
K174 Wastewater treatment sludges from the production of ethylene dichloride or 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin 35822-46-9 0.000035 or CMBST 0.0025 or CMBST
vinyl chloride monomer. (1,2,3,4,6,7,8-HpCDD) \11\ \11\
........................................................................... 1,2,3,4,6,7,8-Heptachlorodibenzofuran 67562-39-4 0.000035 or CMBST 0.0025 or CMBST
(1,2,3,4,6,7,8-HpCDF) \11\ \11\
........................................................................... 1,2,3,4,7,8,9-Heptachlorodibenzofuran 55673-89-7 0.000035 or CMBST 0.0025 or CMBST
(1,2,3,4,7,8,9-HpCDF) \11\ \11\
........................................................................... HxCDDs (All Hexachlorodibenzo-p-dioxins) 34465-46-8 0.000063 or CMBST 0.001 or CMBST
\11\ \11\
........................................................................... HxCDFs (All Hexachlorodibenzofurans) 55684-94-1 0.000063 or CMBST 0.001 or CMBST
\11\ \11\
........................................................................... 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin 3268-87-9 0.000063 or CMBST 0.005 or CMBST
(OCDD) \11\ \11\
........................................................................... 1,2,3,4,6,7,8,9-Octachlorodibenzofuran 39001-02-0 0.000063 or CMBST 0.005 or CMBST
(OCDF) \11\ \11\
........................................................................... PeCDDs (All Pentachlorodibenzo-p-dioxins 36088-22-9 0.000063 or CMBST 0.001 or CMBST
\11\ \11\
........................................................................... PeCDFs (All Pentachlorodibenzofurans) 30402-15-4 0.000035 or CMBST 0.001 or CMBST
\11\ \11\
........................................................................... TCDDs (All tetachlorodibenzo-p-dioxins) 41903-57-5 0.000063 or CMBST 0.001 or CMBST
\11\ \11\
........................................................................... TCDFs (All tetrachlorodibenzofurans) 55722-27-5 0.000063 or CMBST 0.001 or CMBST
\11\ \11\
........................................................................... Arsenic 7440-36-0 1.4 5.0 mg/L TCLP
------------------
K175 Wastewater treatment sludge from the production of vinyl chloride monomer Mercury \12\ 7438-97-6 NA 0.025 mg/L TCLP
using mercuric chloride catalyst in an acetylene-based process pH \12\ NA pH[le]6.0
------------------------------------------------------------------------------
All K175 wastewaters Mercury 7438-97-6 0.15 NA
------------------
[[Page 201]]
K176 Baghouse filters from the production of antimony oxide, including filters Antimony 7440-36-0 1.9 1.15 mg/L TCLP
from the production of intermediates (e.g., antimony metal or crude Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
antimony oxide) Cadmium 7440-43-9 0.69 0.11 mg/L TCLP
Lead 7439-92-1 0.69 0.75 mg/L TCLP
Mercury 7439-97-6 0.15 0.025 mg/L TCLP
K177 Slag from the production of antimony oxide that is speculatively Antimony 7440-36-0 1.9 1.15 mg/L TCLP
accumulated or disposed, including slag from the production of Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
intermediates (e.g., antimony metal or crude antimony oxide) Lead 7439-92-1 0.69 0.75 mg/L TCLP
K178 Residues from manufacturing and manufacturing-site storage of ferric 1,2,3,4,6,7,8- Heptachlorodibenzo-p-dioxin 35822-39-4 0.000035 or CMBST 0.0025 or CMBST
chloride from acids formed during the production of titanium dioxide using (1,2,3,4,6,7,8-HpCDD) ............ \11\ \11\
the chloride-ilmenite process. .......................................... ............ .................. ..................
1,2,3,4,6,7,8- 67562-39-4 0.000035 or CMBST 0.0025 or CMBST
Heptachlorodibenzofuran (1,2,3,4,6,7,8- ............ \11\ \11\
HpCDF) ............ .................. ..................
.......................................... ............ .................. ..................
1,2,3,4,7,8,9- 55673-89-7 0.000035 or CMBST 0.0025 or CMBST
Heptachlorodibenzofuran (1,2,3,4,7,8,9- \11\ \11\
HpCDF) .................. ..................
..........................................
HxCDDs (All Hexachlorodibenzo-p-dioxins) 34465-46-8 0.000063 or CMBST 0.001 or CMBST
\11\ \11\
HxCDFs (All Hexachlorodibenzo-furans) 55684-94-1 0.000063 or CMBST 0.001 or CMBST
\11\ \11\
1,2,3,4,6,7,8,9- Octachlorodibenzo-p- 3268-87-9 0.000063 or CMBST 0.005 or CMBST
dioxin (OCDD) \11\ \11\
1,2,3,4,6,7,8,9- Octachlorodibenzofuran 39001-02-0 0.000063 or CMBST 0.005 or CMBST
(OCDF) \11\ \11\
PeCDDs (All Pentachlorodibenzo-p-dioxins) 36088-22-9 0.000063 or CMBST 0.001 or CMBST
\11\ \11\
PeCDFs (All Pentachlorodibenzo-furans) 30402-15-4 0.000035 or CMBST 0.001 or CMBST
\11\ \11\
TCDDs (All tetrachlorodibenzo-p-dioxins) 41903-57-5 0.000063 or CMBST 0.001 or CMBST
\11\ \11\
TCDFs (All tetrachlorodibenzo-furans) 55722-27-5 0.000063 or CMBST 0.001 or CMBST
\11\ \11\
Thallium 7440-28-0 1.4 0.20 mg/L TCLP
P001 Warfarin, & salts, when present at concentrations greater than 0.3% Warfarin 81-81-2 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
[[Page 202]]
P002 1-Acetyl-2-thiourea 1-Acetyl-2-thiourea 591-08-2 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P003 Acrolein Acrolein 107-02-8 0.29 CMBST
------------------
P004 Aldrin Aldrin 309-00-2 0.021 0.066
------------------
P005 Allyl alcohol Allyl alcohol 107-18-6 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P006 Aluminum phosphide Aluminum phosphide 20859-73-8 CHOXD; CHRED; or CHOXD; CHRED; or
CMBST CMBST
------------------
P007 5-Aminomethyl 3-isoxazolol 5-Aminomethyl 3-isoxazolol 2763-96-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P008 4-Aminopyridine 4-Aminopyridine 504-24-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P009 Ammonium picrate Ammonium picrate 131-74-8 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
P010 Arsenic acid Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
------------------
P011 Arsenic pentoxide Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
------------------
P012 Arsenic trioxide Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
------------------
P013 Barium cyanide Barium 7440-39-3 NA 21 mg/L TCLP
........................................................................... Cyanides (Total) \7\ 57-12-5 1.2 590
[[Page 203]]
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
------------------
P014 Thiophenol (Benzene thiol) Thiophenol (Benzene thiol) 108-98-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P015 Beryllium dust Beryllium 7440-41-7 RMETL; or RTHRM RMETL; or RTHRM
------------------
P016 Dichloromethyl ether (Bis(chloromethyl)ether) Dichloromethyl ether 542-88-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P017 Bromoacetone Bromoacetone 598-31-2 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P018 Brucine Brucine 357-57-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P020 2-sec-Butyl-4,6-dinitrophenol (Dinoseb) 2-sec-Butyl-4,6-dinitrophenol (Dinoseb) 88-85-7 0.066 2.5
------------------
P021 Calcium cyanide Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
------------------
P022 Carbon disulfide Carbon disulfide 75-15-0 3.8 CMBST
........................................................................... Carbon disulfide; alternate \6\ standard 75-15-0 NA 4.8 mg/L TCLP
for nonwastewaters only
------------------
P023 Chloroacetaldehyde Chloroacetaldehyde 107-20-0 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P024 p-Chloroaniline p-Chloroaniline 106-47-8 0.46 16
------------------
P026 1-(o-Chlorophenyl)thiourea 1-(o-Chlorophenyl)thiourea 5344-82-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
[[Page 204]]
P027 3-Chloropropionitrile 3-Chloropropionitrile 542-76-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P028 Benzyl chloride Benzyl chloride 100-44-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P029 Copper cyanide Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
------------------
P030 Cyanides (soluble salts and complexes) Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
------------------
P031 Cyanogen Cyanogen 460-19-5 CHOXD; WETOX; or CHOXD; WETOX; or
CMBST CMBST
------------------
P033 Cyanogen chloride Cyanogen chloride 506-77-4 CHOXD; WETOX; or CHOXD; WETOX; or
CMBST CMBST
------------------
P034 2-Cyclohexyl-4,6-dinitrophenol 2-Cyclohexyl-4,6-dinitrophenol 131-89-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P036 Dichlorophenylarsine Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
------------------
P037 Dieldrin Dieldrin 60-57-1 0.017 0.13
------------------
P038 Diethylarsine Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
------------------
P039 Disulfoton Disulfoton 298-04-4 0.017 6.2
------------------
P040 0,0-Diethyl O-pyrazinyl phosphorothioate 0,0-Diethyl O-pyrazinyl phosphorothioate 297-97-2 CARBN; or CMBST CMBST
------------------
[[Page 205]]
P041 Diethyl-p-nitrophenyl phosphate Diethyl-p-nitrophenyl phosphate 311-45-5 CARBN; or CMBST CMBST
------------------
P042 Epinephrine Epinephrine 51-43-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P043 Diisopropylfluorophosphate (DFP) Diisopropylfluorophosphate (DFP) 55-91-4 CARBN; or CMBST CMBST
------------------
P044 Dimethoate Dimethoate 60-51-5 CARBN; or CMBST CMBST
------------------
P045 Thiofanox Thiofanox 39196-18-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P046 alpha, alpha-Dimethylphenethylamine alpha, alpha-Dimethylphenethylamine 122-09-8 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P047 4,6-Dinitro-o-cresol 4,6-Dinitro-o-cresol 543-52-1 0.28 160
------------------------------------------------------------------------------
4,6-Dinitro-o-cresol salts NA NA (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P048 2,4-Dinitrophenol 2,4-Dinitrophenol 51-28-5 0.12 160
------------------
P049 Dithiobiuret Dithiobiuret 541-53-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P050 Endosulfan Endosulfan I 939-98-8 0.023 0.066
........................................................................... Endosulfan II 33213-6-5 0.029 0.13
........................................................................... Endosulfan sulfate 1031-07-8 0.029 0.13
------------------
P051 Endrin Endrin 72-20-8 0.0028 0.13
........................................................................... Endrin aldehyde 7421-93-4 0.025 0.13
------------------
P054 Aziridine Aziridine 151-56-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
[[Page 206]]
P056 Fluorine Fluoride (measured in wastewaters only) 16984-48-8 35 ADGAS fb NEUTR
------------------
P057 Fluoroacetamide Fluoroacetamide 640-19-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P058 Fluoroacetic acid, sodium salt Fluoroacetic acid, sodium salt 62-74-8 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P059 Heptachlor Heptachlor 76-44-8 0.0012 0.066
........................................................................... Heptachlor epoxide 1024-57-3 0.016 0.066
------------------
P060 Isodrin Isodrin 465-73-6 0.021 0.066
------------------
P062 Hexaethyl tetraphosphate Hexaethyl tetraphosphate 757-58-4 CARBN; or CMBST CMBST
------------------
P063 Hydrogen cyanide Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
------------------
P064 Isocyanic acid, ethyl ester Isocyanic acid, ethyl ester 624-83-9 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P065 Mercury fulminate nonwastewaters, regardless of their total mercury Mercury 7439-97-6 NA IMERC
content, that are not incinerator residues or are not residues from RMERC.
------------------------------------------------------------------------------
Mercury fulminate nonwastewaters that are either incinerator residues or Mercury 7439-97-6 NA RMERC
are residues from RMERC; and contain greater than or equal to 260 mg/kg
total mercury.
------------------------------------------------------------------------------
Mercury fulminate nonwastewaters that are residues from RMERC and contain Mercury 7439-97-6 NA 0.20 mg/L TCLP
less than 260 mg/kg total mercury.
------------------------------------------------------------------------------
[[Page 207]]
Mercury fulminate nonwastewaters that are incinerator residues and contain Mercury 7439-97-6 NA 0.025 mg/L TCLP
less than 260 mg/kg total mercury.
------------------------------------------------------------------------------
All mercury fulminate wastewaters. Mercury 7439-97-6 0.15 NA
------------------
P066 Methomyl Methomyl 16752-77-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P067 2-Methyl-aziridine 2-Methyl-aziridine 75-55-8 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P068 Methyl hydrazine Methyl hydrazine 60-34-4 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
P069 2-Methyllactonitrile 2-Methyllactonitrile 75-86-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P070 Aldicarb Aldicarb 116-06-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P071 Methyl parathion Methyl parathion 298-00-0 0.014 4.6
------------------
P072 1-Naphthyl-2-thiourea 1-Naphthyl-2-thiourea 86-88-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P073 Nickel carbonyl Nickel 7440-02-0 3.98 11 mg/L TCLP
------------------
P074 Nickel cyanide Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
........................................................................... Nickel 7440-02-0 3.98 11 mg/L TCLP
------------------
P075 Nicotine and salts Nicotine and salts 54-11-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P076 Nitric oxide Nitric oxide 10102-43-9 ADGAS ADGAS
------------------
P077 p-Nitroaniline p-Nitroaniline 100-01-6 0.028 28
------------------
[[Page 208]]
P078 Nitrogen dioxide Nitrogen dioxide 10102-44-0 ADGAS ADGAS
------------------
P081 Nitroglycerin Nitroglycerin 55-63-0 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
P082 N-Nitrosodimethylamine N-Nitrosodimethylamine 62-75-9 0.40 2.3
------------------
P084 N-Nitrosomethylvinylamine N-Nitrosomethylvinylamine 4549-40-0 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P085 Octamethylpyrophosphoramide Octamethylpyrophosphoramide 152-16-9 CARBN; or CMBST CMBST
------------------
P087 Osmium tetroxide Osmium tetroxide 20816-12-0 RMETL; or RTHRM RMETL; or RTHRM
------------------
P088 Endothall Endothall 145-73-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P089 Parathion Parathion 56-38-2 0.014 4.6
------------------
P092 Phenyl mercuric acetate nonwastewaters, regardless of their total mercury Mercury 7439-97-6 NA IMERC; or RMERC
content, that are not incinerator residues or are not residues from RMERC.
------------------------------------------------------------------------------
Phenyl mercuric acetate nonwastewaters that are either incinerator residues Mercury 7439-97-6 NA RMERC
or are residues from RMERC; and still contain greater than or equal to 260
mg/kg total mercury.
------------------------------------------------------------------------------
Phenyl mercuric acetate nonwastewaters that are residues from RMERC and Mercury 7439-97-6 NA 0.20 mg/L TCLP
contain less than 260 mg/kg total mercury.
------------------------------------------------------------------------------
Phenyl mercuric acetate nonwastewaters that are incinerator residues and Mercury 7439-97-6 NA 0.025 mg/L TCLP
contain less than 260 mg/kg total mercury.
------------------------------------------------------------------------------
[[Page 209]]
All phenyl mercuric acetate wastewaters. Mercury 7439-97-6 0.15 NA
------------------
P093 Phenylthiourea Phenylthiourea 103-85-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P094 Phorate Phorate 298-02-2 0.021 4.6
------------------
P095 Phosgene Phosgene 75-44-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P096 Phosphine Phosphine 7803-51-2 CHOXD; CHRED; or CHOXD; CHRED; or
CMBST CMBST
------------------
P097 Famphur Famphur 52-85-7 0.017 15
------------------
P098 Potassium cyanide. Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
------------------
P099 Potassium silver cyanide Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
........................................................................... Silver 7440-22-4 0.43 0.14 mg/L TCLP
------------------
P101 Ethyl cyanide (Propanenitrile) Ethyl cyanide (Propanenitrile) 107-12-0 0.24 360
------------------
P102 Propargyl alcohol Propargyl alcohol 107-19-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P103 Selenourea Selenium 7782-49-2 0.82 5.7 mg/L TCLP
------------------
P104 Silver cyanide Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
........................................................................... Silver 7440-22-4 0.43 0.14 mg/L TCLP
------------------
P105 Sodium azide Sodium azide 26628-22-8 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
P106 Sodium cyanide Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
------------------
P108 Strychnine and salts Strychnine and salts 57-24-9 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
[[Page 210]]
P109 Tetraethyldithiopyrophosphate Tetraethyldithiopyrophosphate 3689-24-5 CARBN; or CMBST CMBST
------------------
P110 Tetraethyl lead Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
P111 Tetraethylpyrophosphate Tetraethylpyrophosphate 107-49-3 CARBN; or CMBST CMBST
------------------
P112 Tetranitromethane Tetranitromethane 509-14-8 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
P113 Thallic oxide Thallium (measured in wastewaters only) 7440-28-0 1.4 RTHRM; or STABL
------------------
P114 Thallium selenite Selenium 7782-49-2 0.82 5.7 mg/L TCLP
------------------
P115 Thallium (I) sulfate Thallium (measured in wastewaters only) 7440-28-0 1.4 RTHRM; or STABL
------------------
P116 Thiosemicarbazide Thiosemicarbazide 79-19-6 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P118 Trichloromethanethiol Trichloromethanethiol 75-70-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
P119 Ammonium vanadate Vanadium (measured in wastewaters only) 7440-62-2 4.3 STABL
------------------
P120 Vanadium pentoxide Vanadium (measured in wastewaters only) 7440-62-2 4.3 STABL
------------------
P121 Zinc cyanide Cyanides (Total) \7\ 57-12-5 1.2 590
........................................................................... Cyanides (Amenable) \7\ 57-12-5 0.86 30
------------------
[[Page 211]]
P122 Zinc phosphide Zn3P2, when present at concentrations greater than 10%. Zinc Phosphide 1314-84-7 CHOXD; CHRED; or CHOXD; CHRED; or
CMBST CMBST
------------------
P123 Toxaphene Toxaphene 8001-35-2 0.0095 2.6
------------------
P127 Carbofuran Carbofuran 1563-66-2 0.006 0.14
------------------
P128 Mexacarbate Mexacarbate 315-18-4 0.056 1.4
------------------
P185 Tirpate \10\ Tirpate 26419-73-8 0.056 0.28
------------------
P188 Physostigmine salicylate Physostigmine salicylate 57-64-7 0.056 1.4
------------------
P189 Carbosulfan Carbosulfan 55285-14-8 0.028 1.4
------------------
P190 Metolcarb Metolcarb 1129-41-5 0.056 1.4
------------------
P191 Dimetilan \10\ Dimetilan 644-64-4 0.056 1.4
------------------
P192 Isolan \10\ Isolan 119-38-0 0.056 1.4
------------------
P194 Oxamyl Oxamyl 23135-22-0 0.056 0.28
------------------
P196 Manganese dimethyldithiocarbamate \10\ Dithiocarbamates (total) NA 0.028 28
------------------
P197 Formparanate \10\ Formparante 17702-57-7 0.056 1.4
------------------
P198 Formetanate hydrochloride Formetanate hydrochloride 23422-53-9 0.056 1.4
------------------
P199 Methiocarb Methiocarb 2032-65-7 0.056 1.4
------------------
P201 Promecarb Promecarb 2631-37-0 0.056 1.4
------------------
P202 m-Cumenyl methylcarbamate m-Cumenyl methylcarbamate 64-00-6 0.056 1.4
------------------
P203 Aldicarb sulfone Aldicarb sulfone 1646-88-4 0.056 0.28
------------------
P204 Physostigmine Physostigmine 57-47-6 0.056 1.4
------------------
P205 Ziram Dithiocarbamates (total) NA 0.028 28
------------------
U001 Acetaldehyde Acetaldehyde 75-07-0 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U202 Acetone Acetone 67-64-1 0.28 160
------------------
U003 Acetonitrile Acetonitrile 75-05-8 5.6 CMBST
[[Page 212]]
........................................................................... Acetonitrile; alternate \6\ standard for 75-05-8 NA 38
nonwastewaters only
------------------
U004 Acetophenone Acetophenone 98-86-2 0.010 9.7
------------------
U005 2-Acetylaminofluorene 2-Acetylaminofluorene 53-96-3 0.059 140
------------------
U006 Acetyl chloride Acetyl Chloride 75-36-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U007 Acrylamide Acrylamide 79-06-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U008 Acrylic acid Acrylic acid 79-10-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U009 Acrylonitrile Acrylonitrile 107-13-1 0.24 84
------------------
U010 Mitomycin C Mitomycin C 50-07-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U011 Amitrole Amitrole 61-82-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U012 Aniline Aniline 62-53-3 0.81 14
------------------
[[Page 213]]
U014 Auramine Auramine 492-80-8 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U015 Azaserine Azaserine 115-02-6 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U016 Benz(c)acridine Benz(c)acridine 225-51-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U017 Benzal chloride Benzal chloride 98-87-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U018 Benz(a)anthracene Benz(a)anthracene 56-55-3 0.059 3.4
------------------
U019 Benzene Benzene 71-43-2 0.14 10
------------------
U020 Benzenesulfonyl chloride Benzenesulfonyl chloride 98-09-9 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U021 Benzidine Benzidine 92-87-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U022 Benzo(a)pyrene Benzo(a)pyrene 50-32-8 0.061 3.4
------------------
U023 Benzotrichloride Benzotrichloride 98-07-7 CHOXD; CHRED; CHOCS; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
U024 bis(2-Chloroethoxy)methane bis(2)Chloroethoxy)methane 111-91-1 0.036 7.2
------------------
U025 bis(2-Chloroethyl)ether bis(2-Chloroethyl)ether 111-44-4 0.033 6.0
------------------
U026 Chlornaphazine Chlornaphazine 494-03-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U027 bis(2-Chloroisopropyl)ether bis(2-Chloroisopropyl)ether 39638-32-9 0.055 7.2
------------------
[[Page 214]]
U028 bis(2-Ethylhexyl) phthalate bis(2-Ethylhexyl) phthalate 117-81-7 0.28 28
------------------
U029 Methyl bromide (Bromomethane) Methyl bromide (Bromomethane) 74-83-9 0.11 15
------------------
U030 4-Bromophenyl phenyl ether 4-Bromophenyl phenyl ether 101-55-3 0.055 15
------------------
U031 n-Butyl alcohol n-Butyl alcohol 71-36-3 5.6 2.6
------------------
U032 Calcium chromate Chromium (Total) 7440-47-3 2.77 0.60 mg/L TCLP
------------------
U033 Carbon oxyfluoride Carbon oxyfluoride 353-50-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U034 Trichloroacetaldehyde (Chloral) Trichloroacetaldehyde (Chloral) 75-87-6 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U035 Chlorambucil Chlorambucil 305-03-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U036 Chlordane Chlordane (alpha and gamma isomers) 57-74-9 0.0033 0.26
------------------
U037 Chlorobenzene Chlorobenzene 108-90-7 0.057 60
------------------
U038 Chlorobenzilate Chlorobenzilate 510-15-6 0.10 CMBST
------------------
U039 p-Chloro-m-cresol p-Chloro-m-cresol 59-50-7 0.018 14
------------------
U041 Epichlorohydrin (1-Chloro-2,3-epoxypropane) Epichlorohydrin (1-Chloro-2,3- 106-89-8 (WETOX or CHOXD) CMBST
epoxypropane) fb CARBN; or CMBST
------------------
[[Page 215]]
U042 2-Chloroethyl vinyl ether 2-Chloroethyl vinyl ether 110-75-8 0.062 CMBST
------------------
U043 Vinyl chloride Vinyl chloride 75-01-4 0.27 6.0
------------------
U044 Chloroform Chloroform 67-66-3 0.046 6.0
------------------
U045 Chloromethane (Methyl chloride) Chloromethane (Methyl chloride) 74-87-3 0.19 30
------------------
U046 Chloromethyl methyl ether Chloromethyl methyl ether 107-30-2 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U047 2-Chloronaphthalene 2-Chloronaphthalene 91-58-7 0.055 5.6
------------------
U048 2-Chlorophenol 2-Chlorophenol 95-57-8 0.044 5.7
------------------
U049 4-Chloro-o-toluidine hydrochloride 4-Chloro-o-toluidine hydrochloride 3165-93-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U050 Chrysene Chrysene 218-01-9 0.059 3.4
------------------
U051 Creosote Naphthalene 91-20-3 0.059 5.6
........................................................................... Pentachlorophenol 87-86-5 0.089 7.4
........................................................................... Phenanthrene 85-01-8 0.059 5.6
........................................................................... Pyrene 129-00-0 0.067 8.2
........................................................................... Toluene 108-88-3 0.080 10
........................................................................... Xylenes-mixed isomers (sum of o-, m-, and 1330-20-7 0.32 30
p-xylene concentrations)
........................................................................... Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
U052 Cresols (Cresylic acid) o-Cresol 95-48-7 0.11 5.6
........................................................................... m-Cresol (difficult to distinguish from p- 108-39-4 0.77 5.6
cresol)
........................................................................... p-Cresol (difficult to distinguish from m- 106-44-5 0.77 5.6
cresol)
........................................................................... Cresol-mixed isomers (Cresylic acid) (sum 1319-77-3 0.88 11.2
of o- m-, and p-cresol concentrations)
------------------
U053 Crotonaldehyde Crotonaldehyde 4170-30-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
[[Page 216]]
U055 Cumene Cumene 98-82-8 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U056 Cyclohexane Cyclohexane 110-82-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U057 Cyclohexanone Cyclohexanone 108-94-1 0.36 CMBST
........................................................................... Cyclohexanone; alternate \6\ standard for 108-94-1 NA 0.75 mg/L TCLP
nonwastewaters only
------------------
U058 Cyclophosphamide Cyclophosphamide 50-18-0 CARBN; or CMBST CMBST
------------------
U059 Daunomycin Daunomycin 20830-81-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U060 DDD o,p'-DDD 53-19-0 0.023 0.087
........................................................................... p,p'-DDD 72-54-8 0.023 0.087
------------------
U061 DDT o-p'-DDT 789-02-6 0.0039 0.087
........................................................................... p,p'-DDT 50-29-3 0.0039 0.087
........................................................................... o,p'-DDD 53-19-0 0.023 0.087
........................................................................... p,p'-DDD 72-54-8 0.023 0.087
........................................................................... o,p'-DDE 3424-82-6 0.031 0.087
........................................................................... p,p'-DDE 72-55-9 0.031 0.087
------------------
U062 Diallate Diallate 2303-16-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U063 Dibenz(a,h)anthracene Dibenz(a,h)anthracene 53-70-3 0.055 8.2
------------------
[[Page 217]]
U064 Dibenz(a,i)pyrene Dibenz(a,i)pyrene 189-55-9 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U066 1,2-Dibromo-3-chloropropane 1,2-Dibromo-3-chloropropane 96-12-8 0.11 15
------------------
U067 Ethylene dibromide (1,2-Dibromoethane) Ethylene dibromide (1,2-Dibromoethane) 106-93-4 0.028 15
------------------
U068 Dibromomethane Dibromomethane 74-95-3 0.11 15
------------------
U069 Di-n-butyl phthalate Di-n-butyl phthalate 84-74-2 0.057 28
------------------
U070 o-Dichlorobenzene o-Dichlorobenzene 95-50-1 0.088 6.0
------------------
U071 m-Dichlorobenzene m-Dichlorobenzene 541-73-1 0.036 6.0
------------------
U072 p-Dichlorobenzene p-Dichlorobenzene 106-46-7 0.090 6.0
------------------
U073 3,3'-Dichlorobenzidine 3,3'-Dichlorobenzidine 91-94-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U074 1,4-Dichloro-2-butene cis,1,4-Dichloro-2-butene 1476-11-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
........................................................................... trans-1,4-Dichloro-2-butene 764-41-0 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U075 Dichlorodifluoromethane Dichlorodifluoromethane 75-71-8 0.23 7.2
------------------
U076 1,1-Dichloroethane 1,1-Dichloroethane 75-34-3 0.059 6.0
------------------
U077 1,2-Dichloroethane 1,2-Dichloroethane 107-06-2 0.21 6.0
------------------
U078 1,1-Dichloroethylene 1,1-Dichloroethylene 75-35-4 0.025 6.0
------------------
U079 1,2-Dichloroethylene trans-1,2-Dichloroethylene 156-60-5 0.054 30
------------------
U080 Methylene chloride Methylene chloride 75-09-2 0.089 30
------------------
U081 2,4-Dichlorophenol 2,4-Dichlorophenol 120-83-2 0.044 14
------------------
U082 2,6-Dichlorophenol 2,6-Dichlorophenol 87-65-0 0.044 14
------------------
[[Page 218]]
U083 1,2-Dichloropropane 1,2-Dichloropropane 78-87-5 0.85 18
------------------
U084 1,3-Dichloropropylene cis-1,3-Dichloropropylene 10061-01-5 0.036 18
........................................................................... trans-1,3-Dichloropropylene 10061-02-6 0.036 18
------------------
U085 1,2:3,4-Diepoxybutane 1,2,3,4-Diepoxybutane 1464-53-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U086 N,N'-Diethylhydrazine N,N'-Diethylhydrazine 1615-80-1 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
U087 O,O-Diethyl S-methyldithiophosphate O,O-Diethyl S-methyldithiophosphate 3288-58-2 CARBN; or CMBST CMBST
------------------
U088 Diethyl phthalate Diethyl phthalate 84-66-2 0.20 28
------------------
U089 Diethyl stilbestrol Diethyl stilbestrol 56-53-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U090 Dihydrosafrole Dihydrosafrole 94-58-6 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U091 3,3'-Dimethoxybenzidine 3,3'-Dimethoxybenzidine 119-90-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U092 Dimethylamine Dimethylamine 124-40-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
[[Page 219]]
U093 p-Dimethylaminoazobenzene p-Dimethylaminoazobenzene 60-11-7 0.13 CMBST
------------------
U094 7,12-Dimethylbenz(a)anthracene 7,12-Dimethylbenz(a)anthracene 57-97-6 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U095 3,3'-Dimethylbenzidine 3,3'-Dimethylbenzidine 119-93-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U096 alpha, alpha-Dimethyl benzyl hydroperoxide alpha, alpha-Dimethyl benzyl hydroperoxide 80-15-9 CHOXD; CHRED; CHOXD, CHRED; or
CARBN; BIODG; or CMBST
CMBSt
------------------
U097 Dimethylcarbamoyl chloride Dimethylcarbamoyl chloride 79-44-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U098 1,1-Dimethylhydrazine 1,1-Dimethylhydrazine 57-14-7 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
U099 1,2-Dimethylhydrazine 1,2-Dimethylhydrazine 540-73-8 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
U101 2,4-Dimethylphenol 2,4-Dimethylphenol 105-67-9 0.036 14
------------------
U102 Dimethyl phthalate Dimethyl phthalate 131-11-3 0.047 28
------------------
U103 Dimethyl sulfate Dimethyl sulfate 77-78-1 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
U105 2,4-Dinitrotoluene 2,4-Dinitrotoluene 121-14-2 0.32 140
------------------
U106 2,6-Dinitrotoluene 2,6-Dinitrotoluene 606-20-2 0.55 28
------------------
U107 Di-n-octyl phthalate Di-n-octyl phthalate 117-84-0 0.017 28
------------------
U108 1,4-Dioxane 1,4-Dioxane 123-91-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
........................................................................... 1,4-Dioxane, alternate \6\ 123-91-1 12.0 170
------------------
[[Page 220]]
U109 1,2-Diphenylhydrazine 1,2-Diphenylhydrazine 122-66-7 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
........................................................................... 1,2-Diphenylhydrazine; alternate \6\ 122-66-7 0.087 NA
standard for wastewaters only
------------------
U110 Dipropylamine Dipropylamine 142-84-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U111 Di-n-propylnitrosamine Di-n-propylnitrosamine 621-64-7 0.40 14
------------------
U112 Ethyl acetate Ethyl acetate 141-78-6 0.34 33
------------------
U113 Ethyl acrylate Ethyl acrylate 140-88-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U114 Ethylenebisdithiocarbamic acid salts and esters Ethylenebisdithiocarbamic acid 111-54-6 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U115 Ethylene oxide Ethylene oxide 75-21-8 (WETOX or CHOXD) CHOXD; or CMBST
fb CARBN; or CMBST
........................................................................... Ethylene oxide; alternate \6\ standard for 75-21-8 0.12 NA
wastewaters only
------------------
U116 Ethylene thiourea Ethylene thiourea 96-45-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U117 Ethyl ether Ethyl ether 60-29-7 0.12 160
------------------
[[Page 221]]
U118 Ethyl methacrylate Ethyl methacrylate 97-63-2 0.14 160
------------------
U119 Ethyl methane sulfonate Ethyl methane sulfonate 62-50-0 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U120 Fluoranthene Fluoranthene 206-44-0 0.068 3.4
------------------
U121 Trichlorofluoromethane Trichlorofluoromethane 75-69-4 0.020 30
------------------
U122 Formaldehyde Formaldehyde 50-00-0 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U123 Formic acid Formic acid 64-18-6 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U124 Furan Furan 110-00-9 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U125 Furfural Furfural 98-01-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U126 Gylcidyaldehyde Glycidyaldehyde 765-34-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U127 Hexachlorobenzene Hexachlorobenzene 118-74-1 0.055 10
------------------
U128 Hexachlorobutadiene Hexachlorobutadiene 87-68-3 0.055 5.6
------------------
U129 Lindane alpha-BHC 319-84-6 0.00014 0.066
........................................................................... beta-BHC 319-85-7 0.00014 0.066
........................................................................... delta-BHC 319-86-8 0.023 0.066
........................................................................... gamma-BHC (Lindane) 58-89-9 0.0017 0.066
------------------
U130 Hexachlorocyclopentadiene Hexachlorocyclopentadiene 77-47-4 0.057 2.4
------------------
U131 Hexachloroethane Hexachloroethane 67-72-1 0.055 30
------------------
[[Page 222]]
U132 Hexachlorophene Hexachlorophene 70-30-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U133 Hydrazine Hydrazine 302-01-2 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
U134 Hydrogen fluoride Fluoride (measured in wastewaters only) 16984-48-8 35 ADGAS fb NEUTR; or
NEUTR
------------------
U135 Hydrogen Sulfide Hydrogen Sulfide 7783-06-4 CHOXD; CHRED; or CHOXD; CHRED; or
CMBST CMBST
------------------
U136 Cacodylic acid Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
------------------
U137 Indeno(1,2,3-c,d)pyrene Indeno(1,2,3-c,d)pyrene 193-39-5 0.0055 3.4
------------------
U138 Iodomethane Iodomethane 74-88-4 0.19 65
------------------
U140 Isobutyl alcohol Isobutyl alcohol 78-83-1 5.6 170
------------------
U141 Isosafrole Isosafrole 120-58-1 0.081 2.6
------------------
U142 Kepone Kepone 143-50-8 0.0011 0.13
------------------
U143 Lasiocarpine Lasiocarpine 303-34-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U144 Lead acetate Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
U145 Lead phosphate Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
U146 Lead subacetate Lead 7439-92-1 0.69 0.75 mg/L TCLP
------------------
[[Page 223]]
U147 Maleic anhydride Maleic anhydride 108-31-6 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U148 Maleic hydrazide Maleic hydrazide 123-33-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U149 Malononitrile Malononitrile 109-77-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U150 Melphalan Malphalan 148-82-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U151 U151 (mercury) nonwastewaters that contain greater than or equal to 260 mg/ Mercury 7439-97-6 NA RMERC
kg total mercury.
------------------------------------------------------------------------------
U151 (mercury) nonwastewaters that contain less than 260 mg/kg total Mercury 7439-97-6 NA 0.20 mg/L TCLP
mercury and that are residues from RMERC only.
------------------------------------------------------------------------------
U151 (mercury) nonwastewaters that contain less than 260 mg/kg total Mercury 7439-97-6 NA 0.025 mg/L TCLP
mercury and that are not residues from RMERC.
------------------------------------------------------------------------------
All U151 (mercury) wastewaters. Mercury 7439-97-6 0.15 NA
------------------------------------------------------------------------------
Elemental Mercury Contaminated with Radioactive Materials Mercury 7439-97-6 NA AMLGM
------------------
U152 Methacrylonitrile Methacrylonitrile 126-98-7 0.24 84
------------------
U153 Methanethiol Methanethiol 74-93-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U154 Methanol Methanol 67-56-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
........................................................................... Methanol; alternate \6\ set of standards 67-56-1 5.6 0.75 mg/L TCLP
for both wastewaters and nonwastewaters
------------------
U155 Methapyrilene Methapyrilene 91-80-5 0.081 1.5
------------------
[[Page 224]]
U156 Methyl chlorocarbonate Methyl chlorocarbonate 79-22-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U157 3-Methylcholanthrene 3-Methylcholanthrene 56-49-5 0.0055 15
------------------
U158 4,4'-Methylene bis(2-chloroaniline) 4,4'-Methylene bis(2-chloroaniline) 101-14-4 0.50 30
------------------
U159 Methyl ethyl ketone Methyl ethyl ketone 78-93-3 0.28 36
------------------
U160 Methyl ethyl ketone peroxide Methyl ethyl ketone peroxide 1338-23-4 CHOXD; CHRED; CHOXD; CHRED; or
CARBN; BIODG; or CMBST
CMBST
------------------
U161 Methyl isobutyl ketone Methyl isobutyl ketone 108-10-1 0.14 33
------------------
U162 Methyl methacrylate Methyl methacrylate 80-62-6 0.14 160
------------------
U163 N-Methyl N'-nitro N-nitrosoguanidine N-Methyl N'-nitro N-nitrosoguanidine 70-25-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U164 Methylthiouracil Methylthiouracil 56-04-2 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U165 Naphthalene Naphthalene 91-20-3 0.059 5.6
------------------
U166 1,4-Naphthoquinone 1,4-Naphthoquinone 130-15-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
[[Page 225]]
U167 1-Naphthylamine 1-Naphthylamine 134-32-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U168 2-Naphthylamine 2-Naphthylamine 91-59-8 0.52 CMBST
------------------
U169 Nitrobenzene Nitrobenzene 98-95-3 0.068 14
------------------
U170 p-Nitrophenol p-Nitrophenol 100-02-7 0.12 29
------------------
U171 2-Nitropropane 2-Nitropropane 79-46-9 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U172 N-Nitrosodi-n-butylamine N-Nitrosodi-n-butylamine 924-16-3 0.040 17
------------------
U173 N-Nitrosodiethanolamine N-Nitrosodiethanolamine 1116-54-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U174 N-Nitrosodiethylamine N-Nitrosodiethylamine 55-18-5 0.40 28
------------------
U176 N-Nitroso-N-ethylurea N-Nitroso-N-ethylurea 759-73-9 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U177 N-Nitroso-N-methylurea N-Nitroso-N-methylurea 684-93-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U178 N-Nitroso-N-methylurethane N-Nitroso-N-methylurethane 615-53-2 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U179 N-Nitrosopiperidine N-Nitrosopiperidine 100-75-4 0.013 35
------------------
U180 N-Nitrosopyrrolidine N-Nitrosopyrrolidine 930-55-2 0.013 35
------------------
U181 5-Nitro-o-toluidine 5-Nitro-o-toluidine 99-55-8 0.32 28
------------------
U182 Paraldehyde Paraldehyde 123-63-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
[[Page 226]]
U183 Pentachlorobenzene Pentachlorobenzene 608-93-5 0.055 10
------------------
U184 Pentachloroethane Pentachloroethane 76-01-7 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
........................................................................... Pentachloroethane; alternate \6\ standards 76-01-7 0.055 6.0
for both wastewaters and nonwastewaters
------------------
U185 Pentachloronitrobenzene Pentachloronitrobenzene 82-68-8 0.055 4.8
------------------
U186 1,3-Pentadiene 1,3-Pentadiene 504-60-9 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U187 Phenacetin Phenacetin 62-44-2 0.081 16
------------------
U188 Phenol Phenol 108-95-2 0.039 6.2
------------------
U189 Phosphorus sulfide Phosphorus sulfide 1314-80-3 CHOXD; CHRED; or CHOXd; CHRED; or
CMBST CMBST
------------------
U190 Phthalic anhydride (measured as Phthalic acid or Terephthalic acid Phthalic anhydride (measured as Phthalic 100-21-0 0.055 28
acid or Terephthalic acid)
........................................................................... Phthalic anhydride (measured as Phthalic 85-44-9 0.055 28
acid or Terephthalic acid)
------------------
U191 2-Picoline 2-Picoline 109-06-8 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U192 Pronamide Pronamide 23950-58-5 0.093 1.5
------------------
[[Page 227]]
U193 1,3-Propane sultone 1,3-Propane sultone 1120-71-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U194 n-Propylamine n-Propylamine 107-10-8 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U196 Pyridine Pyridine 110-86-1 0.014 16
------------------
U197 p-Benzoquinone p-Benzoquinone 106-51-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U200 Reserpine Reserpine 50-55-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U201 Resorcinol Resorcinol 108-46-3 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U202 Saccharin and salts Saccharin 81-07-2 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U203 Safrole Safrole 94-59-7 0.081 22
------------------
U204 Selenium dioxide Selenium 7782-49-2 0.82 5.7 mg/L TCLP
------------------
U205 Selenium sulfide Selenium 7782-49-2 0.82 5.7 mg/L TCLP
------------------
U206 Streptozotocin Streptozotocin 18883-66-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U207 1,2,4,5-Tetrachlorobenzene 1,2,4,5-Tetrachlorobenzene 95-94-5 0.055 14
------------------
U208 1,1,1,2-Tetrachloroethane 1,1,1,2-Tetrachloroethane 630-20-6 0.057 6.0
------------------
U209 1,1,2,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane 79-34-5 0.057 6.0
------------------
U210 Tetrachloroethylene Tetrachloroethylene 127-18-4 0.056 6.0
------------------
[[Page 228]]
U211 Carbon tetrachloride Carbon tetrachloride 56-23-5 0.057 6.0
------------------
U213 Tetrahydrofuran Tetrahydrofuran 109-99-9 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U214 Thallium (I) acetate Thallium (measured in wastewaters only) 7440-28-0 1.4 RTHRM; or STABL
------------------
U215 Thallium (I) carbonate Thallium (measured in wastewaters only) 7440-28-0 1.4 RTHRM; or STABL
------------------
U216 Thallium (I) chloride Thallium (measured in wastewaters only) 7440-28-0 1.4 RTHRM; or STABL
------------------
U217 Thallium (I) nitrate Thallium (measured in wastewaters only) 7440-28-0 1.4 RTHRM; or STABL
------------------
U218 Thioacetamide Thioacetamide 62-55-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U219 Thiourea Thiourea 62-56-6 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U220 Toluene Toluene 108-88-3 0.080 10
------------------
U221 Toluenediamine Toluenediamine 25376-45-8 CARBN; or CMBST CMBST
------------------
U222 o-Toluidine hydrochloride o-Toluidine hydrochloride 636-21-5 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
[[Page 229]]
U223 Toluene diisocyanate Toluene diisocyanate 26471-62-5 CARBN; or CMBST CMBST
------------------
U225 Bromoform (Tribromomethane) Bromoform (Tribromomethane) 75-25-2 0.63 15
------------------
U226 1,1,1-Trichloroethane 1,1,1-Trichloroethane 71-55-6 0.054 6.0
------------------
U227 1,1,2-Trichloroethane 1,1,2-Trichloroethane 79-00-5 0.054 6.0
------------------
U228 Trichloroethylene Trichloroethylene 79-01-6 0.054 6.0
------------------
U234 1,3,5-Trinitrobenzene 1,3,5-Trinitrobenzene 99-35-4 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U235 tris-(2,3-Dibromopropyl)-phosphate tris-(2,3-Dibromopropyl)-phosphate 126-72-7 0.11 0.10
------------------
U236 Trypan Blue Trypan Blue 72-57-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U237 Uracil mustard Uracil mustard 66-75-1 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U238 Urethane (Ethyl carbamate) Urethane (Ethyl carbamate) 51-79-6 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U239 Xylenes Xylenes-mixed isomers (sum of o-, m-, and 1330-20-7 0.32 30
p-xylene concentrations)
------------------
U240 2,4-D (2,4-Dichlorophenoxyacetic acid) 2,4-D(2,4-Dichlorophenoxyacetic acid) 94-75-7 0.72 10
------------------------------------------------------------------------------
2,4-D (2,4-Dichlorophenoxyacetic acid) salts and esters .......................................... NA (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U243 Hexachloropropylene Hexachloropropylene 1888-71-7 0.035 30
------------------
U244 Thiram Thiram 137-26-8 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
[[Page 230]]
U246 Cyanogen bromide Cyanogen bromide 506-68-3 CHOXD; WETOX; or CHOXD; WETOX; or
CMBST CMBST
------------------
U247 Methoxychlor Methoxychlor 72-43-5 0.25 0.18
------------------
U248 Warfarin, & salts, when present at concentrations of 0.3% or less Warfarin 81-81-2 (WETOX or CHOXD) CMBST
fb CARBN; or CMBST
------------------
U249 Zinc phosphide, Zn3,P2, when present at concentrations of 10% or less Zinc Phosphide 1314-84-7 CHOXD; CHRED; or CHOXD; CHRED; or
CMBST CMBST
------------------
U271 Benomyl Benomyl 17804-35-2 0.056 1.4
------------------
U278 Bendiocarb Bendiocarb 22781-23-3 0.056 1.4
------------------
U279 Carbaryl Carbaryl 63-25-2 0.006 0.14
------------------
U280 Barban Barban 101-27-9 0.056 1.4
------------------
U328 o-Toluidine o-Toluidine 95-53-4 CMBST; or CHOXD fb CMBST
(BIODG or CARBN);
or BIODG fb CARBN
------------------
U353 p-Toluidine p-Toluidine 106-49-0 CMBST; or CHOXD fb CMBST
(BIODG or CARBN);
or BIODG fb CARBN
------------------
U359 2-Ethoxyethanol 2-Ethoxyethanol 110-80-5 CMBST; or CHOXD fb CMBST
(BIODG or CARBN);
or BIODG fb CARBN
------------------
[[Page 231]]
U364 Bendiocarb phenol \10\ Bendiocarb phenol 22961-82-6 0.056 1.4
------------------
U367 Carbofuran phenol Carbofuran phenol 1563-38-8 0.056 1.4
------------------
U372 Carbendazim Carbendazim 10605-21-7 0.056 1.4
------------------
U373 Propham Propham 122-42-9 0.056 1.4
------------------
U387 Prosulfocarb Prosulfocarb 52888-80-9 0.042 1.4
------------------
U389 Triallate Triallate 2303-17-5 0.042 1.4
------------------
U394 A2213 \10\ A2213 30558-43-1 0.042 1.4
------------------
U395 Diethylene glycol, dicarbamate \10\ Diethylene glycol, dicarbamate 5952-26-1 0.056 1.4
------------------
U404 Triethylamine Triethylamine 121-44-8 0.081 1.5
------------------
U409 Thiophanate-methyl Thiophanate-methyl 23564-05-8 0.056 1.4
------------------
U410 Thiodicarb Thiodicarb 59669-26-0 0.019 1.4
------------------
U411 Propoxur Propoxur 114-26-1 0.056 1.4
------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------
[[Page 232]]
FOOTNOTES TO TREATMENT STANDARD TABLE 268.40
1 The waste descriptions provided in this table do not
replace waste descriptions in 40 CFR 261.
Descriptions of Treatment/Regulatory Subcategories
are provided, as needed, to distinguish between
applicability of different standards.
2 CAS means Chemical Abstract Services. When the waste
code and/or regulated constituents are described as
a combination of a chemical with its salts and/or
esters, the CAS number is given for the parent
compound only.
3 Concentration standards for wastewaters are
expressed in mg/L and are based on analysis of
composite samples.
4 All treatment standards expressed as a Technology
Code or combination of Technology Codes are
explained in detail in 40 CFR 268.42 Table 1--
Technology Codes and Descriptions of Technology-
Based Standards.
5 Except for Metals (EP or TCLP) and Cyanides (Total
and Amenable) the nonwastewater treatment standards
expressed as a concentration were established, in
part, based upon incineration in units operated in
accordance with the technical requirements of 40
CFR Part 264 Subpart O or Part 265 Subpart O, or
based upon combustion in fuel substitution units
operating in accordance with applicable technical
requirements. A facility may comply with these
treatment standards according to provisions in 40
CFR 268.40(d). All concentration standards for
nonwastewaters are based on analysis of grab
samples.
6 Where an alternate treatment standard or set of
alternate standards has been indicated, a facility
may comply with this alternate standard, but only
for the Treatment/Regulatory Subcategory or
physical form (i.e., wastewater and/or
nonwastewater) specified for that alternate
standard.
7 Both Cyanides (Total) and Cyanides (Amenable) for
nonwastewaters are to be analyzed using Method 9010
or 9012, found in ``Test Methods'' for Evaluating
Solid Waste, Physical/Chemical Methods,'' EPA
Publication SW-846, as incorporated by reference in
40 CFR 260.11, with a sample size of 10 grams and a
distillation time of one hour and 15 minutes.
8 These wastes, when rendered nonhazardous and then
subsequently managed in CWA, or CWA-equivalent
systems are not subject to treatment standards.
(See Sec. 268.1(c0(3) and (4)).
9 These wastes, when rendered nonhazardous and then
subsequently injected in a Class SDWA well, are not
subject to treatment standards. (See Sec.
148.1(d)).
10 The treatment standard for this waste may be
satisfied by either meeting the constituent
concentrations in this table or by treating the
waste by the specified technologies: combustion, as
defined by the technology code CMBST at Sec.
268.42 Table 1 of this Part, for nonwastewaters;
and biodegradation as defined by the technology
code BIODG, carbon adsorption as defined by the
technology code CARBN, chemical oxidation as
defined by the technology code CHOXD, or combustion
as defined as technology code CMBST at Sec. 268.42
Table 1 of this Part, for wastewaters.
11 For these wastes, the definition of CMBST is limited
to: (1) combustion units operating under 40 CFR
266, (2) combustion units permitted under 40 CFR
Part 264, Subpart O, or (3) combustion units
operating under 40 CFR 265, Subpart O, which have
obtained a determination of equivalent treatment
under 268.42(b).
12 Disposal of K175 wastes that have complied with all
applicable 40 CFR 268.40 treatment standards must
also be macroencapsulated in accordance with 40 CFR
268.45 Table 1 unless the waste is placed in:
(1) A Subtitle C monofill containing only K175
wastes that meet all applicable 40 CFR 268.40
treatment standards; or
(2) A dedicated Subtitle C landfill cell in which
all other wastes being co-disposed are at pH[le]6.0.
[[Page 233]]
[59 FR 48046, Sept. 19, 1994]
Editorial Note: For Federal Register citations affecting
Sec. 268.40, see the List of CFR Sections Affected, which appears in the
Finding Aids section of the printed volume and on GPO Access.
Sec. 268.41 Treatment standards expressed as concentrations in waste extract.
For the requirements previously found in this section and for
treatment standards in Table CCWE--Constituent Concentrations in Waste
Extracts, refer to Sec. 268.40.
[59 FR 48103, Sept. 19, 1994]
Sec. 268.42 Treatment standards expressed as specified technologies.
Note: For the requirements previously found in this section in Table
2--Technology-Based Standards By RCRA Waste Code, and Table 3--
Technology-Based Standards for Specific Radioactive Hazardous Mixed
Waste, refer to Sec. 268.40.
(a) The following wastes in the table in Sec. 268.40 ``Treatment
Standards for Hazardous Wastes,'' for which standards are expressed as a
treatment method rather than a concentration level, must be treated
using the technology or technologies specified in the table entitled
``Technology Codes and Description of Technology-Based Standards'' in
this section.
Table 1--Technology Codes and Description of Technology-Based Standards
------------------------------------------------------------------------
Technology code Description of technology-based standards
------------------------------------------------------------------------
ADGAS: Venting of compressed gases into an absorbing or
reacting media (i.e., solid or liquid)--venting
can be accomplished through physical release
utilizing valves/piping; physical penetration
of the container; and/or penetration through
detonation.
AMLGM: Amalgamation of liquid, elemental mercury
contaminated with radioactive materials
utilizing inorganic reagents such as copper,
zinc, nickel, gold, and sulfur that result in a
nonliquid, semi-solid amalgam and thereby
reducing potential emissions of elemental
mercury vapors to the air.
BIODG: Biodegradation of organics or non-metallic
inorganics (i.e., degradable inorganics that
contain the elements of phosphorus, nitrogen,
and sulfur) in units operated under either
aerobic or anaerobic conditions such that a
surrogate compound or indicator parameter has
been substantially reduced in concentration in
the residuals (e.g., Total Organic Carbon can
often be used as an indicator parameter for the
biodegradation of many organic constituents
that cannot be directly analyzed in wastewater
residues).
CARBN: Carbon adsorption (granulated or powdered) of
non-metallic inorganics, organo-metallics, and/
or organic constituents, operated such that a
surrogate compound or indicator parameter has
not undergone breakthrough (e.g., Total Organic
Carbon can often be used as an indicator
parameter for the adsorption of many organic
constituents that cannot be directly analyzed
in wastewater residues). Breakthrough occurs
when the carbon has become saturated with the
constituent (or indicator parameter) and
substantial change in adsorption rate
associated with that constituent occurs.
CHOXD: Chemical or electrolytic oxidation utilizing the
following oxidation reagents (or waste
reagents) or combinations of reagents: (1)
Hypochlorite (e.g., bleach); (2) chlorine; (3)
chlorine dioxide; (4) ozone or UV (ultraviolet
light) assisted ozone; (5) peroxides; (6)
persulfates; (7) perchlorates; (8)
permangantes; and/or (9) other oxidizing
reagents of equivalent efficiency, performed in
units operated such that a surrogate compound
or indicator parameter has been substantially
reduced in concentration in the residuals
(e.g., Total Organic Carbon can often be used
as an indicator parameter for the oxidation of
many organic constituents that cannot be
directly analyzed in wastewater residues).
Chemical oxidation specifically includes what
is commonly referred to as alkaline
chlorination.
CHRED: Chemical reduction utilizing the following
reducing reagents (or waste reagents) or
combinations of reagents: (1) Sulfur dioxide;
(2) sodium, potassium, or alkali salts or
sulfites, bisulfites, metabisulfites, and
polyethylene glycols (e.g., NaPEG and KPEG);
(3) sodium hydrosulfide; (4) ferrous salts; and/
or (5) other reducing reagents of equivalent
efficiency, performed in units operated such
that a surrogate compound or indicator
parameter has been substantially reduced in
concentration in the residuals (e.g., Total
Organic Halogens can often be used as an
indicator parameter for the reduction of many
halogenated organic constituents that cannot be
directly analyzed in wastewater residues).
Chemical reduction is commonly used for the
reduction of hexavalent chromium to the
trivalent state.
CMBST: High temperature organic destruction
technologies, such as combustion in
incinerators, boilers, or industrial furnaces
operated in accordance with the applicable
requirements of 40 CFR part 264, subpart O, or
40 CFR part 265, subpart O, or 40 CFR part 266,
subpart H, and in other units operated in
accordance with applicable technical operating
requirements; and certain non-combustive
technologies, such as the Catalytic Extraction
Process.
DEACT: Deactivation to remove the hazardous
characteristics of a waste due to its
ignitability, corrosivity, and/or reactivity.
FSUBS: Fuel substitution in units operated in
accordance with applicable technical operating
requirements.
HLVIT: Vitrification of high level mixed radioactive
wastes in units in compliance with all
applicable radioactive protection requirements
under control of the Nuclear Regulatory
Commission.
IMERC: Incineration of wastes containing organics and
mercury in units operated in accordance with
the technical operating requirements of 40 CFR
part 264 subpart 0 and part 265 subpart 0. All
wastewater and nonwastewater residues derived
from this process must then comply with the
corresponding treatment standards per waste
code with consideration of any applicable
subcategories (e.g., High or Low Mercury
Subcategories).
[[Page 234]]
INCIN: Incineration in units operated in accordance
with the technical operating requirements of 40
CFR part 264 subpart 0 and part 265 subpart 0.
LLEXT: Liquid-liquid extraction (often referred to as
solvent extraction) of organics from liquid
wastes into an immiscible solvent for which the
hazardous constituents have a greater solvent
affinity, resulting in an extract high in
organics that must undergo either incineration,
reuse as a fuel, or other recovery/reuse and a
raffinate (extracted liquid waste)
proportionately low in organics that must
undergo further treatment as specified in the
standard.
MACRO: Macroencapsulation with surface coating
materials such as polymeric organics (e.g.,
resins and plastics) or with a jacket of inert
inorganic materials to substantially reduce
surface exposure to potential leaching media.
Macroencapsulation specifically does not
include any material that would be classified
as a tank or container according to 40 CFR
260.10.
NEUTR: Neutralization with the following reagents (or
waste reagents) or combinations of reagents:
(1) Acids; (2) bases; or (3) water (including
wastewaters) resulting in a pH greater than 2
but less than 12.5 as measured in the aqueous
residuals.
NLDBR: No land disposal based on recycling.
POLYM: Formation of complex high-molecular weight
solids through polymerization of monomers in
high-TOC D001 non-wastewaters which are
chemical components in the manufacture of
plastics.
PRECP: Chemical precipitation of metals and other
inorganics as insoluble precipitates of oxides,
hydroxides, carbonates, sulfides, sulfates,
chlorides, flourides, or phosphates. The
following reagents (or waste reagents) are
typically used alone or in combination: (1)
Lime (i.e., containing oxides and/or hydroxides
of calcium and/or magnesium; (2) caustic (i.e.,
sodium and/or potassium hydroxides; (3) soda
ash (i.e., sodium carbonate); (4) sodium
sulfide; (5) ferric sulfate or ferric chloride;
(6) alum; or (7) sodium sulfate. Additional
floculating, coagulation or similar reagents/
processes that enhance sludge dewatering
characteristics are not precluded from use.
RBERY: Thermal recovery of Beryllium.
RCGAS: Recovery/reuse of compressed gases including
techniques such as reprocessing of the gases
for reuse/resale; filtering/adsorption of
impurities; remixing for direct reuse or
resale; and use of the gas as a fuel source.
RCORR: Recovery of acids or bases utilizing one or more
of the following recovery technologies: (1)
Distillation (i.e., thermal concentration); (2)
ion exchange; (3) resin or solid adsorption;
(4) reverse osmosis; and/or (5) incineration
for the recovery of acid--Note: this does not
preclude the use of other physical phase
separation or concentration techniques such as
decantation, filtration (including
ultrafiltration), and centrifugation, when used
in conjunction with the above listed recovery
technologies.
RLEAD: Thermal recovery of lead in secondary lead
smelters.
RMERC: Retorting or roasting in a thermal processing
unit capable of volatilizing mercury and
subsequently condensing the volatilized mercury
for recovery. The retorting or roasting unit
(or facility) must be subject to one or more of
the following: (a) a National Emissions
Standard for Hazardous Air Pollutants (NESHAP)
for mercury; (b) a Best Available Control
Technology (BACT) or a Lowest Achievable
Emission Rate (LAER) standard for mercury
imposed pursuant to a Prevention of Significant
Deterioration (PSD) permit; or (c) a state
permit that establishes emission limitations
(within meaning of section 302 of the Clean Air
Act) for mercury. All wastewater and
nonwastewater residues derived from this
process must then comply with the corresponding
treatment standards per waste code with
consideration of any applicable subcategories
(e.g., High or Low Mercury Subcategories).
RMETL: Recovery of metals or inorganics utilizing one
or more of the following direct physical/
removal technologies: (1) Ion exchange; (2)
resin or solid (i.e., zeolites) adsorption; (3)
reverse osmosis; (4) chelation/solvent
extraction; (5) freeze crystalization; (6)
ultrafiltration and/or (7) simple precipitation
(i.e., crystalization)--Note: This does not
preclude the use of other physical phase
separation or concentration techniques such as
decantation, filtration (including
ultrafiltration), and centrifugation, when used
in conjunction with the above listed recovery
technologies.
RORGS: Recovery of organics utilizing one or more of
the following technologies: (1) Distillation;
(2) thin film evaporation; (3) steam stripping;
(4) carbon adsorption; (5) critical fluid
extraction; (6) liquid-liquid extraction; (7)
precipitation/crystalization (including freeze
crystallization); or (8) chemical phase
separation techniques (i.e., addition of acids,
bases, demulsifiers, or similar chemicals);--
Note: this does not preclude the use of other
physical phase separation techniques such as a
decantation, filtration (including
ultrafiltration), and centrifugation, when used
in conjunction with the above listed recovery
technologies.
RTHRM: Thermal recovery of metals or inorganics from
nonwastewaters in units identified as
industrial furnaces according to 40 CFR 260.10
(1), (6), (7), (11), and (12) under the
definition of ``industrial furnaces''.
RZINC: Resmelting in high temperature metal recovery
units for the purpose of recovery of zinc.
STABL: Stabilization with the following reagents (or
waste reagents) or combinations of reagents:
(1) Portland cement; or (2) lime/pozzolans
(e.g., fly ash and cement kiln dust)--this does
not preclude the addition of reagents (e.g.,
iron salts, silicates, and clays) designed to
enhance the set/cure time and/or compressive
strength, or to overall reduce the leachability
of the metal or inorganic.
SSTRP: Steam stripping of organics from liquid wastes
utilizing direct application of steam to the
wastes operated such that liquid and vapor flow
rates, as well as, temperature and pressure
ranges have been optimized, monitored, and
maintained. These operating parameters are
dependent upon the design parameters of the
unit such as, the number of separation stages
and the internal column design. Thus, resulting
in a condensed extract high in organics that
must undergo either incineration, reuse as a
fuel, or other recovery/reuse and an extracted
wastewater that must undergo further treatment
as specified in the standard.
WETOX: Wet air oxidation performed in units operated
such that a surrogate compound or indicator
parameter has been substantially reduced in
concentration in the residuals (e.g., Total
Organic Carbon can often be used as an
indicator parameter for the oxidation of many
organic constituents that cannot be directly
analyzed in wastewater residues).
[[Page 235]]
WTRRX: Controlled reaction with water for highly
reactive inorganic or organic chemicals with
precautionary controls for protection of
workers from potential violent reactions as
well as precautionary controls for potential
emissions of toxic/ignitable levels of gases
released during the reaction.
------------------------------------------------------------------------
Note 1: When a combination of these technologies (i.e., a treatment
train) is specified as a single treatment standard, the order of
application is specified in Sec. 268.42, Table 2 by indicating the
five letter technology code that must be applied first, then the
designation ``fb.'' (an abbreviation for ``followed by''), then the
five letter technology code for the technology that must be applied
next, and so on.
Note 2: When more than one technology (or treatment train) are specified
as alternative treatment standards, the five letter technology codes
(or the treatment trains) are separated by a semicolon (;) with the
last technology preceded by the word ``OR''. This indicates that any
one of these BDAT technologies or treatment trains can be used for
compliance with the standard.
(b) Any person may submit an application to the Administrator
demonstrating that an alternative treatment method can achieve a measure
of performance equivalent to that achieved by methods specified in
paragraphs (a), (c), and (d) of this section for wastes or specified in
Table 1 of Sec. 268.45 for hazardous debris. The applicant must submit
information demonstrating that his treatment method is in compliance
with federal, state, and local requirements and is protective of human
health and the environment. On the basis of such information and any
other available information, the Administrator may approve the use of
the alternative treatment method if he finds that the alternative
treatment method provides a measure of performance equivalent to that
achieved by methods specified in paragraphs (a), (c), and (d) of this
section for wastes or in Table 1 of Sec. 268.45 for hazardous debris.
Any approval must be stated in writing and may contain such provisions
and conditions as the Administrator deems appropriate. The person to
whom such approval is issued must comply with all limitations contained
in such a determination.
(c) As an alternative to the otherwise applicable subpart D
treatment standards, lab packs are eligible for land disposal provided
the following requirements are met:
(1) The lab packs comply with the applicable provisions of 40 CFR
264.316 and 40 CFR 265.316;
(2) The lab pack does not contain any of the wastes listed in
Appendix IV to part 268;
(3) The lab packs are incinerated in accordance with the
requirements of 40 CFR part 264, subpart O or 40 CFR part 265, subpart
O; and
(4) Any incinerator residues from lab packs containing D004, D005,
D006, D007, D008, D010, and D011 are treated in compliance with the
applicable treatment standards specified for such wastes in subpart D of
this part.
(d) Radioactive hazardous mixed wastes are subject to the treatment
standards in Sec. 268.40. Where treatment standards are specified for
radioactive mixed wastes in the Table of Treatment Standards, those
treatment standards will govern. Where there is no specific treatment
standard for radioactive mixed waste, the treatment standard for the
hazardous waste (as designated by EPA waste code) applies. Hazardous
debris containing radioactive waste is subject to the treatment
standards specified in Sec. 268.45.
[51 FR 40642, Nov. 7, 1986, as amended at 52 FR 25790, July 8, 1987; 55
FR 22692, June 1, 1990; 56 FR 3884, Jan. 31, 1991; 57 FR 8089, Mar. 6,
1992; 57 FR 37273, Aug. 18, 1992; 58 FR 29885, May 24, 1993; 59 FR
31552, June 20, 1994; 59 FR 48103, Sept. 19, 1994; 60 FR 302, Jan. 3,
1995; 61 FR 15654, Apr. 8, 1996; 62 FR 26025, May 12, 1997; 63 FR 28738,
May 26, 1998]
Sec. 268.43 Treatment standards expressed as waste concentrations.
For the requirements previously found in this section and for
treatment standards in Table CCW--Constituent Concentrations in Wastes,
refer to Sec. 268.40.
[59 FR 48103, Sept. 19, 1994]
Sec. 268.44 Variance from a treatment standard.
(a) Based on a petition filed by a generator or treater of hazardous
waste, the Administrator may approve a variance from an applicable
treatment standard if:
[[Page 236]]
(1) It is not physically possible to treat the waste to the level
specified in the treatment standard, or by the method specified as the
treatment standard. To show that this is the case, the petitioner must
demonstrate that because the physical or chemical properties of the
waste differ significantly from waste analyzed in developing the
treatment standard, the waste cannot be treated to the specified level
or by the specified method; or
(2) It is inappropriate to require the waste to be treated to the
level specified in the treatment standard or by the method specified as
the treatment standard, even though such treatment is technically
possible. To show that this is the case, the petitioner must either
demonstrate that:
(i) Treatment to the specified level or by the specified method is
technically inappropriate (for example, resulting in combustion of large
amounts of mildly contaminated environmental media); or
(ii) For remediation waste only, treatment to the specified level or
by the specified method is environmentally inappropriate because it
would likely discourage aggressive remediation.
(b) Each petition must be submitted in accordance with the
procedures in Sec. 260.20.
(c) Each petition must include the following statement signed by the
petitioner or an authorized representative:
I certify under penalty of law that I have personally examined and
am familiar with the information submitted in this petition and all
attached documents, and that, based on my inquiry of those individuals
immediately responsible for obtaining the information, I believe that
the submitted information is true, accurate, and complete. I am aware
that these are significant penalties for submitting false information,
including the possibility of fine and imprisonment.
(d) After receiving a petition for variance from a treatment
standard, the Administrator may request any additional information or
samples which he may require to evaluate the petition. Additional copies
of the complete petition may be requested as needed to send to affected
states and Regional Offices.
(e) The Administrator will give public notice in the Federal
Register of the intent to approve or deny a petition and provide an
opportunity for public comment. The final decision on a variance from a
treatment standard will be published in the Federal Register.
(f) A generator, treatment facility, or disposal facility that is
managing a waste covered by a variance from the treatment standards must
comply with the waste analysis requirements for restricted wastes found
under Sec. 268.7.
(g) During the petition review process, the applicant is required to
comply with all restrictions on land disposal under this part once the
effective date for the waste has been reached.
(h) Based on a petition filed by a generator or treater of hazardous
waste, the Administrator or his or her delegated representative may
approve a site-specific variance from an applicable treatment standard
if:
(1) It is not physically possible to treat the waste to the level
specified in the treatment standard, or by the method specified as the
treatment standard. To show that this is the case, the petitioner must
demonstrate that because the physical or chemical properties of the
waste differ significantly from waste analyzed in developing the
treatment standard, the waste cannot be treated to the specified level
or by the specified method; or
(2) It is inappropriate to require the waste to be treated to the
level specified in the treatment standard or by the method specified as
the treatment standard, even though such treatment is technically
possible. To show that this is the case, the petitioner must either
demonstrate that:
(i) Treatment to the specified level or by the specified method is
technically inappropriate (for example, resulting in combustion of large
amounts of mildly contaminated environmental media where the treatment
standard is not based on combustion of such media); or
(ii) For remediation waste only, treatment to the specified level or
by the specified method is environmentally inappropriate because it
would likely discourage aggressive remediation.
[[Page 237]]
(3) For contaminated soil only, treatment to the level or by the
method specified in the soil treatment standards would result in
concentrations of hazardous constituents that are below (i.e., lower
than) the concentrations necessary to minimize short- and long-term
threats to human health and the environment. Treatment variances
approved under this paragraph must:
(i) At a minimum, impose alternative land disposal restriction
treatment standards that, using a reasonable maximum exposure scenario:
(A) For carcinogens, achieve constituent concentrations that result
in the total excess risk to an individual exposed over a lifetime
generally falling within a range from 10 -4 to 10
-6; and
(B) For constituents with non-carcinogenic effects, achieve
constituent concentrations that an individual could be exposed to on a
daily basis without appreciable risk of deleterious effect during a
lifetime.
(ii) Not consider post-land-disposal controls.
(4) For contaminated soil only, treatment to the level or by the
method specified in the soil treatment standards would result in
concentrations of hazardous constituents that are below (i.e., lower
than) natural background concentrations at the site where the
contaminated soil will land disposed.
(5) Public notice and a reasonable opportunity for public comment
must be provided before granting or denying a petition.
(i) Each application for a site-specific variance from a treatment
standard must include the information in Sec. 260.20(b)(1)-(4);
(j) After receiving an application for a site-specific variance from
a treatment standard, the Assistant Administrator, or his delegated
representative, may request any additional information or samples which
may be required to evaluate the application.
(k) A generator, treatment facility, or disposal facility that is
managing a waste covered by a site-specific variance from a treatment
standard must comply with the waste analysis requirements for restricted
wastes found under Sec. 268.7.
(l) During the application review process, the applicant for a site-
specific variance must comply with all restrictions on land disposal
under this part once the effective date for the waste has been reached.
(m) For all variances, the petitioner must also demonstrate that
compliance with any given treatment variance is sufficient to minimize
threats to human health and the environment posed by land disposal of
the waste. In evaluating this demonstration, EPA may take into account
whether a treatment variance should be approved if the subject waste is
to be used in a manner constituting disposal pursuant to 40 CFR 266.20
through 266.23.
(n) [Reserved]
(o) The following facilities are excluded from the treatment
standards under Sec. 268.40, and are subject to the following
constituent concentrations:
[[Page 238]]
Table--Wastes Excluded From the Treatment Standards Under Sec. 268.40
--------------------------------------------------------------------------------------------------------------------------------------------------------
Wastewaters Nonwastewaters
Regulated hazardous -------------------------------------------------------
Facility name\1\ and address Waste code See also constituent Concentration Concentration
(mg/l) Notes (mg/kg) Notes
--------------------------------------------------------------------------------------------------------------------------------------------------------
Ball-Foster Glass Container D010 Table CCWE in 268.40 Selenium............ NA NA 25 NA
Corporation, El Monte, CA (\6\),
(\7\).
Craftsman Plating and Tinning, F006 Table CCWE in 268.40 Cyanides (Total).... 1.2 (\2\) 1800 (\4\)
Corp., Chicago, IL.
................ Cyanides (Amenable). .86 (\2\ and 30 (\4\)
\3\)
................ Cadmium............. 1.6 ........... NA ...........
................ Chromium............ .32 ........... NA ...........
................ Lead................ .040 ........... NA ...........
................ Nickel.............. .44 ........... NA ...........
CWM Chemical Services, LLC, Model K088\9\ Standards under Sec. Arsenic............. 1.4 NA 5.0 mg/L TCLP NA
City, New York. 268.40.
Dupont Environmental Treatment-- K088 Standards under Sec. Arsenic............. 1.4 NA 5.0 mg/L TCLP NA
Chambers Works Wastewater 268.40.
Treatment Plant, Deepwater, NJ
\8\.
Owens Brockway Glass Container D010 Table CCWE in 268.40 Selenium............ NA NA 51 NA
Company, Vernon, CA (\5\), (\7\).
Northwestern Plating Works, Inc., F006 Table CCWE in 268.40 Cyanides (Total).... 1.2 (\2\ and 970 (\4\)
Chicago, IL. \3\)
................ Cyanides (Amenable). .86 (\2\) 30 (\4\)
................ Cadmium............. 1.6 ........... NA ...........
................ Chromium............ .32 ........... NA ...........
................ Lead................ .040 ........... NA ...........
................ Nickel.............. .44 ........... NA ...........
U.S. Ecology Idaho, Incorporated, K088\10\ Standards under Sec. Arsenic............. 1.4 NA 5.0 mg/L TCLP NA
Grandview, Idaho. 268.40.
--------------------------------------------------------------------------------------------------------------------------------------------------------
(\1\)--A facility may certify compliance with these treatment standards according to provisions in 40 CFR 268.7.
(\2\)--Cyanide Wastewater Standards for F006 are based on analysis of composite samples.
(\3\)--These facilities must comply with 0.86 mg/l for amenable cyanides in the wastewater exiting the alkaline chlorination system. These facilities
must also comply with 40 CFR Sec. 268.7.a.4 for appropriate monitoring frequency consistent with the facilities' waste analysis plan.
(\4\)--Cyanide nonwastewaters are analyzed using SW-846 Method 9010 or 9012, sample size 10 grams, distillation time, 1 hour and 15 minutes.
(\5\)--Alternative D010 selenium standard only applies to dry scrubber solid from glass manufacturing wastes.
(\6\)--Alternative D010 selenium standard only applies to electrostatic precipitator dust generated during glass manufacturing operations.
(\7\)--D010 wastes generated by these two facilities are subject to the following conditions: (a) the wastes must be treated by Chemical Waste
Management, Inc. at their Kettleman Hills facility in Kettleman City, California; and (b) this treatment variance will be valid until May 11, 2002.
\9\ This treatment standard applies only to K088-derived bag house dust, incinerator ash, and filtercake at this facility.
\10\ This treatment standard applies only to K088-derived air emission control dust generated by this facility.
Note: NA means Not Applicable.
[51 FR 40642, Nov. 7, 1986, as amended at 52 FR 21017, June 4, 1987; 53
FR 31221, Aug. 17, 1988; 54 FR 36972, Sept. 6, 1989; 56 FR 12355, Mar.
25, 1991; 61 FR 55727, Oct. 28, 1996; 62 FR 26025, May 12, 1997; 62 FR
64509, Dec. 5, 1997; 63 FR 28738, May 26, 1998; 64 FR 28391, May 26,
1999; 66 FR 33890, June 26, 2001; 67 FR 35928, May 22, 2002]
[[Page 239]]
Effective Date Note: At 67 FR 36818, May 28, 2002, in Sec. 268.44,
the table in paragraph (o) is amended by removing the entry for ``Ball
Foster Glass Container Corp, El Monte, CA''; adding in alphabetical
order a new entry for ``St. Gobain Containers, El Monte, CA''; and
revising footnote 7, effective July 12, 2002. For the convenience of the
user, the added and revised text is set forth as follows:
Sec. 268.44 Variance from a treatment standard.
* * * * *
(o) * * *
[[Page 240]]
Table--Wastes Excluded From the Treatment Standards Under Sec. 268.40
--------------------------------------------------------------------------------------------------------------------------------------------------------
Wastewaters Nonwastewaters
Regulated hazardous ---------------------------------------------------
Facility name \(1)\ and address Waste code See also constituent Concentration Concentration
(mg/L) Notes (mg/kg) Notes
--------------------------------------------------------------------------------------------------------------------------------------------------------
* * * * * * *
St. Gobain Containers, El Monte, D010 Standards under Sec. Selenium............. NA NA 25 NA
CA \(6)\ \(7)\. 268.40.
--------------------------------------------------------------------------------------------------------------------------------------------------------
\(1)\ A facility may certify compliance with these treatment standards according to provisions in 40 CFR 268.7.
* * * * * * *
\(6)\ Alternative D010 selenium standard only applies to dry scrubber solid from glass manufacturing wastes.
\(7)\ D010 wastes generated by these two facilities are subject to the following conditions: (a) the wastes must be treated by Chemical Waste
Management, Inc. at their Kettleman Hills facility in Kettleman City, California; and (b) this treatment variance will be valid until July 12, 2005.
Note: NA means Not Applicable.
[[Page 241]]
Sec. 268.45 Treatment standards for hazardous debris.
(a) Treatment standards. Hazardous debris must be treated prior to
land disposal as follows unless EPA determines under Sec. 261.3(f)(2) of
this chapter that the debris is no longer contaminated with hazardous
waste or the debris is treated to the waste-specific treatment standard
provided in this subpart for the waste contaminating the debris:
(1) General. Hazardous debris must be treated for each ``contaminant
subject to treatment'' defined by paragraph (b) of this section using
the technology or technologies identified in Table 1 of this section.
(2) Characteristic debris. Hazardous debris that exhibits the
characteristic of ignitability, corrosivity, or reactivity identified
under Secs. 261.21, 261.22, and 261.23 of this chapter, respectively,
must be deactivated by treatment using one of the technologies
identified in Table 1 of this section.
(3) Mixtures of debris types. The treatment standards of Table 1 in
this section must be achieved for each type of debris contained in a
mixture of debris types. If an immobilization technology is used in a
treatment train, it must be the last treatment technology used.
(4) Mixtures of contaminant types. Debris that is contaminated with
two or more contaminants subject to treatment identified under paragraph
(b) of this section must be treated for each contaminant using one or
more treatment technologies identified in Table 1 of this section. If an
immobilization technology is used in a treatment train, it must be the
last treatment technology used.
(5) Waste PCBs. Hazardous debris that is also a waste PCB under 40
CFR part 761 is subject to the requirements of either 40 CFR part 761 or
the requirements of this section, whichever are more stringent.
(b) Contaminants subject to treatment. Hazardous debris must be
treated for each ``contaminant subject to treatment.'' The contaminants
subject to treatment must be determined as follows:
(1) Toxicity characteristic debris. The contaminants subject to
treatment for debris that exhibits the Toxicity Characteristic (TC) by
Sec. 261.24 of this chapter are those EP constituents for which the
debris exhibits the TC toxicity characteristic.
(2) Debris contaminated with listed waste. The contaminants subject
to treatment for debris that is contaminated with a prohibited listed
hazardous waste are those constituents or wastes for which treatment
standards are established for the waste under Sec. 268.40.
(3) Cyanide reactive debris. Hazardous debris that is reactive
because of cyanide must be treated for cyanide.
(c) Conditioned exclusion of treated debris. Hazardous debris that
has been treated using one of the specified extraction or destruction
technologies in Table 1 of this section and that does not exhibit a
characteristic of hazardous waste identified under subpart C, part 261,
of this chapter after treatment is not a hazardous waste and need not be
managed in a subtitle C facility. Hazardous debris contaminated with a
listed waste that is treated by an immobilization technology specified
in Table 1 is a hazardous waste and must be managed in a subtitle C
facility.
(d) Treatment residuals--(1) General requirements. Except as
provided by paragraphs (d)(2) and (d)(4) of this section:
(i) Residue from the treatment of hazardous debris must be separated
from the treated debris using simple physical or mechanical means; and
(ii) Residue from the treatment of hazardous debris is subject to
the waste-specific treatment standards provided by subpart D of this
part for the waste contaminating the debris.
(2) Nontoxic debris. Residue from the deactivation of ignitable,
corrosive, or reactive characteristic hazardous debris (other than
cyanide-reactive) that is not contaminated with a contaminant subject to
treatment defined by paragraph (b) of this section, must be deactivated
prior to land disposal and is not subject to the waste-specific
treatment standards of subpart D of this part.
(3) Cyanide-reactive debris. Residue from the treatment of debris
that is reactive because of cyanide must meet the treatment standards
for D003 in ``Treatment Standards for Hazardous Wastes'' at Sec. 268.40.
[[Page 242]]
(4) Ignitable nonwastewater residue. Ignitable nonwastewaster
residue containing equal to or greater than 10% total organic carbon is
subject to the technology specified in the treatment standard for D001:
Ignitable Liquids.
(5) Residue from spalling. Layers of debris removed by spalling are
hazardous debris that remain subject to the treatment standards of this
section.
Table 1--Alternative Treatment Standards For Hazardous Debris \1\
------------------------------------------------------------------------
Performance and/or
Technology description design and operating Contaminant
standard restrictions \2\
------------------------------------------------------------------------
A. Extraction Technologies:
1. Physical Extraction
a. Abrasive Blasting: Glass, Metal, All Debris: None.
Removal of contaminated Plastic, Rubber:
debris surface layers Treatment to a
using water and/or air clean debris
pressure to propel a surface.\3\.
solid media (e.g., steel Brick, Cloth,
shot, aluminum oxide Concrete, Paper,
grit, plastic beads). Pavement, Rock,
Wood: Removal of at
least 0.6 cm of the
surface layer;
treatment to a
clean debris
surface.\3\.
b. Scarification, Same as above....... Same as above.
Grinding, and Planing:
Process utilizing
striking piston heads,
saws, or rotating
grinding wheels such that
contaminated debris
surface layers are
removed.
c. Spalling: Drilling or Same as above....... Same as above.
chipping holes at
appropriate locations and
depth in the contaminated
debris surface and
applying a tool which
exerts a force on the
sides of those holes such
that the surface layer is
removed. The surface
layer removed remains
hazardous debris subject
to the debris treatment
standards.
d. Vibratory Finishing: Same as above....... Same as above.
Process utilizing
scrubbing media, flushing
fluid, and oscillating
energy such that
hazardous contaminants or
contaminated debris
surface layers are
removed.\4\
e. High Pressure Steam and Same as above....... Same as above.
Water Sprays: Application
of water or steam sprays
of sufficient
temperature, pressure,
residence time,
agitation, surfactants,
and detergents to remove
hazardous contaminants
from debris surfaces or
to remove contaminated
debris surface layers.
2. Chemical Extraction
a. Water Washing and All Debris: Brick, Cloth,
Spraying: Application of Treatment to a Concrete, Paper,
water sprays or water clean debris Pavement, Rock,
baths of sufficient surface \3\; Wood: Contaminant
temperature, pressure, Brick, Cloth, must be soluble to
residence time, Concrete, Paper, at least 5% by
agitation, surfactants, Pavement, Rock, weight in water
acids, bases, and Wood: Debris must solution or 5% by
detergents to remove be no more than 1.2 weight in emulsion;
hazardous contaminants cm (\1/2\ inch) in if debris is
from debris surfaces and one dimension contaminated with a
surface pores or to (i.e., thickness dioxin-listed
remove contaminated limit,\5\ except waste,\6\ an
debris surface layers. that this thickness ``Equivalent
limit may be waived Technology''
under an approval under Sec.
``Equivalent 268.42(b) must be
Technology'' obtained.\8\
approval under Sec.
268.42(b);\8\
debris surfaces
must be in contact
with water solution
for at least 15
minutes.
b. Liquid Phase Solvent Same as above....... Brick, Cloth,
Extraction: Removal of Concrete, Paper,
hazardous contaminants Pavement, Rock,
from debris surfaces and Wood: Same as
surface pores by applying above, except that
a nonaqueous liquid or contaminant must be
liquid solution which soluble to at least
causes the hazardous 5% by weight in the
contaminants to enter the solvent.
liquid phase and be
flushed away from the
debris along with the
liquid or liquid solution
while using appropriate
agitation, temperature,
and residence time.\4\
[[Page 243]]
c. Vapor Phase Solvent Same as above, Same as above.
Extraction: Application except that brick,
of an organic vapor using cloth, concrete,
sufficient agitation, paper, pavement,
residence time, and rock and wood
temperature to cause surfaces must be in
hazardous contaminants on contact with the
contaminated debris organic vapor for
surfaces and surface at least 60 minutes.
pores to enter the vapor
phase and be flushed away
with the organic
vapor.\4\
3. Thermal Extraction
a. High Temperature Metals For refining Debris contaminated
Recovery: Application of furnaces, treated with a dioxin-
sufficient heat, debris must be listed waste:\5\
residence time, mixing, separated from Obtain an
fluxing agents, and/or treatment residuals ``Equivalent
carbon in a smelting, using simple Technology''
melting, or refining physical or approval under Sec.
furnace to separate mechanical 268.42(b).\8\
metals from debris. means,\9\ and,
prior to further
treatment, such
residuals must meet
the waste-specific
treatment standards
for organic
compounds in the
waste contaminating
the debris.
b. Thermal Desorption: All Debris: Obtain All Debris: Metals
Heating in an enclosed an ``Equivalent other than mercury.
chamber under either Technology''
oxidizing or nonoxidizing approval under Sec.
atmospheres at sufficient 268.42(b);\8\
temperature and residence treated debris must
time to vaporize be separated from
hazardous contaminants treatment residuals
from contaminated using simple
surfaces and surface physical or
pores and to remove the mechanical
contaminants from the means,\9\ and,
heating chamber in a prior to further
gaseous exhaust gas.\7\ treatment, such
residue must meet
the waste-specific
treatment standards
for organic
compounds in the
waste contaminating
the debris.
Brick, Cloth,
Concrete, Paper,
Pavement, Rock,
Wood: Debris must
be no more than 10
cm (4 inches) in
one dimension
(i.e., thickness
limit),\5\ except
that this thickness
limit may be waived
under the
``Equivalent
Technology''
approval.
B. Destruction Technologies:
1. Biological Destruction All Debris: Obtain All Debris: Metal
(Biodegradation): Removal an ``Equivalent contaminants.
of hazardous contaminants Technology''
from debris surfaces and approval under Sec.
surface pores in an 268.42(b);\8\
aqueous solution and treated debris must
biodegration of organic be separated from
or nonmetallic inorganic treatment residuals
compounds (i.e., using simple
inorganics that contain physical or
phosphorus, nitrogen, or mechanical
sulfur) in units operated means,\9\ and,
under either aerobic or prior to further
anaerobic conditions. treatment, such
residue must meet
the waste-specific
treatment standards
for organic
compounds in the
waste contaminating
the debris.
Brick, Cloth,
Concrete, Paper,
Pavement, Rock,
Wood: Debris must
be no more than 1.2
cm (\1/2\ inch) in
one dimension
(i.e., thickness
limit),\5\ except
that this thickness
limit may be waived
under the
``Equivalent
Technology''
approval.
2. Chemical Destruction
a. Chemical Oxidation: All Debris: Obtain All Debris: Metal
Chemical or electolytic an ``Equivalent contaminants.
oxidation utilizing the Technology''
following oxidation approval under Sec.
reagents (or waste 268.42(b);\8\
reagents) or combination treated debris must
of reagents--(1) be separated from
hypochlorite (e.g., treatment residuals
bleach); (2) chlorine; using simple
(3) chlorine dioxide; (4) physical or
ozone or UV (ultraviolet mechanical
light) assisted ozone; means,\9\ and,
(5) peroxides; (6) prior to further
persulfates; (7) treatment, such
perchlorates; (8) perman- residue must meet
ganates; and/or (9) other the waste-specific
oxidizing reagents of treatment standards
equivalent destruction for organic
efficiency.\4\ Chemical compounds in the
oxidation specifically waste contaminating
includes what is referred the debris.
to as alkaline Brick, Cloth,
chlorination. Concrete, Paper,
Pavement, Rock,
Wood: Debris must
be no more than 1.2
cm (\1/2\ inch) in
one dimension
(i.e., thickness
limit),\5\ except
that this thickness
limit may be waived
under the
``Equivalent
Technology''
approval.
[[Page 244]]
b. Chemical Reduction: Same as above....... Same as above.
Chemical reaction
utilizing the following
reducing reagents (or
waste reagents) or
combination of reagents:
(1) sulfur dioxide; (2)
sodium, potassium, or
alkali salts of sulfites,
bisulfites, and
metabisulfites, and
polyethylene glycols
(e.g., NaPEG and KPEG);
(3) sodium hydrosulfide;
(4) ferrous salts; and/or
(5) other reducing
reagents of equivalent
efficiency.\4\
3. Thermal Destruction: Treated debris must Brick, Concrete,
Treatment in an be separated from Glass, Metal,
incinerator operating in treatment residuals Pavement, Rock,
accordance with Subpart O using simple Metal: Metals other
of Parts 264 or 265 of physical or than mercury,
this chapter; a boiler or mechanical except that there
industrial furnace means,\9\ and, are no metal
operating in accordance prior to further restrictions for
with Subpart H of Part treatment, such vitrification.
266 of this chapter, or residue must meet Debris contaminated
other thermal treatment the waste-specific with a dioxin-
unit operated in treatment standards listed waste.\6\
accordance with Subpart for organic Obtain an
X, Part 264 of this compounds in the ``Equivalent
chapter, or Subpart P, waste contaminating Technology''
Part 265 of this chapter, the debris. approval under Sec.
but excluding for 268.42(b),\8\
purposes of these debris except that this
treatment standards requirement does
Thermal Desorption units. not apply to
vitrification.
C. Immobilization
Technologies:
1. Macroencapsulation: Encapsulating None.
Application of surface material must
coating materials such as completely
polymeric organics (e.g., encapsulate debris
resins and plastics) or and be resistant to
use of a jacket of inert degradation by the
inorganic materials to debris and its
substantially reduce contaminants and
surface exposure to materials into
potential leaching media. which it may come
into contact after
placement
(leachate, other
waste, microbes).
2. Microencapsulation: Leachability of the None.
Stabilization of the hazardous
debris with the following contaminants must
reagents (or waste be reduced.
reagents) such that the
leachability of the
hazardous contaminants is
reduced: (1) Portland
cement; or (2) lime/
pozzolans (e.g., fly ash
and cement kiln dust).
Reagents (e.g., iron
salts, silicates, and
clays) may be added to
enhance the set/cure time
and/or compressive
strength, or to reduce
the leachability of the
hazardous
constituents.\5\
3. Sealing: Application of Sealing must avoid None.
an appropriate material exposure of the
which adheres tightly to debris surface to
the debris surface to potential leaching
avoid exposure of the media and sealant
surface to potential must be resistent
leaching media. When to degradation by
necessary to effectively the debris and its
seal the surface, sealing contaminants and
entails pretreatment of materials into
the debris surface to which it may come
remove foreign matter and into contact after
to clean and roughen the placement
surface. Sealing (leachate, other
materials include epoxy, waste, microbes).
silicone, and urethane
compounds, but paint may
not be used as a sealant.
------------------------------------------------------------------------
\1\ Hazardous debris must be treated by either these standards or the
waste-specific treatment standards for the waste contaminating the
debris. The treatment standards must be met for each type of debris
contained in a mixture of debris types, unless the debris is converted
into treatment residue as a result of the treatment process. Debris
treatment residuals are subject to the waste-specific treatment
standards for the waste contaminating the debris.
\2\ Contaminant restriction means that the technology is not BDAT for
that contaminant. If debris containing a restricted contaminant is
treated by the technology, the contaminant must be subsequently
treated by a technology for which it is not restricted in order to be
land disposed (and excluded from Subtitle C regulation).
\3\ ``Clean debris surface'' means the surface, when viewed without
magnification, shall be free of all visible contaminated soil and
hazardous waste except that residual staining from soil and waste
consisting of light shadows, slight streaks, or minor discolorations,
and soil and waste in cracks, crevices, and pits may be present
provided that such staining and waste and soil in cracks, crevices,
and pits shall be limited to no more than 5% of each square inch of
surface area.
[[Page 245]]
\4\ Acids, solvents, and chemical reagents may react with some debris
and contaminants to form hazardous compounds. For example, acid
washing of cyanide-contaminated debris could result in the formation
of hydrogen cyanide. Some acids may also react violently with some
debris and contaminants, depending on the concentration of the acid
and the type of debris and contaminants. Debris treaters should refer
to the safety precautions specified in Material Safety Data Sheets for
various acids to avoid applying an incompatible acid to a particular
debris/contaminant combination. For example, concentrated sulfuric
acid may react violently with certain organic compounds, such as
acrylonitrile.
\5\ If reducing the particle size of debris to meet the treatment
standards results in material that no longer meets the 60 mm minimum
particle size limit for debris, such material is subject to the waste-
specific treatment standards for the waste contaminating the material,
unless the debris has been cleaned and separated from contaminated
soil and waste prior to size reduction. At a minimum, simple physical
or mechanical means must be used to provide such cleaning and
separation of nondebris materials to ensure that the debris surface is
free of caked soil, waste, or other nondebris material.
\6\ Dioxin-listed wastes are EPA Hazardous Waste numbers FO20, FO21,
FO22, FO23, FO26, and FO27.
\7\ Thermal desorption is distinguished from Thermal Destruction in that
the primary purpose of Thermal Desorption is to volatilize
contaminants and to remove them from the treatment chamber for
subsequent destruction or other treatment.
\8\ The demonstration ``Equivalent Technology'' under Sec. 268.42(b)
must document that the technology treats contaminants subject to
treatment to a level equivalent to that required by the performance
and design and operating standards for other technologies in this
table such that residual levels of hazardous contaminants will not
pose a hazard to human health and the environment absent management
controls.
\9\ Any soil, waste, and other nondebris material that remains on the
debris surface (or remains mixed with the debris) after treatment is
considered a treatment residual that must be separated from the debris
using, at a minimum, simple physical or mechanical means. Examples of
simple physical or mechanical means are vibratory or trommel screening
or water washing. The debris surface need not be cleaned to a ``clean
debris surface'' as defined in note 3 when separating treated debris
from residue; rather, the surface must be free of caked soil, waste,
or other nondebris material. Treatment residuals are subject to the
waste-specific treatment standards for the waste contaminating the
debris.
[57 FR 37277, Aug. 18, 1992, as amended at 59 FR 48103, Sept. 19, 1994;
63 FR 28738, May 26, 1998]
Sec. 268.46 Alternative treatment standards based on HTMR.
For the treatment standards previously found in this section, refer
to Sec. 268.40.
[59 FR 48103, Sept. 19, 1994]
Sec. 268.48 Universal treatment standards.
(a) Table UTS identifies the hazardous constituents, along with the
nonwastewater and wastewater treatment standard levels, that are used to
regulate most prohibited hazardous wastes with numerical limits. For
determining compliance with treatment standards for underlying hazardous
constituents as defined in Sec. 268.2(i), these treatment standards may
not be exceeded. Compliance with these treatment standards is measured
by an analysis of grab samples, unless otherwise noted in the following
Table UTS.
Universal Treatment Standards
[Note: NA means not applicable]
------------------------------------------------------------------------
Wastewater Nonwastewater
standard standard
Regulated ------------------------------------
constituent CAS \1\ number Concentration in
common name Concentration in mg/kg\3\ unless
mg/l\2\ noted as ``mg/l
TCLP''
------------------------------------------------------------------------
Organic
Constituents
------------------
Acenaphthylene 208-96-8 0.059 3.4
------------------
Acenaphthene 83-32-9 0.059 3.4
------------------
Acetone 67-64-1 0.28 160
------------------
Acetonitrile 75-05-8 5.6 38
------------------
Acetophenone 96-86-2 0.010 9.7
------------------
2- 53-96-3 0.059 140
Acetylaminofluor
ene
------------------
Acrolein 107-02-8 0.29 NA
------------------
Acrylamide 79-06-1 19 23
------------------
Acrylonitrile 107-13-1 0.24 84
------------------
Aldicarb sulfone 1646-88-4 0.056 0.28
\6\
------------------
[[Page 246]]
Aldrin 309-00-2 0.021 0.066
------------------
4-Aminobiphenyl 92-67-1 0.13 NA
------------------
Aniline 62-53-3 0.81 14
------------------
Anthracene 120-12-7 0.059 3.4
------------------
Aramite 140-57-8 0.36 NA
------------------
alpha-BHC 319-84-6 0.00014 0.066
------------------
beta-BHC 319-85-7 0.00014 0.066
------------------
delta-BHC 319-86-8 0.023 0.066
------------------
gamma-BHC 58-89-9 0.0017 0.066
------------------
Barban \6\ 101-27-9 0.056 1.4
------------------
Bendiocarb \6\ 22781-23-3 0.056 1.4
------------------
Benomyl \6\ 17804-35-2 0.056 1.4
------------------
Benzene 71-43-2 0.14 10
------------------
Benz(a)anthracene 56-55-3 0.059 3.4
------------------
Benzal chloride 98-87-3 0.055 6.0
------------------
Benzo(b)fluoranth 205-99-2 0.11 6.8
ene (difficult
to distinguish
from
benzo(k)fluorant
hene)
------------------
Benzo(k)fluoranth 207-08-9 0.11 6.8
ene (difficult
to distinguish
from
benzo(b)fluorant
hene)
------------------
Benzo(g,h,i)peryl 191-24-2 0.0055 1.8
ene
------------------
Benzo(a)pyrene 50-32-8 0.061 3.4
------------------
Bromodichlorometh 75-27-4 0.35 15
ane
------------------
Bromomethane/ 74-83-9 0.11 15
Methyl bromide
------------------
4-Bromophenyl 101-55-3 0.055 15
phenyl ether
------------------
n-Butyl alcohol 71-36-3 5.6 2.6
------------------
Butylate \6\ 2008-41-5 0.042 1.4
------------------
Butyl benzyl 85-68-7 0.017 28
phthalate
------------------
2-sec-Butyl-4,6- 88-85-7 0.066 2.5
dinitrophenol/
Dinoseb
------------------
Carbaryl \6\ 63-25-2 0.006 0.14
------------------
Carbenzadim \6\ 10605-21-7 0.056 1.4
------------------
Carbofuran \6\ 1563-66-2 0.006 0.14
------------------
Carbofuran phenol 1563-38-8 0.056 1.4
\6\
------------------
Carbon disulfide 75-15-0 3.8 4.8 mg/l TCLP
------------------
Carbon 56-23-5 0.057 6.0
tetrachloride
------------------
Carbosulfan \6\ 55285-14-8 0.028 1.4
------------------
Chlordane (alpha 57-74-9 0.0033 0.26
and gamma
isomers)
------------------
[[Page 247]]
p-Chloroaniline 106-47-8 0.46 16
------------------
Chlorobenzene 108-90-7 0.057 6.0
------------------
Chlorobenzilate 510-15-6 0.10 NA
------------------
2-Chloro-1,3- 126-99-8 0.057 0.28
butadiene
------------------
Chlorodibromometh 124-48-1 0.057 15
ane
------------------
Chloroethane 75-00-3 0.27 6.0
------------------
bis(2- 111-91-1 0.036 7.2
Chloroethoxy)met
hane
------------------
bis(2- 111-44-4 0.033 6.0
Chloroethyl)ethe
r
------------------
Chloroform 67-66-3 0.046 6.0
------------------
bis(2- 39638-32-9 0.055 7.2
Chloroisopropyl)
ether
------------------
p-Chloro-m-cresol 59-50-7 0.018 14
------------------
2-Chloroethyl 110-75-8 0.062 NA
vinyl ether
------------------
Chloromethane/ 74-87-3 0.19 30
Methyl chloride
------------------
2- 91-58-7 0.055 5.6
Chloronaphthalen
e
------------------
2-Chloropchenol 95-57-8 0.044 5.7
------------------
3-Chloropropylene 107-05-1 0.036 30
------------------
Chrysene 218-01-9 0.059 3.4
------------------
o-Cresol 95-48-7 0.11 5.6
------------------
m-Cresol 108-39-4 0.77 5.6
(difficult to
distinguish from
p-cresol)
------------------
p-Cresol 106-44-5 0.77 5.6
(difficult to
distinguish from
m-cresol)
------------------
m-Cumenyl 64-00-6 0.056 1.4
methylcarbamate
\6\
------------------
Cyclohexanone 108-94-1 0.36 0.75 mg/l TCLP
------------------
o,p'-DDD 53-19-0 0.023 0.087
------------------
p,p'-DDD 72-54-8 0.023 0.087
------------------
o,p'-DDE 3424-82-6 0.031 0.087
------------------
p,p'-DDE 72-55-9 0.031 0.087
------------------
o,p'-DDT 789-02-6 0.0039 0.087
------------------
p,p'-DDT 50-29-3 0.0039 0.087
------------------
Dibenz(a,h)anthra 53-70-3 0.055 8.2
cene
------------------
Dibenz(a,e)pyrene 192-65-4 0.061 NA
------------------
1,2-Dibromo-3- 96-12-8 0.11 15
chloropropane
------------------
1,2-Dibromoethane/ 106-93-4 0.028 15
Ethylene
dibromide
------------------
Dibromomethane 74-95-3 0.11 15
------------------
m-Dichlorobenzene 541-73-1 0.036 6.0
------------------
[[Page 248]]
o-Dichlorobenzene 95-50-1 0.088 6.0
------------------
p-Dichlorobenzene 106-46-7 0.090 6.0
------------------
Dichlorodifluorom 75-71-8 0.23 7.2
ethane
------------------
1,1- 75-34-3 0.059 6.0
Dichloroethane
------------------
1,2- 107-06-2 0.21 6.0
Dichloroethane
------------------
1,1- 75-35-4 0.025 6.0
Dichloroethylene
------------------
trans-1,2- 156-60-5 0.054 30
Dichloroethylene
------------------
2,4- 120-83-2 0.044 14
Dichlorophenol
------------------
2,6- 87-65-0 0.044 14
Dichlorophenol
------------------
2,4- 94-75-7 0.72 10
Dichlorophenoxya
cetic acid/2,4-D
------------------
1,2- 78-87-5 0.85 18
Dichloropropane
------------------
cis-1,3- 10061-01-5 0.036 18
Dichloropropylen
e
------------------
trans-1,3- 10061-02-6 0.036 18
Dichloropropylen
e
------------------
Dieldrin 60-57-1 0.017 0.13
------------------
Diethyl phthalate 84-66-2 0.20 28
------------------
p- 60-11-7 0.13 NA
Dimethylaminoazo
benzene
------------------
2,4-Dimethyl 105-67-9 0.036 14
phenol
------------------
Dimethyl 131-11-3 0.047 28
phthalate
------------------
Di-n-butyl 84-74-2 0.057 28
phthalate
------------------
1,4- 100-25-4 0.32 2.3
Dinitrobenzene
------------------
4,6-Dinitro-o- 534-52-1 0.28 160
cresol
------------------
2,4-Dinitrophenol 51-28-5 0.12 160
------------------
2,4- 121-14-2 0.32 140
Dinitrotoluene
------------------
2,6- 606-20-2 0.55 28
Dinitrotoluene
------------------
Di-n-octyl 117-84-0 0.017 28
phthalate
------------------
Di-n- 621-64-7 0.40 14
propylnitrosamin
e
------------------
1,4-Dioxane 123-91-1 12.0 170
------------------
Diphenylamine 122-39-4 0.92 13
(difficult to
distinguish from
diphenylnitrosam
ine)
------------------
Diphenylnitrosami 86-30-6 0.92 13
ne (difficult to
distinguish from
diphenylamine)
------------------
1,2- 122-66-7 0.087 NA
Diphenylhydrazin
e
------------------
Disulfoton 298-04-4 0.017 6.2
------------------
Dithiocarbamates NA 0.028 28
(total) \6\
------------------
Endosulfan I 959-98-8 0.023 0.066
------------------
Endosulfan II 33213-65-9 0.029 0.13
------------------
[[Page 249]]
Endosulfan 1031-07-8 0.029 0.13
sulfate
------------------
Endrin 72-20-8 0.0028 0.13
------------------
Endrin aldehyde 7421-93-4 0.025 0.13
------------------
EPTC \6\ 759-94-4 0.042 1.4
------------------
Ethyl acetate 141-78-6 0.34 33
------------------
Ethyl benzene 100-41-4 0.057 10
------------------
Ethyl cyanide/ 107-12-0 0.24 360
Propanenitrile
------------------
Ethyl ether 60-29-7 0.12 160
------------------
Ethyl 97-63-2 0.14 160
methacrylate
------------------
Ethylene oxide 75-21-8 0.12 NA
------------------
Famphur 52-85-7 0.017 15
------------------
Fluoranthene 206-44-0 0.068 3.4
------------------
Fluorene 86-73-7 0.059 3.4
------------------
Formetanate 23422-53-9 0.056 1.4
hydrochloride \6
\
------------------
Heptachlor 76-44-8 0.0012 0.066
------------------
1,2,3,4,6,7,8- 35822-46-9 0.000035 .0025
Heptachlorodiben
zo-p-dioxin
(1,2,3,4,6,7,8-
HpCDD)
------------------
1,2,3,4,6,7,8- 67562-39-5 0.000035 .0025
Heptachlorodiben
zofluran
(1,2,3,4,6,7,8-
HpCDF)
------------------
1,2,3,4,6,7,8- 55673-89-7 0.000035 .0025
Heptachlorodiben
zofluran
(1,2,3,4,7,8,9-
HpCDF)
------------------
Heptachlor 1024-57-3 0.016 0.066
epoxide
------------------
Hexachlorobenzene 118-74-1 0.055 10
------------------
Hexachlorobutadie 87-68-3 0.055 5.6
ne
------------------
Hexachlorocyclope 77-47-4 0.057 2.4
ntadiene
------------------
HxCDDs (All NA 0.000063 0.001
Hexachlorodibenz
o-p-dioxins)
------------------
HxCDFs (All NA 0.000063 0.001
Hexachlorodibenz
ofurans)
------------------
Hexachloroethane 67-72-1 0.055 30
------------------
Indeno(1,2,3-c,d) 193-39-5 0.0055 3.4
pyrene
------------------
Iodomethane 74-88-4 0.19 65
------------------
Isobutyl alcohol 78-83-1 5.6 170
------------------
Isodrin 465-73-6 0.021 0.066
------------------
Isosafrole 120-58-1 0.081 2.6
------------------
Kepone 143-50-0 0.0011 0.13
------------------
Methacrylonitrile 126-98-7 0.24 84
------------------
Methanol 67-56-1 5.6 0.75 mg/l TCLP
------------------
Methapyrilene 91-80-5 0.081 1.5
------------------
[[Page 250]]
Methiocarb \6\ 2032-65-7 0.056 1.4
------------------
Methomyl \6\ 16752-77-5 0.028 0.14
------------------
Methoxychlor 72-43-5 0.25 0.18
------------------
3- 56-49-5 0.0055 15
Methylcholanthre
ne
------------------
4,4-Methylene 101-14-4 0.50 30
bis(2-
chloroaniline)
------------------
Methylene 75-09-2 0.089 30
chloride
------------------
Methyl ethyl 78-93-3 0.28 36
ketone
------------------
Methyl isobutyl 108-10-1 0.14 33
ketone
------------------
Methyl 80-62-6 0.14 160
methacrylate
------------------
Methyl 66-27-3 0.018 NA
methanesulfonate
------------------
Methyl parathion 298-00-0 0.014 4.6
------------------
Metolcarb \6\ 1129-41-5 0.056 1.4
------------------
Mexacarbate \6\ 315-18-4 0.056 1.4
------------------
Molinate \6\ 2212-67-1 0.042 1.4
------------------
Naphthalene 91-20-3 0.059 5.6
------------------
2-Naphthylamine 91-59-8 0.52 NA
------------------
o-Nitroaniline 88-74-4 0.27 14
------------------
p-Nitroaniline 100-01-6 0.028 28
------------------
Nitrobenzene 98-95-3 0.068 14
------------------
5-Nitro-o- 99-55-8 0.32 28
toluidine
------------------
o-Nitrophenol 88-75-5 0.028 13
------------------
p-Nitrophenol 100-02-7 0.12 29
------------------
N- 55-18-5 0.40 28
Nitrosodiethylam
ine
------------------
N- 62-75-9 0.40 2.3
Nitrosodimethyla
mine
------------------
N-Nitroso-di-n- 924-16-3 0.40 17
butylamine
------------------
N- 10595-95-6 0.40 2.3
Nitrosomethyleth
ylamine
------------------
N- 59-89-2 0.40 2.3
Nitrosomorpholin
e
------------------
N- 100-75-4 0.013 35
Nitrosopiperidin
e
------------------
N- 930-55-2 0.013 35
Nitrosopyrrolidi
ne
------------------
1,2,3,4,6,7,8,9- 3268-87-9 0.000063 0.005
Octachlorodibenz
o-p-dioxin
(OCDD)
------------------
1,2,3,4,6,7,8,9- 39001-02-0 0.000063 0.005
Octachlorodibenz
ofluran (OCDF)
------------------
Oxamyl \6\ 23135-22-0 0.056 0.28
------------------
Parathion 56-38-2 0.014 4.6
------------------
Total PCBs (sum 1336-36-3 0.10 10
of all PCB
isomers, or all
Aroclors)\8\
------------------
[[Page 251]]
Pebulate \6\ 1114-71-2 0.042 1.4
------------------
Pentachlorobenzen 608-93-5 0.055 10
e
------------------
PeCDDs (All NA 0.000063 0.001
Pentachlorodiben
zo-p-dioxins)
------------------
PeCDFs (All NA 0.000035 0.001
Pentachlorodiben
zofurans)
------------------
Pentachloroethane 76-01-7 0.055 6.0
------------------
Pentachloronitrob 82-68-8 0.055 4.8
enzene
------------------
Pentachlorophenol 87-86-5 0.089 7.4
------------------
Phenacetin 62-44-2 0.081 16
------------------
Phenanthrene 85-01-8 0.059 5.6
------------------
Phenol 108-95-2 0.039 6.2
------------------
Phorate 298-02-2 0.021 4.6
------------------
Phthalic acid 100-21-0 0.055 28
------------------
Phthalic 85-44-9 0.055 28
anhydride
------------------
Physostigmine \6\ 57-47-6 0.056 1.4
------------------
Physostigmine 57-64-7 0.056 1.4
salicylate \6\
------------------
Promecarb \6\ 2631-37-0 0.056 1.4
------------------
Pronamide 23950-58-5 0.093 1.5
------------------
Propham \6\ 122-42-9 0.056 1.4
------------------
Propoxur \6\ 114-26-1 0.056 1.4
------------------
Prosulfocarb \6\ 52888-80-9 0.042 1.4
------------------
Pyrene 129-00-0 0.067 8.2
------------------
Pyridine 110-86-1 0.014 16
------------------
Safrole 94-59-7 0.081 22
------------------
Silvex/2,4,5-TP 93-72-1 0.72 7.9
------------------
1,2,4,5- 95-94-3 0.055 14
Tetrachlorobenze
ne
------------------
TCDDs (All NA 0.000063 0.001
Tetrachlorodiben
zo-p-dioxins)
------------------
TCDFs (All NA 0.000063 0.001
Tetrachlorodiben
zofurans)
------------------
1,1,1,2- 630-20-6 0.057 6.0
Tetrachloroethan
e
------------------
1,1,2,2- 79-34-5 0.057 6.0
Tetrachloroethan
e
------------------
Tetrachloroethyle 127-18-4 0.056 6.0
ne
------------------
2,3,4,6- 58-90-2 0.030 7.4
Tetrachloropheno
l
------------------
Thiodicarb \6\ 59669-26-0 0.019 1.4
------------------
Thiophanate- 23564-05-8 0.056 1.4
methyl \6\
------------------
Toluene 108-88-3 0.080 10
------------------
[[Page 252]]
Toxaphene 8001-35-2 0.0095 2.6
------------------
Triallate \6\ 2303-17-5 0.042 1.4
------------------
Tribromomethane/ 75-25-2 0.63 15
Bromoform
------------------
1,2,4- 120-82-1 0.055 19
Trichlorobenzene
------------------
1,1,1- 71-55-6 0.054 6.0
Trichloroethane
------------------
1,1,2- 79-00-5 0.054 6.0
Trichloroethane
------------------
Trichloroethylene 79-01-6 0.054 6.0
------------------
Trichlorofluorome 75-69-4 0.020 30
thane
------------------
2,4,5- 95-95-4 0.18 7.4
Trichlorophenol
------------------
2,4,6- 88-06-2 0.035 7.4
Trichlorophenol
------------------
2,4,5- 93-76-5 0.72 7.9
Trichlorophenoxy
acetic acid/
2,4,5-T
------------------
1,2,3- 96-18-4 0.85 30
Trichloropropane
------------------
1,1,2-Trichloro- 76-13-1 0.057 30
1,2,2-
trifluoroethane
------------------
Triethylamine \6\ 121-44-8 0.081 1.5
------------------
tris-(2,3- 126-72-7 0.11 0.10
Dibromopropyl)
phosphate
------------------
Vernolate \6\ 1929-77-7 0.042 1.4
------------------
Vinyl chloride 75-01-4 0.27 6.0
------------------
Xylenes-mixed 1330-20-7 0.32 30
isomers (sum of
o-, m-, and p-
xylene
concentrations)
------------------
Inorganic
Constituents
------------------
Antimony 7440-36-0 1.9 1.15 mg/l TCLP
------------------
Arsenic 7440-38-2 1.4 5.0 mg/l TCLP
------------------
Barium 7440-39-3 1.2 21 mg/l TCLP
------------------
Beryllium 7440-41-7 0.82 1.22 mg/l TCLP
------------------
Cadmium 7440-43-9 0.69 0.11 mg/l TCLP
------------------
Chromium (Total) 7440-47-3 2.77 0.60 mg/l TCLP
------------------
Cyanides (Total) 57-12-5 1.2 590
\4\
------------------
Cyanides 57-12-5 0.86 30
(Amenable) \4\
------------------
Fluoride \5\ 16984-48-8 35 NA
------------------
Lead 7439-92-1 0.69 0.75 mg/l TCLP
------------------
Mercury-- 7439-97-6 NA 0.20 mg/l TCLP
Nonwastewater
from Retort
------------------
Mercury--All 7439-97-6 0.15 0.025 mg/l TCLP
Others
------------------
Nickel 7440-02-0 3.98 11 mg/l TCLP
------------------
Selenium \7\ 7782-49-2 0.82 5.7 mg/l TCLP
------------------
Silver 7440-22-4 0.43 0.14 mg/l TCLP
------------------
[[Page 253]]
Sulfide \5\ 18496-25-8 14 NA
------------------
Thallium 7440-28-0 1.4 0.20 mg/l TCLP
------------------
Vanadium \5\ 7440-62-2 4.3 1.6 mg/l TCLP
------------------
Zinc \5\ 7440-66-6 2.61 4.3 mg/l TCLP
------------------------------------------------------------------------
FOOTNOTES TO TABLE UTS
1 CAS means Chemical Abstract Services. When the waste
code and/or regulated constituents are described as
a combination of a chemical with it's salts and/or
esters, the CAS number is given for the parent
compound only.
2 Concentration standards for wastewaters are
expressed in mg/l and are based on analysis of
composite samples.
3 Except for Metals (EP or TCLP) and Cyanides (Total
and Amenable) the nonwastewater treatment standards
expressed as a concentration were established,
inpart, based upon incineration in units operated
in accordance with the technical requirements of 40
CFR part 264, subpart O or 40 CFR part 265, subpart
O, or based upon combustion in fuel substitution
units operating in accordance with applicable
technical requirements. A facility may comply with
these treatment standards according to provisions
in 40 CFR 268.40(d). All concentration standards
for nonwastewaters are based on analysis of grab
samples.
4 Both Cyanides (Total) and Cyanides (Amenable) for
nonwastewaters are to be analyzed using Method 9010
or 9012, found in ``Test Methods for Evaluating
Solid Waste, Physical/Chemical Methods,'' EPA
Publication SW-846, as incorporated by reference in
40 CFR 260.11, with a sample size of 10 grams and a
distillation time of one hour and 15 minutes.
5 These constituents are not ``underlying hazardous
constituents'' in characteristic wastes, according
to the definition at Sec. 268.2(i).
6 Between August 26, 1996, and March 4, 1998, these
constituents are not ``underlying hazardous
constituents'' as defined at Sec. 268.2(i) of this
Part.
7 This constituent is not an underlying hazardous
constituent as defined at Sec. 268.2(i) of this
Part because its UTS level is greater than its TC
level, thus a treatment selenium waste would always
be characteristically hazardous, unless it is
treated to below its characteristic level.
8 This standard is temporarily deferred for soil
exhibiting a hazardous characteristic due to D004-
D011 only.
[59 FR 48103, Sept. 19, 1994, as amended by 60 FR 302, Jan. 3, 1995; 61
FR 15654, Apr. 8 1996; 61 FR 33690, June 28, 1996; 62 FR 7596, Feb. 19,
1997; 63 FR 24626, May 4, 1998; 63 FR 28739, May 26, 1998; 63 FR 47417,
Sept. 4, 1998; 64 FR 25417, May 11, 1999; 65 FR 14475, Mar. 17, 2000]
Sec. 268.49 Alternative LDR treatment standards for contaminated soil.
(a) Applicability. You must comply with LDRs prior to placing soil
that exhibits a characteristic of hazardous waste, or exhibited a
characteristic of hazardous waste at the time it was generated, into a
land disposal unit. The following chart describes whether you must
comply with LDRs prior to placing soil contaminated by listed hazardous
waste into a land disposal unit:
[[Page 254]]
----------------------------------------------------------------------------------------------------------------
If LDRs And if LDRs And if Then you
----------------------------------------------------------------------------------------------------------------
Applied to the listed waste Apply to the .................. Must comply with LDRs
when it contaminated the soil*. listed waste now.
Didn't apply to the listed Apply to the The soil is Must comply with LDRs.
waste when it contaminated the listed waste now. determined to
soil*. contain the
listed waste when
the soil is first
generated.
Didn't apply to the listed Apply to the The soil is Needn't comply with LDRs.
waste when it contaminated the listed waste now. determined not to
soil*. contain the
listed waste when
the soil is first
generated.
Didn't apply to the listed Don't apply to the .................. Needn't comply with LDRs.
waste when it contaminated the listed waste now.
soil*.
----------------------------------------------------------------------------------------------------------------
* For dates of LDR applicability, see 40 CFR Part 268 Appendix VII. To determine the date any given listed
hazardous waste contaminated any given volume of soil, use the last date any given listed hazardous waste was
placed into any given land disposal unit or, in the case of an accidental spill, the date of the spill.
(b) Prior to land disposal, contaminated soil identified by
paragraph (a) of this section as needing to comply with LDRs must be
treated according to the applicable treatment standards specified in
paragraph (c) of this section or according to the Universal Treatment
Standards specified in 40 CFR 268.48 applicable to the contaminating
listed hazardous waste and/or the applicable characteristic of hazardous
waste if the soil is characteristic. The treatment standards specified
in paragraph (c) of this section and the Universal Treatment Standards
may be modified through a treatment variance approved in accordance with
40 CFR 268.44.
(c) Treatment standards for contaminated soils. Prior to land
disposal, contaminated soil identified by paragraph (a) of this section
as needing to comply with LDRs must be treated according to all the
standards specified in this paragraph or according to the Universal
Treatment Standards specified in 40 CFR 268.48.
(1) All soils. Prior to land disposal, all constituents subject to
treatment must be treated as follows:
(A) For non-metals except carbon disulfide, cyclohexanone, and
methanol, treatment must achieve 90 percent reduction in total
constituent concentrations, except as provided by paragraph (c)(1)(C) of
this section.
(B) For metals and carbon disulfide, cyclohexanone, and methanol,
treatment must achieve 90 percent reduction in constituent
concentrations as measured in leachate from the treated media (tested
according to the TCLP) or 90 percent reduction in total constituent
concentrations (when a metal removal treatment technology is used),
except as provided by paragraph (c)(1)(C)of this section.
(C) When treatment of any constituent subject to treatment to a 90
percent reduction standard would result in a concentration less than 10
times the Universal Treatment Standard for that constituent, treatment
to achieve constituent concentrations less than 10 times the universal
treatment standard is not required. Universal Treatment Standards are
identified in 40 CFR 268.48 Table UTS.
(2) Soils that exhibit the characteristic of ignitability,
corrosivity or reactivity. In addition to the treatment required by
paragraph (c)(1) of this section, prior to land disposal, soils that
exhibit the characteristic of ignitability, corrosivity, or reactivity
must be treated to eliminate these characteristics.
(3) Soils that contain nonanalyzable constituents. In addition to
the treatment requirements of paragraphs (c)(1) and (2) of this section,
prior to land disposal, the following treatment is required for soils
that contain nonanalyzable constituents:
(A) For soil that contains only analyzable and nonanalyzable organic
constituents, treatment of the analyzable organic constituents to the
levels specified in paragraphs (c)(1) and (2) of this section; or,
(B) For soil that contains only nonanalyzable constituents,
treatment by the method(s) specified in Sec. 268.42 for the waste
contained in the soil.
[[Page 255]]
(d) Constituents subject to treatment. When applying the soil
treatment standards in paragraph (c) of this section, constituents
subject to treatment are any constituents listed in Sec. 268.48 Table
UTS-Universal Treatment Standards that are reasonably expected to be
present in any given volume of contaminated soil, except flouride,
selenium, sulfides, vanadium, zinc, and that are present at
concentrations greater than ten times the universal treatment standard.
PCBs are not constituent subject to treatment in any given volume of
soil which exhibits the toxicity characteristic solely because of the
presence of metals.
(e) Management of treatment residuals. Treatment residuals from
treating contaminated soil identified by paragraph (a) of this section
as needing to comply with LDRs must be managed as follows:
(1) Soil residuals are subject to the treatment standards of this
section;
(2) Non-soil residuals are subject to:
(A) For soils contaminated by listed hazardous waste, the RCRA
Subtitle C standards applicable to the listed hazardous waste; and
(B) For soils that exhibit a characteristic of hazardous waste, if
the non-soil residual also exhibits a characteristic of hazardous waste,
the treatment standards applicable to the characteristic hazardous
waste.
[63 FR 28751, May 26, 1998, as amended at 64 FR 25417, May 11, 1999; 64
FR 56472, Oct. 20, 1999; 65 FR 81381, Dec. 26, 2000]
Subpart E--Prohibitions on Storage
Sec. 268.50 Prohibitions on storage of restricted wastes.
(a) Except as provided in this section, the storage of hazardous
wastes restricted from land disposal under subpart C of this part of
RCRA section 3004 is prohibited, unless the following conditions are
met:
(1) A generator stores such wastes in tanks, containers, or
containment buildings on-site solely for the purpose of the accumulation
of such quantities of hazardous waste as necessary to facilitate proper
recovery, treatment, or disposal and the generator complies with the
requirements in Sec. 262.34 and parts 264 and 265 of this chapter.
(2) An owner/operator of a hazardous waste treatment, storage, or
disposal facility stores such wastes in tanks, containers, or
containment buildings solely for the purpose of the accumulation of such
quantities of hazardous waste as necessary to facilitate proper
recovery, treatment, or disposal and:
(i) Each container is clearly marked to identify its contents and
the date each period of accumulation begins;
(ii) Each tank is clearly marked with a description of its contents,
the quantity of each hazardous waste received, and the date each period
of accumulation begins, or such information for each tank is recorded
and maintained in the operating record at that facility. Regardless of
whether the tank itself is marked, an owner/operator must comply with
the operating record requirements specified in Sec. 264.73 or
Sec. 265.73.
(3) A transporter stores manifested shipments of such wastes at a
transfer facility for 10 days or less.
(b) An owner/operator of a treatment, storage or disposal facility
may store such wastes for up to one year unless the Agency can
demonstrate that such storage was not solely for the purpose of
accumulation of such quantities of hazardous waste as are necessary to
facilitate proper recovery, treatment, or disposal.
(c) A owner/operator of a treatment, storage or disposal facility
may store such wastes beyond one year; however, the owner/operator bears
the burden of proving that such storage was solely for the purpose of
accumulation of such quantities of hazardous waste as are necessary to
facilitate proper recovery, treatment, or disposal.
(d) If a generator's waste is exempt from a prohibition on the type
of land disposal utilized for the waste (for example, because of an
approved case-by-case extension under Sec. 268.5, an approved Sec. 268.6
petition, or a national capacity variance under subpart C), the
prohibition in paragraph (a) of this section does not apply during the
period of such exemption.
(e) The prohibition in paragraph (a) of this section does not apply
to hazardous wastes that meet the treatment standards specified under
Secs. 268.41, 268.42, and 268.43 or the treatment standards specified
under the variance
[[Page 256]]
in Sec. 268.44, or, where treatment standards have not been specified,
is in compliance with the applicable prohibitions specified in
Sec. 268.32 or RCRA section 3004.
(f) Liquid hazardous wastes containing polychlorinated biphenyls
(PCBs) at concentrations greater than or equal to 50 ppm must be stored
at a facility that meets the requirements of 40 CFR 761.65(b) and must
be removed from storage and treated or disposed as required by this part
within one year of the date when such wastes are first placed into
storage. The provisions of paragraph (c) of this section do not apply to
such PCB wastes prohibited under Sec. 268.32 of this part.
(g) The prohibition and requirements in this do not apply to
hazardous remediation wastes stored in a staging pile approved pursuant
to Sec. 264.554 of this chapter.
[51 FR 40642, Nov. 7, 1986; 52 FR 21017, June 4, 1987, as amended at 52
FR 25791, July 8, 1987; 54 FR 36972, Sept. 6, 1989; 57 FR 37281, Aug.
18, 1992; 63 FR 65940, Nov. 30, 1998]
Appendixes I-II to Part 268 [Reserved]
Appendix III to Part 268--List of Halogenated Organic Compounds
Regulated Under Sec. 268.32
In determining the concentration of HOCs in a hazardous waste for
purposes of the Sec. 268.32 land disposal prohibition, EPA has defined
the HOCs that must be included in a calculation as any compounds having
a carbon-halogen bond which are listed in this Appendix (see
Sec. 268.2). Appendix III to Part 268 consists of the following
compounds:
I. Volatiles
1. Bromodichloromethane
2. Bromomethane
3. Carbon Tetrachloride
4. Chlorobenzene
5. 2-Chloro-1,3-butadiene
6. Chlorodibromomethane
7. Chloroethane
8. 2-Chloroethyl vinyl ether
9. Chloroform
10. Chloromethane
11. 3-Chloropropene
12. 1,2-Dibromo-3-chloropropane
13. 1,2-Dibromomethane
14. Dibromomethane
15. Trans-1,4-Dichloro-2--butene
16. Dichlorodifluoromethane
17. 1,1-Dichloroethane
18. 1,2-Dichloroethane
19. 1,1-Dichloroethylene
20. Trans-1,2-Dichloroethene
21. 1,2-Dichloropropane
22. Trans-1,3-Dichloropropene
23. cis-1,3-Dichloropropene
24. Iodomethane
25. Methylene chloride
26. 1,1,1,2-Tetrachloroethane
27. 1,1,2,2-Tetrachloroethane
28. Tetrachloroethene
29. Tribromomethane
30. 1,1,1-Trichloroethane
31. 1,1,2-Trichloroethane
32. Trichlorothene
33. Trichloromonofluoromethane
34. 1,2,3-Thrichloropropane
35. Vinyl Chloride
II. Semivolatiles
1. Bis(2-chloroethoxy)ethane
2. Bis(2-chloroethyl)ether
3. Bis(2-chloroisopropyl)ether
4. p-Chloroaniline
5. Chlorobenzilate
6. p-Chloro-m-cresol
7. 2-Chloronaphthalene
8. 2-Chlorphenol
9. 3-Chloropropionitrile
10. m-Dichlorobenzene
11. o-Dichlorobenzene
12. p-Dichlorobenzene
13. 3.3'-Dichlorobenzidine
14. 2,4-Dichlorophenol
15. 2,6-Dichlorophenol
16. Hexachlorobenzene
17. Hexachlorobutadiene
18. Hexachlorocyclopentadiene
19. Hexachloroethane
20. Hexachloroprophene
21. Hexachlorpropene
22. 4,4'-Methylenebis(2-chloroanaline)
23. Pentachlorobenzene
24. Pentachloroethane
25. Pentachloronitrobenzene
26. Pentachlorophenol
27. Pronamide
28. 1,2,4,5-Tetrachlorobenzene
29. 2,3,4,6-Tetrachlorophenol
30. 1,2,4-Trichlorobenzene
31. 2,4,5-Trichlorophenol
32. 2,4,6-Trichlorophenol
33. Tris(2,3-dibromopropyl)phosphate
III. Organochlorine Pesticides
1. Aldrin
2. alpha-BHC
3. beta-BHC
4. delta-BHC
5. gamma-BHC
6. Chlorodane
7. DDD
8. DDE
9. DDT
10. Dieldrin
11. Endosulfan I
12. Endosulfan II
[[Page 257]]
13. Endrin
14. Endrin aldehyde
15. Heptachlor
16. Heptachlor epoxide
17. Isodrin
18. Kepone
19. Methoxyclor
20. Toxaphene
IV. Phenoxyacetic Acid Herbicides
1. 2,4-Dichlorophenoxyacetic acid
2. Silvex
3. 2,4,5-T
V. PCBs
1. Aroclor 1016
2. Aroclor 1221
3. Aroclor 1232
4. Aroclor 1242
5. Aroclor 1248
6. Aroclor 1254
7. Aroclor 1260
8. PCBs not otherwise specified
VI. Dioxins and Furans
1. Hexachlorodibenzo-p-dioxins
2. Hexachlorodibenzofuran
3. Pentachlorodibenzo-p-dioxins
4. Pentachlorodibenzofuran
5. Tetrachlorodibenzo-p-dioxins
6. Tetrachlorodibenzofuran
7. 2,3,7,8-Tetrachlorodibenzo-p-dioxin
[65 FR 81380, Dec. 26, 2000]
Appendix IV to Part 268--Wastes Excluded From Lab Packs Under the
Alternative Treatment Standards of Sec. 268.42(c)
Hazardous waste with the following EPA Hazardous Waste Codes may not
be placed in lab packs under the alternative lab pack treatment
standards of Sec. 268.42(c): D009, F019, K003, K004, K005, K006, K062,
K071, K100, K106, P010, P011, P012, P076, P078, U134, U151.
[59 FR 48107 Sept. 19, 1994]
Appendix V to Part 268 [Reserved]
Appendix VI to Part 268--Recommended Technologies to Achieve
Deactivation of Characteristics in Section 268.42
The treatment standard for many characteristic wastes is stated in
the Sec. 268.40 Table of Treatment Standards as ``Deactivation and meet
UTS.'' EPA has determined that many technologies, when used alone or in
combination, can achieve the deactivation portion of the treatment
standard. Characteristic wastes that are not managed in a facility
regulated by the Clean Water Act (CWA) or in a CWA-equivalent facility,
and that also contain underlying hazardous constituents (see
Sec. 268.2(i)) must be treated not only by a ``deactivating'' technology
to remove the characteristic, but also to achieve the universal
treatment standards (UTS) for underlying hazardous constituents. The
following appendix presents a partial list of technologies, utilizing
the five letter technology codes established in 40 CFR 268.42 Table 1,
that may be useful in meeting the treatment standard. Use of these
specific technologies is not mandatory and does not preclude direct
reuse, recovery, and/or the use of other pretreatment technologies,
provided deactivation is achieved and underlying hazardous constituents
are treated to achieve the UTS.
------------------------------------------------------------------------
Waste code/subcategory Nonwastewaters Wastewaters
------------------------------------------------------------------------
D001 Ignitable Liquids based on RORGS................... n.a.
261.21(a)(1)--Low TOC INCIN...................
Nonwastewater Subcategory WETOX...................
(containing 1% to <10% TOC). CHOXD...................
BIODG...................
D001 Ignitable Liquids based on n.a..................... RORGS
261.21(a)(1)--Ignitable INCIN
Wastewater Subcategory WETOX
(containing <1% TOC). CHOXD
BIODG
D001 Compressed Gases based on RCGAS................... n.a.
261.21(A)(3). INCIN...................
FSUBS...................
ADGAS fb. INCIN.........
ADGAS fb. (CHOXD; or
CHRED).
D001 Ignitable Reactives based WTRRX................... n.a.
on 261.21(a)(2). CHOXD...................
CHRED...................
STABL...................
INCIN...................
D001 Ignitable Oxidizers based CHRED................... CHRED
on 261.21(a)(4). INCIN................... INCIN
[[Page 258]]
D002 Acid Subcategory based on RCORR................... NEUTR
261.22(a)(1) with pH less than NEUTR................... INCIN
or equal to 2. INCIN...................
D002 Alkaline Subcategory based NEUTR................... NEUTR
on 261.22(a)(1) with pH greater INCIN................... INCIN
than or equal to 12.5.
D002 Other Corrosives based on CHOXD................... CHOXD
261.22(a)(2). CHRED................... CHRED
INCIN................... INCIN
STABL...................
D003 Water Reactives based on INCIN................... n.a.
261.23(a) (2), (3), and (4). WTRRX...................
CHOXD...................
CHRED...................
D003 Reactive Sulfides based on CHOXD................... CHOXD
261.23(a)(5). CHRED................... CHRED
INCIN................... BIODG
STABL................... INCIN
D003 Explosives based on INCIN................... INCIN
261.23(a) (6), (7), and (8). CHOXD................... CHOXD
CHRED................... CHRED
BIODG
CARBN
D003 Other Reactives based on INCIN................... INCIN
261.23(a)(1). CHOXD................... CHOXD
CHRED................... CHRED
BIODG
CARBN
K044 Wastewater treatment CHOXD................... CHOXD
sludges from the manufacturing CHRED................... CHRED
and processing of explosives. INCIN................... BIODG
CARBN
INCIN
K045 Spent carbon from the CHOXD................... CHOXD
treatment of wastewaters CHRED................... CHRED
containing explosives. INCIN................... BIODG
CARBN
INCIN
K047 Pink/red water from TNT CHOXD................... CHOXD
operations. CHRED................... CHRED
INCIN................... BIODG
CARBN
INCIN
------------------------------------------------------------------------
Note: ``n.a.'' stands for ``not applicable''; ``fb.'' stands for
``followed by''.
[55 FR 22714, June 1, 1990, as amended at 62 FR 26025, May 12, 1997]
Appendix VII to Part 268--LDR Effective Dates of Surface
Disposed Prohibited Hazardous Wastes
Table 1--Effective Dates of Surface Disposed Wastes (Non-Soil and Debris) Regulated in the LDRS a--Comprehensive
List
----------------------------------------------------------------------------------------------------------------
Waste code Waste category Effective date
----------------------------------------------------------------------------------------------------------------
D001 c................................ All (except High TOC Ignitable Liquids). Aug. 9, 1993.
D001.................................. High TOC Ignitable Liquids.............. Aug. 8, 1990.
D002 c................................ All..................................... Aug. 9, 1993.
D003.................................. Newly identified surface-disposed May 26, 2000.
elemental phosphorus processing wastes.
D004.................................. Newly identified D004 and mineral Aug. 24, 1998.
processing wastes.
D004.................................. Mixed radioactive/newly identified D004 May 26, 2000
or mineral processing wastes.
D005.................................. Newly identified D005 and mineral Aug. 24, 1998.
processing wastes.
D005.................................. Mixed radioactive/newly identified D005 May 26, 2000.
or mineral processing wastes.
D006.................................. Newly identified D006 and mineral Aug. 24, 1998.
processing wastes.
D006.................................. Mixed radioactive/newly identified D006 May 26, 2000.
or mineral processing wastes.
D007.................................. Newly identified D007 and mineral Aug. 24, 1998.
processing wastes.
D007.................................. Mixed radioactive/newly identified D007 May 26, 2000.
or mineral processing wastes.
[[Page 259]]
D008.................................. Newly identified D008 and mineral Aug. 24, 1998.
processing waste.
D008.................................. Mixed radioactive/newly identified D008 May 26, 2000.
or mineral processing wastes.
D009.................................. Newly identified D009 and mineral Aug. 24, 1998.
processing waste.
D009.................................. Mixed radioactive/newly identified D009 May 26, 2000.
or mineral processing wastes.
D010.................................. Newly identified D010 and mineral Aug. 24, 1998.
processing wastes.
D010.................................. Mixed radioactive/newly identified D010 May 26, 2000.
or mineral processing wastes.
D011.................................. Newly identified D011 and mineral Aug. 24, 1998.
processing wastes.
D011.................................. Mixed radioactive/newly identified D011 May 26, 2000.
or mineral processing wastes.
D012 (that exhibit the toxicity All..................................... Dec. 14, 1994.
characteristic based on the TCLP) d.
D013 (that exhibit the toxicity All..................................... Dec. 14, 1994.
characteristic based on the TCLP) d.
D014 (that exhibit the toxicity All..................................... Dec. 14, 1994.
characteristic based on the TCLP) d.
D015 (that exhibit the toxicity All..................................... Dec. 14, 1994.
characteristic based on the TCLP) d.
D016 (that exhibit the toxicity All..................................... Dec. 14, 1994.
characteristic based on the TCLP) d.
D017 (that exhibit the toxicity All..................................... Dec. 14, 1994.
characteristic based on the TCLP) d.
D018.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D018.................................. All others.............................. Dec. 19, 1994.
D019.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D019.................................. All others.............................. Dec. 19, 1994.
D020.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D020.................................. All others.............................. Dec. 19, 1994.
D021.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D021.................................. All others.............................. Dec. 19, 1994.
D022.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D022.................................. All others.............................. Dec. 19, 1994.
D023.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D023.................................. All others.............................. Dec. 19, 1994.
D024.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D024.................................. All others.............................. Dec. 19, 1994.
D025.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D025.................................. All others.............................. Dec. 19, 1994.
D026.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D026.................................. All others.............................. Dec. 19, 1994.
D027.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D027.................................. All others.............................. Dec. 19, 1994.
D028.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D028.................................. All others.............................. Dec. 19, 1994.
D029.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D029.................................. All others.............................. Dec. 19, 1994.
D030.................................. Mixed with radioactive wastes........... Sept. 19. 1996.
D030.................................. All others.............................. Dec. 19, 1994.
D031.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D031.................................. All others.............................. Dec. 19, 1994.
D032.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D032.................................. All others.............................. Dec. 19, 1994.
D033.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D033.................................. All others.............................. Dec. 19, 1994.
D034.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D034.................................. All others.............................. Dec. 19, 1994.
D035.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D035.................................. All others.............................. Dec. 19, 1994.
D036.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D036.................................. All others.............................. Dec. 19, 1994.
D037.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D037.................................. All others.............................. Dec. 19, 1994.
D038.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D038.................................. All others.............................. Dec. 19, 1994.
D039.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D039.................................. All others.............................. Dec. 19, 1994.
D040.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D040.................................. All others.............................. Dec. 19, 1994.
D041.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
[[Page 260]]
D041.................................. All others.............................. Dec. 19, 1994.
D042.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D042.................................. All others.............................. Dec. 19, 1994.
D043.................................. Mixed with radioactive wastes........... Sept. 19, 1996.
D043.................................. All others.............................. Dec. 19, 1994.
F001.................................. Small quantity generators, CERCLA Nov. 8, 1988.
response/RCRA corrective action,
initial generator's solvent-water
mixtures, solvent-containing sludges
and solids.
F001.................................. All others.............................. Nov. 8, 1986.
F002 (1,1,2-trichloroethane).......... Wastewater and Nonwastewater............ Aug. 8, 1990.
F002.................................. Small quantity generators, CERCLA Nov. 8, 1988.
response/RCRA corrective action,
initial generator's solvent-water
mixtures, solvent-containing sludges
and solids.
F002.................................. All others.............................. Nov. 8, 1986.
F003.................................. Small quantity generators, CERCLA Nov. 8, 1988.
response/RCRA corrective action,
initial generator's solvent-water
mixtures, solvent-containing sludges
and solids.
F003.................................. All others.............................. Nov. 8, 1986.
F004.................................. Small quantity generators, CERCLA Nov. 8, 1988.
response/RCRA corrective action,
initial generator's solvent-water
mixtures, solvent-containing sludges
and solids.
F004.................................. All others.............................. Nov. 8, 1986.
F005 (benzene, 2-ethoxy ethanol, 2- Wastewater and Nonwastewater............ Aug. 8, 1990.
nitropropane).
F005.................................. Small quantity generators, CERCLA Nov. 8, 1988.
response/RCRA corrective action,
initial generator's solvent-water
mixtures, solvent-containing sludges
and solids.
F005.................................. All others.............................. Nov. 8, 1986.
F006.................................. Wastewater.............................. Aug. 8, 1990.
F006.................................. Nonwastewater........................... Aug. 8, 1988.
F006 (cyanides)....................... Nonwastewater........................... July 8, 1989.
F007.................................. All..................................... July 8, 1989.
F008.................................. All..................................... July 8, 1989.
F009.................................. All..................................... July 8, 1989.
F010.................................. All..................................... June 8, 1989.
F011 (cyanides)....................... Nonwastewater........................... Dec. 8, 1989.
F011.................................. All others.............................. July 8, 1989.
F012 (cyanides)....................... Nonwastewater........................... Dec. 8, 1989.
F012.................................. All others.............................. July 8, 1989.
F019.................................. All..................................... Aug. 8, 1990.
F020.................................. All..................................... Nov. 8, 1988.
F021.................................. All..................................... Nov. 8, 1988.
F025.................................. All..................................... Aug. 8, 1990.
F026.................................. All..................................... Nov. 8, 1988.
F027.................................. All..................................... Nov. 8, 1988.
F028.................................. All..................................... Nov. 8, 1988.
F032.................................. Mixed with radioactive wastes........... May 12, 1999
F032.................................. All others.............................. Aug. 12, 1997.
F034.................................. Mixed with radioactive wastes........... May 12, 1999
F034.................................. All others.............................. Aug. 12, 1997.
F035.................................. Mixed with radioactive wastes........... May 12, 1999.
F035.................................. All others.............................. Aug. 12, 1997.
F037.................................. Not generated from surface impoundment June 30, 1993.
cleanouts or closures.
F037.................................. Generated from surface impoundment June 30, 1994.
cleanouts or closures.
F037.................................. Mixed with radioactive wastes........... June 30, 1994.
F038.................................. Not generated from surface impoundment June 30, 1993.
cleanouts or closures.
F038.................................. Generated from surface impoundment June 30, 1994.
cleanouts or closures.
F038.................................. Mixed with radioactive wastes........... June 30, 1994.
F039.................................. Wastewater.............................. Aug. 8, 1990.
F039.................................. Nonwastewater........................... May 8, 1992.
K001 (organics) b..................... All..................................... Aug. 8, 1988.
K001.................................. All others.............................. Aug. 8, 1988.
K002.................................. All..................................... Aug. 8, 1990.
K003.................................. All..................................... Aug. 8, 1990.
K004.................................. Wastewater.............................. Aug. 8, 1990.
K004.................................. Nonwastewater........................... Aug. 8, 1988.
K005.................................. Wastewater.............................. Aug. 8, 1990.
K005.................................. Nonwastewater........................... June 8, 1989.
K006.................................. All..................................... Aug. 8, 1990.
[[Page 261]]
K007.................................. Wastewater.............................. Aug. 8, 1990.
K007.................................. Nonwastewater........................... June 8, 1989.
K008.................................. Wastewater.............................. Aug. 8, 1990.
K008.................................. Nonwastewater........................... Aug. 8, 1988.
K009.................................. All..................................... June 8, 1989.
K010.................................. All..................................... June 8, 1989.
K011.................................. Wastewater.............................. Aug. 8, 1990.
K011.................................. Nonwastewater........................... June 8, 1989.
K013.................................. Wastewater.............................. Aug. 8, 1990.
K013.................................. Nonwastewater........................... June 8, 1989.
K014.................................. Wastewater.............................. Aug. 8, 1990.
K014.................................. Nonwastewater........................... June 8, 1989.
K015.................................. Wastewater.............................. Aug. 8, 1988.
K015.................................. Nonwastewater........................... Aug. 8, 1990.
K016.................................. All..................................... Aug. 8, 1988.
K017.................................. All..................................... Aug. 8, 1990.
K018.................................. All..................................... Aug. 8, 1988.
K019.................................. All..................................... Aug. 8, 1988.
K020.................................. All..................................... Aug. 8, 1988.
K021.................................. Wastewater.............................. Aug. 8, 1990.
K021.................................. Nonwastewater........................... Aug. 8, 1988.
K022.................................. Wastewater.............................. Aug. 8, 1990.
K022.................................. Nonwastewater........................... Aug. 8, 1988.
K023.................................. All..................................... June 8, 1989.
K024.................................. All..................................... Aug. 8, 1988.
K025.................................. Wastewater.............................. Aug. 8, 1990.
K025.................................. Nonwastewater........................... Aug. 8, 1988.
K026.................................. All..................................... Aug. 8, 1990.
K027.................................. All..................................... June 8, 1989.
K028 (metals)......................... Nonwastewater........................... Aug. 8, 1990.
K028.................................. All others.............................. June 8, 1989.
K029.................................. Wastewater.............................. Aug. 8, 1990.
K029.................................. Nonwastewater........................... June 8, 1989.
K030.................................. All..................................... Aug. 8, 1988.
K031.................................. Wastewater.............................. Aug. 8, 1990.
K031.................................. Nonwastewater........................... May 8, 1992.
K032.................................. All..................................... Aug. 8, 1990.
K033.................................. All..................................... Aug. 8, 1990.
K034.................................. All..................................... Aug. 8, 1990.
K035.................................. All..................................... Aug. 8, 1990.
K036.................................. Wastewater.............................. June 8, 1989.
K036.................................. Nonwastewater........................... Aug. 8, 1988.
K037 b................................ Wastewater.............................. Aug. 8, 1988.
K037.................................. Nonwastewater........................... Aug. 8, 1988.
K038.................................. All..................................... June 8, 1989.
K039.................................. All..................................... June 8, 1989.
K040.................................. All..................................... June 8, 1989.
K041.................................. All..................................... Aug. 8, 1990.
K042.................................. All..................................... Aug. 8, 1990.
K043.................................. All..................................... June 8, 1989.
K044.................................. All..................................... Aug. 8, 1988.
K045.................................. All..................................... Aug. 8, 1988.
K046 (Nonreactive).................... Nonwastewater........................... Aug. 8, 1988.
K046.................................. All others.............................. Aug. 8, 1990.
K047.................................. All..................................... Aug. 8, 1988.
K048.................................. Wastewater.............................. Aug. 8, 1990.
K048.................................. Nonwastewater........................... Nov. 8, 1990.
K049.................................. Wastewater.............................. Aug. 8, 1990.
K049.................................. Nonwastewater........................... Nov. 8, 1990.
K050.................................. Wastewater.............................. Aug. 8, 1990.
K050.................................. Nonwastewater........................... Nov. 8, 1990.
K051.................................. Wastewater.............................. Aug. 8, 1990.
K051.................................. Nonwastewater........................... Nov. 8, 1990.
K052.................................. Wastewater.............................. Aug. 8, 1990.
K052.................................. Nonwastewater........................... Nov. 8, 1990.
K060.................................. Wastewater.............................. Aug. 8, 1990.
K060.................................. Nonwastewater........................... Aug. 8, 1988.
K061.................................. Wastewater.............................. Aug. 8, 1990.
K061.................................. Nonwastewater........................... June 30, 1992.
K062.................................. All..................................... Aug. 8, 1988.
K069 (Non-Calcium Sulfate)............ Nonwastewater........................... Aug. 8, 1988.
[[Page 262]]
K069.................................. All others.............................. Aug. 8, 1990.
K071.................................. All..................................... Aug. 8, 1990.
K073.................................. All..................................... Aug. 8, 1990.
K083.................................. All..................................... Aug. 8, 1990.
K084.................................. Wastewater.............................. Aug. 8, 1990.
K084.................................. Nonwastewater........................... May 8, 1992.
K085.................................. All..................................... Aug. 8, 1990.
K086 (organics) b..................... All..................................... Aug. 8, 1988.
K086.................................. All others.............................. Aug. 8, 1988.
K087.................................. All..................................... Aug. 8, 1988.
K088.................................. All others.............................. Oct. 8, 1997.
K088.................................. All others.............................. Jan. 8, 1997.
K093.................................. All..................................... June 8, 1989.
K094.................................. All..................................... June 8, 1989.
K095.................................. Wastewater.............................. Aug. 8, 1990.
K095.................................. Nonwastewater........................... June 8, 1989.
K096.................................. Wastewater.............................. Aug. 8, 1990.
K096.................................. Nonwastewater........................... June 8, 1989.
K097.................................. All..................................... Aug. 8, 1990.
K098.................................. All..................................... Aug. 8, 1990.
K099.................................. All..................................... Aug. 8, 1988.
K100.................................. Wastewater.............................. Aug. 8, 1990.
K100.................................. Nonwastewater........................... Aug. 8, 1988.
K101 (organics)....................... Wastewater.............................. Aug. 8, 1988.
K101 (metals)......................... Wastewater.............................. Aug. 8, 1990.
K101 (organics)....................... Nonwastewater........................... Aug. 8, 1988.
K101 (metals)......................... Nonwastewater........................... May 8, 1992.
K102 (organics)....................... Wastewater.............................. Aug. 8, 1988.
K102 (metals)......................... Wastewater.............................. Aug. 8, 1990.
K102 (organics)....................... Nonwastewater........................... Aug. 8, 1988.
K102 (metals)......................... Nonwastewater........................... May 8, 1992.
K103.................................. All..................................... Aug. 8, 1988.
K104.................................. All..................................... Aug. 8, 1988.
K105.................................. All..................................... Aug. 8, 1990.
K106.................................. Wastewater.............................. Aug. 8, 1990.
K106.................................. Nonwastewater........................... May 8, 1992.
K107.................................. Mixed with radioactive wastes........... June 30, 1994.
K107.................................. All others.............................. Nov. 9, 1992.
K108.................................. Mixed with radioactive wastes........... June 30, 1994.
K108.................................. All others.............................. Nov. 9, 1992.
K109.................................. Mixed with radioactive wastes........... June 30, 1994.
K109.................................. All others.............................. Nov. 9, 1992.
K110.................................. Mixed with radioactive wastes........... June 30, 1994.
K110.................................. All others.............................. Nov. 9, 1992.
K111.................................. Mixed with radioactive wastes........... June 30, 1994.
K111.................................. All others.............................. Nov. 9, 1992.
K112.................................. Mixed with radioactive wastes........... June 30, 1994.
K112.................................. All others.............................. Nov. 9, 1992.
K113.................................. All..................................... June 8, 1989.
K114.................................. All..................................... June 8, 1989.
K115.................................. All..................................... June 8, 1989.
K116.................................. All..................................... June 8, 1989.
K117.................................. Mixed with radioactive wastes........... June 30, 1994.
K117.................................. All others.............................. Nov. 9, 1992.
K118.................................. Mixed with radioactive wastes........... June 30, 1994.
K118.................................. All others.............................. Nov. 9, 1992.
K123.................................. Mixed with radioactive wastes........... June 30, 1994.
K123.................................. All others.............................. Nov. 9, 1992.
K124.................................. Mixed with radioactive wastes........... June 30, 1994.
K124.................................. All others.............................. Nov. 9, 1992.
K125.................................. Mixed with radioactive wastes........... June 30, 1994.
K125.................................. All others.............................. Nov. 9, 1992.
K126.................................. Mixed with radioactive wastes........... June 30, 1994.
K126.................................. All others.............................. Nov. 9, 1992.
K131.................................. Mixed with radioactive wastes........... June 30, 1994.
K131.................................. All others.............................. Nov. 9, 1992.
K132.................................. Mixed with radioactive wastes........... June 30, 1994.
K132.................................. All others.............................. Nov. 9, 1992.
K136.................................. Mixed with radioactive wastes........... June 30, 1994.
K136.................................. All others.............................. Nov. 9, 1992.
K141.................................. Mixed with radioactive wastes........... Sep. 19, 1996.
[[Page 263]]
K141.................................. All others.............................. Dec. 19, 1994.
K142.................................. Mixed with radioactive wastes........... Sep. 19, 1996..
K142.................................. All others.............................. Dec. 19, 1994.
K143.................................. Mixed with radioactive wastes........... Sep. 19, 1996.
K143.................................. All others.............................. Dec. 19, 1994.
K144.................................. Mixed with radioactive wastes........... Sep. 19, 1996.
K144.................................. All others.............................. Dec. 19, 1994.
K145.................................. Mixed with radioactive wastes........... Sep. 19, 1996.
K145.................................. All others.............................. Dec. 19, 1994.
K147.................................. Mixed with radioactive wastes........... Sep. 19, 1996.
K147.................................. All others.............................. Dec. 19, 1994.
K148.................................. Mixed with radioactive wastes........... Sep. 19, 1996.
K148.................................. All others.............................. Dec. 19, 1994.
K149.................................. Mixed with radioactive wastes........... Sep. 19, 1996.
K149.................................. All others.............................. Dec. 19, 1994.
K150.................................. Mixed with radioactive wastes........... Sep. 19, 1996.
K150.................................. All others.............................. Dec. 19, 1994.
K151.................................. Mixed with radioactive wastes........... Sep. 19, 1996.
K151.................................. All others.............................. Dec. 19, 1994.
K156.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
K156.................................. All others.............................. July 8, 1996.
K157.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
K157.................................. All others.............................. July 8, 1996.
K158.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
K158.................................. All others.............................. July 8, 1996.
K159.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
K159.................................. All others.............................. July 8, 1996.
K160.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
K160.................................. All others.............................. July 8, 1996.
K161.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
K161.................................. All others.............................. July 8, 1996.
P001.................................. All..................................... Aug. 8, 1990.
P002.................................. All..................................... Aug. 8, 1990.
P003.................................. All..................................... Aug. 8, 1990.
P004.................................. All..................................... Aug. 8, 1990.
P005.................................. All..................................... Aug. 8, 1990.
P006.................................. All..................................... Aug. 8, 1990.
P007.................................. All..................................... Aug. 8, 1990.
P008.................................. All..................................... Aug. 8, 1990.
P009.................................. All..................................... Aug. 8, 1990.
P010.................................. Wastewater.............................. Aug. 8, 1990.
P010.................................. Nonwastewater........................... May 8, 1992.
P011.................................. Wastewater.............................. Aug. 8, 1990.
P011.................................. Nonwastewater........................... May 8, 1992.
P012.................................. Wastewater.............................. Aug. 8, 1990.
P012.................................. Nonwastewater........................... May 8, 1992.
P013 (barium)......................... Nonwastewater........................... Aug. 8, 1990.
P013.................................. All others.............................. June 8, 1989.
P014.................................. All..................................... Aug. 8, 1990.
P015.................................. All..................................... Aug. 8, 1990.
P016.................................. All..................................... Aug. 8, 1990.
P017.................................. All..................................... Aug. 8, 1990.
P018.................................. All..................................... Aug. 8, 1990.
P020.................................. All..................................... Aug. 8, 1990.
P021.................................. All..................................... June 8, 1989.
P022.................................. All..................................... Aug. 8, 1990.
P023.................................. All..................................... Aug. 8, 1990.
P024.................................. All..................................... Aug. 8, 1990.
P026.................................. All..................................... Aug. 8, 1990.
P027.................................. All..................................... Aug. 8, 1990.
P028.................................. All..................................... Aug. 8, 1990.
P029.................................. All..................................... June 8, 1989.
P030.................................. All..................................... June 8, 1989.
P031.................................. All..................................... Aug. 8, 1990.
P033.................................. All..................................... Aug. 8, 1990.
P034.................................. All..................................... Aug. 8, 1990.
P036.................................. Wastewater.............................. Aug. 8, 1990.
P036.................................. Nonwastewater........................... May 8, 1992.
P037.................................. All..................................... Aug. 8, 1990.
P038.................................. Wastewater.............................. Aug. 8, 1990.
P038.................................. Nonwastewater........................... May 8, 1992.
[[Page 264]]
P039.................................. All..................................... June 8, 1989.
P040.................................. All..................................... June 8, 1989.
P041.................................. All..................................... June 8, 1989.
P042.................................. All..................................... Aug. 8, 1990.
P043.................................. All..................................... June 8, 1989.
P044.................................. All..................................... June 8, 1989.
P045.................................. All..................................... Aug. 8, 1990.
P046.................................. All..................................... Aug. 8, 1990.
P047.................................. All..................................... Aug. 8, 1990.
P048.................................. All..................................... Aug. 8, 1990.
P049.................................. All..................................... Aug. 8, 1990.
P050.................................. All..................................... Aug. 8, 1990.
P051.................................. All..................................... Aug. 8, 1990.
P054.................................. All..................................... Aug. 8, 1990.
P056.................................. All..................................... Aug. 8, 1990.
P057.................................. All..................................... Aug. 8, 1990.
P058.................................. All..................................... Aug. 8, 1990.
P059.................................. All..................................... Aug. 8, 1990.
P060.................................. All..................................... Aug. 8, 1990.
P062.................................. All..................................... June 8, 1989.
P063.................................. All..................................... June 8, 1989.
P064.................................. All..................................... Aug. 8, 1990.
P065.................................. Wastewater.............................. Aug. 8, 1990.
P065.................................. Nonwastewater........................... May 8, 1992.
P066.................................. All..................................... Aug. 8, 1990.
P067.................................. All..................................... Aug. 8, 1990.
P068.................................. All..................................... Aug. 8, 1990.
P069.................................. All..................................... Aug. 8, 1990.
P070.................................. All..................................... Aug. 8, 1990.
P071.................................. All..................................... June 8, 1989.
P072.................................. All..................................... Aug. 8, 1990.
P073.................................. All..................................... Aug. 8, 1990.
P074.................................. All..................................... June 8, 1989.
P075.................................. All..................................... Aug. 8, 1990.
P076.................................. All..................................... Aug. 8, 1990.
P077.................................. All..................................... Aug. 8, 1990.
P078.................................. All..................................... Aug. 8, 1990.
P081.................................. All..................................... Aug. 8, 1990.
P082.................................. All..................................... Aug. 8, 1990.
P084.................................. All..................................... Aug. 8, 1990.
P085.................................. All..................................... June 8, 1989.
P087.................................. All..................................... May 8, 1992.
P088.................................. All..................................... Aug. 8, 1990.
P089.................................. All..................................... June 8, 1989.
P092.................................. Wastewater.............................. Aug. 8, 1990.
P092.................................. Nonwastewater........................... May 8, 1992.
P093.................................. All..................................... Aug. 8, 1990.
P094.................................. All..................................... June 8, 1989.
P095.................................. All..................................... Aug. 8, 1990.
P096.................................. All..................................... Aug. 8, 1990.
P097.................................. All..................................... June 8, 1989.
P098.................................. All..................................... June 8, 1989.
P099 (silver)......................... Wastewater.............................. Aug. 8, 1990.
P099.................................. All others.............................. June 8, 1989.
P101.................................. All..................................... Aug. 8, 1990.
P102.................................. All..................................... Aug. 8, 1990.
P103.................................. All..................................... Aug. 8, 1990.
P104 (silver)......................... Wastewater.............................. Aug. 8, 1990.
P104.................................. All others.............................. June 8, 1989.
P105.................................. All..................................... Aug. 8, 1990.
P106.................................. All..................................... June 8, 1989.
P108.................................. All..................................... Aug. 8, 1990.
P109.................................. All..................................... June 8, 1989.
P110.................................. All..................................... Aug. 8, 1990.
P111.................................. All..................................... June 8, 1989.
P112.................................. All..................................... Aug. 8, 1990.
P113.................................. All..................................... Aug. 8, 1990.
P114.................................. All..................................... Aug. 8, 1990.
P115.................................. All..................................... Aug. 8, 1990.
P116.................................. All..................................... Aug. 8, 1990.
P118.................................. All..................................... Aug. 8, 1990.
[[Page 265]]
P119.................................. All..................................... Aug. 8, 1990.
P120.................................. All..................................... Aug. 8, 1990.
P121.................................. All..................................... June 8, 1989.
P122.................................. All..................................... Aug. 8, 1990.
P123.................................. All..................................... Aug. 8, 1990.
P127.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P127.................................. All others.............................. July 8, 1996.
P128.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P128.................................. All others.............................. July 8, 1996.
P185.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P185.................................. All others.............................. July 8, 1996.
P188.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P188.................................. All others.............................. July 8, 1996.
P189.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P189.................................. All others.............................. July 8, 1996.
P190.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P190.................................. All others.............................. July 8, 1996.
P191.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P191.................................. All others.............................. July 8, 1996.
P192.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P192.................................. All others.............................. July 8, 1996.
P194.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P194.................................. All others.............................. July 8, 1996.
P196.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P196.................................. All others.............................. July 8, 1996.
P197.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P197.................................. All others.............................. July 8, 1996.
P198.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P198.................................. All others.............................. July 8, 1996.
P199.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P199.................................. All others.............................. July 8, 1996.
P201.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P201.................................. All others.............................. July 8, 1996.
P202.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P202.................................. All others.............................. July 8, 1996.
P203.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P203.................................. All others.............................. July 8, 1996.
P204.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P204.................................. All others.............................. July 8, 1996.
P205.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
P205.................................. All others.............................. July 8, 1996.
U001.................................. All..................................... Aug. 8, 1990.
U002.................................. All..................................... Aug. 8, 1990.
U003.................................. All..................................... Aug. 8, 1990.
U004.................................. All..................................... Aug. 8, 1990.
U005.................................. All..................................... Aug. 8, 1990.
U006.................................. All..................................... Aug. 8, 1990.
U007.................................. All..................................... Aug. 8, 1990.
U008.................................. All..................................... Aug. 8, 1990.
U009.................................. All..................................... Aug. 8, 1990.
U010.................................. All..................................... Aug. 8, 1990.
U011.................................. All..................................... Aug. 8, 1990.
U012.................................. All..................................... Aug. 8, 1990.
U014.................................. All..................................... Aug. 8, 1990.
U015.................................. All..................................... Aug. 8, 1990.
U016.................................. All..................................... Aug. 8, 1990.
U017.................................. All..................................... Aug. 8, 1990.
U018.................................. All..................................... Aug. 8, 1990.
U019.................................. All..................................... Aug. 8, 1990.
U020.................................. All..................................... Aug. 8, 1990.
U021.................................. All..................................... Aug. 8, 1990.
U022.................................. All..................................... Aug. 8, 1990.
U023.................................. All..................................... Aug. 8, 1990.
U024.................................. All..................................... Aug. 8, 1990.
U025.................................. All..................................... Aug. 8, 1990.
U026.................................. All..................................... Aug. 8, 1990.
U027.................................. All..................................... Aug. 8, 1990.
U028.................................. All..................................... June 8, 1989.
U029.................................. All..................................... Aug. 8, 1990.
U030.................................. All..................................... Aug. 8, 1990.
U031.................................. All..................................... Aug. 8, 1990.
[[Page 266]]
U032.................................. All..................................... Aug. 8, 1990.
U033.................................. All..................................... Aug. 8, 1990.
U034.................................. All..................................... Aug. 8, 1990.
U035.................................. All..................................... Aug. 8, 1990.
U036.................................. All..................................... Aug. 8, 1990.
U037.................................. All..................................... Aug. 8, 1990.
U038.................................. All..................................... Aug. 8, 1990.
U039.................................. All..................................... Aug. 8, 1990.
U041.................................. All..................................... Aug. 8, 1990.
U042.................................. All..................................... Aug. 8, 1990.
U043.................................. All..................................... Aug. 8, 1990.
U044.................................. All..................................... Aug. 8, 1990.
U045.................................. All..................................... Aug. 8, 1990.
U046.................................. All..................................... Aug. 8, 1990.
U047.................................. All..................................... Aug. 8, 1990.
U048.................................. All..................................... Aug. 8, 1990.
U049.................................. All..................................... Aug. 8, 1990.
U050.................................. All..................................... Aug. 8, 1990.
U051.................................. All..................................... Aug. 8, 1990.
U052.................................. All..................................... Aug. 8, 1990.
U053.................................. All..................................... Aug. 8, 1990.
U055.................................. All..................................... Aug. 8, 1990.
U056.................................. All..................................... Aug. 8, 1990.
U057.................................. All..................................... Aug. 8, 1990.
U058.................................. All..................................... June 8, 1989.
U059.................................. All..................................... Aug. 8, 1990.
U060.................................. All..................................... Aug. 8, 1990.
U061.................................. All..................................... Aug. 8, 1990.
U062.................................. All..................................... Aug. 8, 1990.
U063.................................. All..................................... Aug. 8, 1990.
U064.................................. All..................................... Aug. 8, 1990.
U066.................................. All..................................... Aug. 8, 1990.
U067.................................. All..................................... Aug. 8, 1990.
U068.................................. All..................................... Aug. 8, 1990.
U069.................................. All..................................... June 30, 1992.
U070.................................. All..................................... Aug. 8, 1990.
U071.................................. All..................................... Aug. 8, 1990.
U072.................................. All..................................... Aug. 8, 1990.
U073.................................. All..................................... Aug. 8, 1990.
U074.................................. All..................................... Aug. 8, 1990.
U075.................................. All..................................... Aug. 8, 1990.
U076.................................. All..................................... Aug. 8, 1990.
U077.................................. All..................................... Aug. 8, 1990.
U078.................................. All..................................... Aug. 8, 1990.
U079.................................. All..................................... Aug. 8, 1990.
U080.................................. All..................................... Aug. 8, 1990.
U081.................................. All..................................... Aug. 8, 1990.
U082.................................. All..................................... Aug. 8, 1990.
U083.................................. All..................................... Aug. 8, 1990.
U084.................................. All..................................... Aug. 8, 1990.
U085.................................. All..................................... Aug. 8, 1990.
U086.................................. All..................................... Aug. 8, 1990.
U087.................................. All..................................... June 8, 1989.
U088.................................. All..................................... June 8, 1989.
U089.................................. All..................................... Aug. 8, 1990.
U090.................................. All..................................... Aug. 8, 1990.
U091.................................. All..................................... Aug. 8, 1990.
U092.................................. All..................................... Aug. 8, 1990.
U093.................................. All..................................... Aug. 8, 1990.
U094.................................. All..................................... Aug. 8, 1990.
U095.................................. All..................................... Aug. 8, 1990.
U096.................................. All..................................... Aug. 8, 1990.
U097.................................. All..................................... Aug. 8, 1990.
U098.................................. All..................................... Aug. 8, 1990.
U099.................................. All..................................... Aug. 8, 1990.
U101.................................. All..................................... Aug. 8, 1990.
U102.................................. All..................................... June 8, 1989.
U103.................................. All..................................... Aug. 8, 1990.
U105.................................. All..................................... Aug. 8, 1990.
U106.................................. All..................................... Aug. 8, 1990.
U107.................................. All..................................... June 8, 1989.
[[Page 267]]
U108.................................. All..................................... Aug. 8, 1990.
U109.................................. All..................................... Aug. 8, 1990.
U110.................................. All..................................... Aug. 8, 1990.
U111.................................. All..................................... Aug. 8, 1990.
U112.................................. All..................................... Aug. 8, 1990.
U113.................................. All..................................... Aug. 8, 1990.
U114.................................. All..................................... Aug. 8, 1990.
U115.................................. All..................................... Aug. 8, 1990.
U116.................................. All..................................... Aug. 8, 1990.
U117.................................. All..................................... Aug. 8, 1990.
U118.................................. All..................................... Aug. 8, 1990.
U119.................................. All..................................... Aug. 8, 1990.
U120.................................. All..................................... Aug. 8, 1990.
U121.................................. All..................................... Aug. 8, 1990.
U122.................................. All..................................... Aug. 8, 1990.
U123.................................. All..................................... Aug. 8, 1990.
U124.................................. All..................................... Aug. 8, 1990.
U125.................................. All..................................... Aug. 8, 1990.
U126.................................. All..................................... Aug. 8, 1990.
U127.................................. All..................................... Aug. 8, 1990.
U128.................................. All..................................... Aug. 8, 1990.
U129.................................. All..................................... Aug. 8, 1990.
U130.................................. All..................................... Aug. 8, 1990.
U131.................................. All..................................... Aug. 8, 1990.
U132.................................. All..................................... Aug. 8, 1990.
U133.................................. All..................................... Aug. 8, 1990.
U134.................................. All..................................... Aug. 8, 1990.
U135.................................. All..................................... Aug. 8, 1990.
U136.................................. Wastewater.............................. Aug. 8, 1990.
U136.................................. Nonwastewater........................... May 8, 1992.
U137.................................. All..................................... Aug. 8, 1990.
U138.................................. All..................................... Aug. 8, 1990.
U140.................................. All..................................... Aug. 8, 1990.
U141.................................. All..................................... Aug. 8, 1990.
U142.................................. All..................................... Aug. 8, 1990.
U143.................................. All..................................... Aug. 8, 1990.
U144.................................. All..................................... Aug. 8, 1990.
U145.................................. All..................................... Aug. 8, 1990.
U146.................................. All..................................... Aug. 8, 1990.
U147.................................. All..................................... Aug. 8, 1990.
U148.................................. All..................................... Aug. 8, 1990.
U149.................................. All..................................... Aug. 8, 1990.
U150.................................. All..................................... Aug. 8, 1990.
U151.................................. Wastewater.............................. Aug. 8, 1990.
U151.................................. Nonwastewater........................... May 8, 1992.
U152.................................. All..................................... Aug. 8, 1990.
U153.................................. All..................................... Aug. 8, 1990.
U154.................................. All..................................... Aug. 8, 1990.
U155.................................. All..................................... Aug. 8, 1990.
U156.................................. All..................................... Aug. 8, 1990.
U157.................................. All..................................... Aug. 8, 1990.
U158.................................. All..................................... Aug. 8, 1990.
U159.................................. All..................................... Aug. 8, 1990.
U160.................................. All..................................... Aug. 8, 1990.
U161.................................. All..................................... Aug. 8, 1990.
U162.................................. All..................................... Aug. 8, 1990.
U163.................................. All..................................... Aug. 8, 1990.
U164.................................. All..................................... Aug. 8, 1990.
U165.................................. All..................................... Aug. 8, 1990.
U166.................................. All..................................... Aug. 8, 1990.
U167.................................. All..................................... Aug. 8, 1990.
U168.................................. All..................................... Aug. 8, 1990.
U169.................................. All..................................... Aug. 8, 1990.
U170.................................. All..................................... Aug. 8, 1990.
U171.................................. All..................................... Aug. 8, 1990.
U172.................................. All..................................... Aug. 8, 1990.
U173.................................. All..................................... Aug. 8, 1990.
U174.................................. All..................................... Aug. 8, 1990.
U176.................................. All..................................... Aug. 8, 1990.
U177.................................. All..................................... Aug. 8, 1990.
U178.................................. All..................................... Aug. 8, 1990.
[[Page 268]]
U179.................................. All..................................... Aug. 8, 1990.
U180.................................. All..................................... Aug. 8, 1990.
U181.................................. All..................................... Aug. 8, 1990.
U182.................................. All..................................... Aug. 8, 1990.
U183.................................. All..................................... Aug. 8, 1990.
U184.................................. All..................................... Aug. 8, 1990.
U185.................................. All..................................... Aug. 8, 1990.
U186.................................. All..................................... Aug. 8, 1990.
U187.................................. All..................................... Aug. 8, 1990.
U188.................................. All..................................... Aug. 8, 1990.
U189.................................. All..................................... Aug. 8, 1990.
U190.................................. All..................................... June 8, 1989.
U191.................................. All..................................... Aug. 8, 1990.
U192.................................. All..................................... Aug. 8, 1990.
U193.................................. All..................................... Aug. 8, 1990.
U194.................................. All..................................... June 8, 1989.
U196.................................. All..................................... Aug. 8, 1990.
U197.................................. All..................................... Aug. 8, 1990.
U200.................................. All..................................... Aug. 8, 1990.
U201.................................. All..................................... Aug. 8, 1990.
U202.................................. All..................................... Aug. 8, 1990.
U203.................................. All..................................... Aug. 8, 1990.
U204.................................. All..................................... Aug. 8, 1990.
U205.................................. All..................................... Aug. 8, 1990.
U206.................................. All..................................... Aug. 8, 1990.
U207.................................. All..................................... Aug. 8, 1990.
U208.................................. All..................................... Aug. 8, 1990.
U209.................................. All..................................... Aug. 8, 1990.
U210.................................. All..................................... Aug. 8, 1990.
U211.................................. All..................................... Aug. 8, 1990.
U213.................................. All..................................... Aug. 8, 1990.
U214.................................. All..................................... Aug. 8, 1990.
U215.................................. All..................................... Aug. 8, 1990.
U216.................................. All..................................... Aug. 8, 1990.
U217.................................. All..................................... Aug. 8, 1990.
U218.................................. All..................................... Aug. 8, 1990.
U219.................................. All..................................... Aug. 8, 1990.
U220.................................. All..................................... Aug. 8, 1990.
U221.................................. All..................................... June 8, 1989.
U222.................................. All..................................... Aug. 8, 1990.
U223.................................. All..................................... June 8, 1989.
U225.................................. All..................................... Aug. 8, 1990.
U226.................................. All..................................... Aug. 8, 1990.
U227.................................. All..................................... Aug. 8, 1990.
U228.................................. All..................................... Aug. 8, 1990.
U234.................................. All..................................... Aug. 8, 1990.
U235.................................. All..................................... June 8, 1989.
U236.................................. All..................................... Aug. 8, 1990.
U237.................................. All..................................... Aug. 8, 1990.
U238.................................. All..................................... Aug. 8, 1990.
U239.................................. All..................................... Aug. 8, 1990.
U240.................................. All..................................... Aug. 8, 1990.
U243.................................. All..................................... Aug. 8, 1990.
U244.................................. All..................................... Aug. 8, 1990.
U246.................................. All..................................... Aug. 8, 1990.
U247.................................. All..................................... Aug. 8, 1990.
U248.................................. All..................................... Aug. 8, 1990.
U249.................................. All..................................... Aug. 8, 1990.
U271.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U271.................................. All others.............................. July 8, 1996.
U277.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U277.................................. All others.............................. July 8, 1996.
U278.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U278.................................. All others.............................. July 8, 1996.
U279.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U279.................................. All others.............................. July 8, 1996.
U280.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U280.................................. All others.............................. July 8, 1996.
U328.................................. Mixed with radioactive wastes........... June 30, 1994.
U328.................................. All others.............................. Nov. 9, 1992.
U353.................................. Mixed with radioactive wastes........... June 30, 1994.
[[Page 269]]
U353.................................. All others.............................. Nov. 9, 1992.
U359.................................. Mixed with radioactive wastes........... June 30, 1994.
U359.................................. All others.............................. Nov. 9, 1992.
U364.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U364.................................. All others.............................. July 8, 1996.
U365.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U365.................................. All others.............................. July 8, 1996.
U366.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U366.................................. All others.............................. July 8, 1996.
U367.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U367.................................. All others.............................. July 8, 1996.
U372.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U372.................................. All others.............................. July 8, 1996.
U373.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U373.................................. All others.............................. July 8, 1996.
U375.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U375.................................. All others.............................. July 8, 1996.
U376.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U376.................................. All others.............................. July 8, 1996.
U377.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U377.................................. All others.............................. July 8, 1996.
U378.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U378.................................. All others.............................. July 8, 1996.
U379.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U379.................................. All others.............................. July 8, 1996.
U381.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U381.................................. All others.............................. July 8, 1996.
U382.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U382.................................. All others.............................. July 8, 1996.
U383.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U383.................................. All others.............................. July 8, 1996.
U384.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U384.................................. All others.............................. July 8, 1996.
U385.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U385.................................. All others.............................. July 8, 1996.
U386.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U386.................................. All others.............................. July 8, 1996.
U387.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U387.................................. All others.............................. July 8, 1996.
U389.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U389.................................. All others.............................. July 8, 1996.
U390.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U390.................................. All others.............................. July 8, 1996.
U391.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U391.................................. All others.............................. July 8, 1996.
U392.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U392.................................. All others.............................. July 8, 1996.
U393.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U393.................................. All others.............................. July 8, 1996.
U394.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U394.................................. All others.............................. July 8, 1996.
U395.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U395.................................. All others.............................. July 8, 1996.
U396.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U396.................................. All others.............................. July 8, 1996.
U400.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U400.................................. All others.............................. July 8, 1996.
U401.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U401.................................. All others.............................. July 8, 1996.
U402.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U402.................................. All others.............................. July 8, 1996.
U403.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U403.................................. All others.............................. July 8, 1996.
U404.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U404.................................. All others.............................. July 8, 1996.
U407.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U407.................................. All others.............................. July 8, 1996.
U409.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U409.................................. All others.............................. July 8, 1996.
U410.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U410.................................. All others.............................. July 8, 1996.
[[Page 270]]
U411.................................. Mixed with radioactive wastes........... Apr. 8, 1998.
U411.................................. All others.............................. July 8, 1996.
----------------------------------------------------------------------------------------------------------------
a This table does not include mixed radioactive wastes (from the First, Second, and Third Third rules) which
received national capacity variance until May 8, 1992. This table also does not include contaminated soil and
debris wastes.
b The standard was revised in the Third Third Final Rule (55 FR 22520, June 1, 1990).
c The standard was revised in the Third Third Emergency Rule (58 FR 29860, May 24, 1993); the original effective
date was August 8, 1990.
d The standard was revised in the Phase II Final Rule (59 FR 47982, Sept. 19, 1994); the original effective date
was August 8, 1990.
e The standards for selected reactive wastes was revised in the Phase III Final Rule (61 FR 15566, Apr. 8,
1996); the original effective date was August 8, 1990.
Table 2--Summary of Effective Dates of Land Disposal Restrictions for
Contaminated Soil and Debris (CSD)
------------------------------------------------------------------------
Restricted hazardous waste in CSD Effective date
------------------------------------------------------------------------
1. Solvent-(F001-F005) and dioxin-(F020-F023 Nov. 8, 1990.
and F026-F028) containing soil and debris
from CERCLA response or RCRA corrective
actions.
2. Soil and debris not from CERCLA response Nov. 8, 1988.
or RCRA corrective actions contaminated with
less than 1% total solvents (F001-F005) or
dioxins (F020-F023 and F026-F028).
3 All soil and debris contaminated with First Aug. 8, 1990.
Third wastes for which treatment standards
are based on incineration.
4. All soil and debris contaminated with June 8, 1991.
Second Third wastes for which treatment
standards are based on incineration.
5. All soil and debris contaminated with May 8, 1992.
Third Third wastes or, First or Second Third
``soft hammer'' wastes which had treatment
standards promulgated in the Third Third
rule, for which treatment standards are
based on incineration, vitrification, or
mercury retorting, acid leaching followed by
chemical precipitation, or thermal recovery
of metals; as well as all inorganic solids
debris contaminated with D004-D011 wastes,
and all soil and debris contaminated with
mixed RCRA/radioactive wastes.
6. Soil and debris contaminated with D012- Dec. 19, 1994.
D043, K141-K145, and K147-151 wastes.
7. Debris (only) contaminated with F037, Dec. 19, 1994
F038, K107-K112, K117, K118, K123-K126,
K131, K132, K136, U328, U353, U359.
8. Soil and debris contaminated with K156- July 8, 1996.
K161, P127, P128, P188-P192, P194, P196-
P199, P201-P205, U271, U277-U280, U364-U367,
U372, U373, U375-U379, U381-U387, U389-U396,
U400-U404, U407, and U409-U411 wastes.
9. Soil and debris contaminated with K088 Oct. 8, 1997.
wastes.
10. Soil and debris contaminated with April 8, 1998.
radioactive wastes mixed with K088, K156-
K161, P127, P128, P188-P192, P194, P196-
P199, P201-P205, U271, U277-U280, U364-U367,
U372, U373, U375-U379, U381-U387, U389-U396,
U400-U404, U407, and U409-U411 wastes.
11. Soil and debris contaminated with F032, May 12, 1997.
F034, and F035.
12. Soil and debris contaminated with newly Aug. 24, 1998.
identified D004-D011 toxicity characteristic
wastes and mineral processing wastes..
13. Soil and debris contaminated with mixed May 26, 2000.
radioactive newly identified D004-D011
characteristic wastes and mineral processing
wastes..
------------------------------------------------------------------------
Note: Appendix VII is provided for the convenience of the reader.
[62 FR 26025, May 12, 1997, as amended at 63 FR 28751, May 26, 1998; 65
FR 36367, June 8, 2000]
Effective Date Note: At 66 FR 27297, May 16, 2001, appendix VII to
part 268 was amended by adding a wastestream to table 1 effective August
14, 2001. For the convenience of the user, the added text is set forth
as follows:
Appendix VII to Part 268
----------------------------------------------------------------------------------------------------------------
Waste code Waste category Effective date
----------------------------------------------------------------------------------------------------------------
* * * * * * *
U048..................................... All.............................. Aug. 8, 1990.
----------------------------------------------------------------------------------------------------------------
[[Page 271]]
Appendix VIII to Part 268--LDR Effective Dates of Injected
Prohibited Hazardous Wastes
National Capacity LDR Variances for UIC Wastes \a\
----------------------------------------------------------------------------------------------------------------
Waste code Waste category Effective date
----------------------------------------------------------------------------------------------------------------
F001-F005............................. All spent F001-F005 solvent containing Aug. 8, 1990.
less than 1 percent total F001-F005
solvent constituents.
D001 (except High TOC Ignitable All..................................... Feb. 10, 1994.
Liquids Subcategory)c.
D001 (High TOC Ignitable Nonwastewater........................... Sept. 19, 1995.
Characteristic Liquids Subcategory).
D002b................................. All..................................... May 8, 1992.
D002c................................. All..................................... Feb. 10, 1994.
D003 (cyanides)....................... All..................................... May 8, 1992.
D003 (sulfides)....................... All..................................... May 8, 1992.
D003 (explosives, reactives).......... All..................................... May 8, 1992.
D007.................................. All..................................... May 8, 1992.
D009.................................. Nonwastewater........................... May 8, 1992.
D012.................................. All..................................... Sept. 19, 1995.
D013.................................. All..................................... Sept. 19, 1995.
D014.................................. All..................................... Sept. 19, 1995.
D015.................................. All..................................... Sept. 19, 1995.
D016.................................. All..................................... Sept. 19, 1995.
D017.................................. All..................................... Sept. 19, 1995.
D018.................................. All, including mixed with radioactive Apr. 8, 1998.
wastes.
D019.................................. All, including mixed with radioactive Apr. 8, 1998.
wastes.
D020.................................. All, including mixed with radioactive Apr. 8, 1998.
wastes.
D021.................................. All, including mixed with radioactive Apr. 8, 1998.
wastes.
D022.................................. All, including mixed with radioactive Apr. 8, 1998.
wastes.
D023.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D024.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D025.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D026.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D027.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D028.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D029.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D030.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D031.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D032.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D033.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D034.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D035.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D036.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D037.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D038.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D039.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D040.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D041.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D042.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
D043.................................. All, including mixed radioactive wastes. Apr. 8, 1998.
F007.................................. All..................................... June 8, 1991.
F032.................................. All, including mixed radioactive wastes. May 12, 1999.
F034.................................. All, including mixed radioactive wastes. May 12,1999.
F035.................................. All, including mixed radioactive wastes. May 12, 1999.
F037.................................. All..................................... Nov. 8, 1992.
F038.................................. All..................................... Nov. 8, 1992.
F039.................................. Wastewater.............................. May 8, 1992.
K009.................................. Wastewater.............................. June 8, 1991.
K011.................................. Nonwastewater........................... June 8, 1991.
K011.................................. Wastewater.............................. May 8, 1992.
K011.................................. Nonwastewater........................... June 8, 1991.
K011.................................. Wastewater.............................. May 8, 1992.
K013.................................. Nonwastewater........................... June 8, 1991.
K013.................................. Wastewater.............................. May 8, 1992.
K014.................................. All..................................... May 8, 1992.
K016 (dilute)......................... All..................................... June 8, 1991.
K049.................................. All..................................... Aug. 8, 1990.
K050.................................. All..................................... Aug. 8, 1990.
K051.................................. All..................................... Aug. 8, 1990.
K052.................................. All..................................... Aug. 8, 1990.
K062.................................. All..................................... Aug. 8, 1990.
K071.................................. All..................................... Aug. 8, 1990.
K088.................................. All..................................... Jan. 8, 1997.
K104.................................. All..................................... Aug. 8, 1990.
[[Page 272]]
K107.................................. All..................................... Nov. 8, 1992.
K108.................................. All..................................... Nov. 9, 1992.
K109.................................. All..................................... Nov. 9, 1992.
K110.................................. All..................................... Nov. 9, 1992.
K111.................................. All..................................... Nov. 9, 1992.
K112.................................. All..................................... Nov. 9, 1992.
K117.................................. All..................................... June 30, 1995.
K118.................................. All..................................... June 30, 1995.
K123.................................. All..................................... Nov. 9, 1992.
K124.................................. All..................................... Nov. 9, 1992.
K125.................................. All..................................... Nov. 9, 1992.
K126.................................. All..................................... Nov. 9, 1992.
K131.................................. All..................................... June 30, 1995.
K132.................................. All..................................... June 30, 1995.
K136.................................. All..................................... Nov. 9, 1992.
K141.................................. All..................................... Dec. 19, 1994.
K142.................................. All..................................... Dec. 19, 1994.
K143.................................. All..................................... Dec. 19, 1994.
K144.................................. All..................................... Dec. 19, 1994.
K145.................................. All..................................... Dec. 19, 1994.
K147.................................. All..................................... Dec. 19, 1994.
K148.................................. All..................................... Dec. 19, 1994.
K149.................................. All..................................... Dec. 19, 1994.
K150.................................. All..................................... Dec. 19, 1994.
K151.................................. All..................................... Dec. 19, 1994.
K156.................................. All..................................... July 8, 1996.
K157.................................. All..................................... July 8, 1996.
K158.................................. All..................................... July 8, 1996.
K159.................................. All..................................... July 8, 1996.
K160.................................. All..................................... July 8, 1996.
K161.................................. All..................................... July 8, 1996.
NA.................................... Newly identified mineral processing May 26, 2000.
wastes from titanium dioxide production
and mixed radioactive/newly identified
D004-D011 characteristic wastes and
mineral processing wastes..
P127.................................. All..................................... July 8, 1996.
P128.................................. All..................................... July 8, 1996.
P185.................................. All..................................... July 8, 1996.
P188.................................. All..................................... July 8, 1996.
P189.................................. All..................................... July 8, 1996.
P190.................................. All..................................... July 8, 1996.
P191.................................. All..................................... July 8, 1996.
P192.................................. All..................................... July 8, 1996.
P194.................................. All..................................... July 8, 1996.
P196.................................. All..................................... July 8, 1996.
P197.................................. All..................................... July 8, 1996.
P198.................................. All..................................... July 8, 1996.
P199.................................. All..................................... July 8, 1996.
P201.................................. All..................................... July 8, 1996.
P202.................................. All..................................... July 8, 1996.
P203.................................. All..................................... July 8, 1996.
P204.................................. All..................................... July 8, 1996.
P205.................................. All..................................... July 8, 1996.
U271.................................. All..................................... July 8, 1996.
U277.................................. All..................................... July 8, 1996.
U278.................................. All..................................... July 8, 1996.
U279.................................. All..................................... July 8, 1996.
U280.................................. All..................................... July 8, 1996.
U328.................................. All..................................... Nov. 9, 1992.
U353.................................. All..................................... Nov. 9, 1992.
U359.................................. All..................................... Nov. 9, 1992.
U364.................................. All..................................... July 8, 1996.
U365.................................. All..................................... July 8, 1996.
U366.................................. All..................................... July 8, 1996.
U367.................................. All..................................... July 8, 1996.
U372.................................. All..................................... July 8, 1996.
U373.................................. All..................................... July 8, 1996.
U375.................................. All..................................... July 8, 1996.
U376.................................. All..................................... July 8, 1996.
U377.................................. All..................................... July 8, 1996.
U378.................................. All..................................... July 8, 1996.
U379.................................. All..................................... July 8, 1996.
[[Page 273]]
U381.................................. All..................................... July 8, 1996.
U382.................................. All..................................... July 8, 1996.
U383.................................. All..................................... July 8, 1996.
U384.................................. All..................................... July 8, 1996.
U385.................................. All..................................... July 8, 1996.
U386.................................. All..................................... July 8, 1996.
U387.................................. All..................................... July 8, 1996.
U389.................................. All..................................... July 8, 1996.
U390.................................. All..................................... July 8, 1996.
U391.................................. All..................................... July 8, 1996.
U392.................................. All..................................... July 8, 1996.
U395.................................. All..................................... July 8, 1996.
U396.................................. All..................................... July 8, 1996.
U400.................................. All..................................... July 8, 1996.
U401.................................. All..................................... July 8, 1996.
U402.................................. All..................................... July 8, 1996.
U403.................................. All..................................... July 8, 1996.
U404.................................. All..................................... July 8, 1996.
U407.................................. All..................................... July 8, 1996.
U409.................................. All..................................... July 8, 1996.
U410.................................. All..................................... July 8, 1996.
U411.................................. All..................................... July 8, 1996.
----------------------------------------------------------------------------------------------------------------
a Wastes that are deep well disposed on-site receive a six-month variance, with restrictions effective in
November 1990.
b Deepwell injected D002 liquids with a pH less than 2 must meet the California List treatment standards on
August 8, 1990.
c Managed in systems defined in 40 CFR 144.6(e) and 14.6(e) as Class V injection wells, that do not engage in
CWA-equivalent treatment before injection.
Note: This table is provided for the convenience of the reader.
[62 FR 26037, May 12, 1997, as amended at 63 FR 28752, May 26, 1998]
Appendix IX to Part 268--Extraction Procedure (EP) Toxicity Test Method
and Structural Integrity Test (Method 1310)
Note: The EP (Method 1310) is published in ``Test Methods for
Evaluating Solid Waste, Physical/Chemical Methods,'' EPA Publication SW-
846, as incorporated by reference in Sec. 260.11 of this chapter.
[58 FR 46051, Aug. 31, 1993]
Appendix X to Part 268 [Reserved]
Appendix XI to Part 268--Metal Bearing Wastes Prohibited
From Dilution in a Combustion Unit According to 40 CFR
268.3(c) \1\
---------------------------------------------------------------------------
\1\ A combustion unit is defined as any thermal technology subject
to 40 CFR part 264, subpart O; Part 265, subpart O; and/or 266, subpart
H.
------------------------------------------------------------------------
Waste code Waste description
------------------------------------------------------------------------
D004......................... Toxicity Characteristic for Arsenic.
D005......................... Toxicity Characteristic for Barium.
D006......................... Toxicity Characteristic for Cadmium.
D007......................... Toxicity Characteristic for Chromium.
D008......................... Toxicity Characteristic for Lead.
D009......................... Toxicity Characteristic for Mercury.
D010......................... Toxicity Characteristic for Selenium.
D011......................... Toxicity Characteristic for Silver.
F006......................... Wastewater treatment sludges from
electroplating operations except from
the following processes: (1) sulfuric
acid anodizing of aluminum; (2) tin
plating carbon steel; (3) zinc plating
(segregated basis) on carbon steel; (4)
aluminum or zinc-plating on carbon
steel; (5) cleaning/stripping associated
with tin, zinc and aluminum plating on
carbon steel; and (6) chemical etching
and milling of aluminum.
F007......................... Spent cyanide plating bath solutions from
electroplating operations.
F008......................... Plating bath residues from the bottom of
plating baths from electroplating
operations where cyanides are used in
the process.
F009......................... Spent stripping and cleaning bath
solutions from electroplating operations
where cyanides are used in the process.
F010......................... Quenching bath residues from oil baths
from metal treating operations where
cyanides are used in the process.
[[Page 274]]
F011......................... Spent cyanide solutions from salt bath
pot cleaning from metal heat treating
operations.
F012......................... Quenching waste water treatment sludges
from metal heat treating operations
where cyanides are used in the process.
F019......................... Wastewater treatment sludges from the
chemical conversion coating of aluminum
except from zirconium phosphating in
aluminum car washing when such
phosphating is an exclusive conversion
coating process.
K002......................... Wastewater treatment sludge from the
production of chrome yellow and orange
pigments.
K003......................... Wastewater treatment sludge from the
production of molybdate orange pigments.
K004......................... Wastewater treatment sludge from the
production of zinc yellow pigments.
K005......................... Wastewater treatment sludge from the
production of chrome green pigments.
K006......................... Wastewater treatment sludge from the
production of chrome oxide green
pigments (anhydrous and hydrated).
K007......................... Wastewater treatment sludge from the
production of iron blue pigments.
K008......................... Oven residue from the production of
chrome oxide green pigments.
K061......................... Emission control dust/sludge from the
primary production of steel in electric
furnaces.
K069......................... Emission control dust/sludge from
secondary lead smelting.
K071......................... Brine purification muds from the mercury
cell processes in chlorine production,
where separately prepurified brine is
not used.
K100......................... Waste leaching solution from acid
leaching of emission control dust/sludge
from secondary lead smelting.
K106......................... Sludges from the mercury cell processes
for making chlorine.
P010......................... Arsenic acid H3 AsO4
P011......................... Arsenic oxide As2 O5
P012......................... Arsenic trioxide
P013......................... Barium cyanide
P015......................... Beryllium
P029......................... Copper cyanide Cu(CN)
P074......................... Nickel cyanide Ni(CN)2
P087......................... Osmium tetroxide
P099......................... Potassium silver cyanide
P104......................... Silver cyanide
P113......................... Thallic oxide
P114......................... Thallium (l) selenite
P115......................... Thallium (l) sulfate
P119......................... Ammonium vanadate
P120......................... Vanadium oxide V2 O5
P121......................... Zinc cyanide.
U032......................... Calcium chromate.
U145......................... Lead phosphate.
U151......................... Mercury.
U204......................... Selenious acid.
U205......................... Selenium disulfide.
U216......................... Thallium (I) chloride.
U217......................... Thallium (I) nitrate.
------------------------------------------------------------------------
[61 FR 15658, Apr. 8, 1996]